Electrodeposition of lithium phthalocyanine thin films: Part I. Structure and morphology

1999 ◽  
Vol 14 (5) ◽  
pp. 2162-2172 ◽  
Author(s):  
M. Brinkmann ◽  
S. Graff ◽  
C. Chaumont ◽  
J-J. André
Keyword(s):  
Thin Film ◽  
Thin Films ◽  
Indium Tin Oxide ◽  
Film Growth ◽  
Oxidation Potential ◽  
Thin Film Growth ◽  
Ex Situ ◽  
X Ray Diffraction ◽  
X Ray ◽  
Film Synthesis

A new thin film synthesis route based on the electrochemical oxidation of PcLi2 and deposition of lithium phthalocyanine (PcLi) onto indium tin oxide (ITO) substrate is demonstrated. The effects on the thin film morphology of various parameters such as the electrolysis time, the nature of the solvent, and the oxidation potential are investigated. The thin film growth is studied via x-ray diffraction, potential step experiments, and ex situ scanning electron microscopy. Various morphologies of the x-form thin films are observed for different electrolysis times and solvents. Thin films grown in acetonitrile of thickness above 1 μm consist in unidirectionally oriented needle-shaped crystallites.

Combinatorial (Ba,Sr)TiO3 thin film growth: X-ray diffraction and Raman spectroscopy

2009 ◽  
Vol 106 (3) ◽  
pp. 034108 ◽  
Author(s):  
H. Bouyanfif ◽  
J. Wolfman ◽  
M. El Marssi ◽  
Y. Yuzyuk ◽  
R. Bodeux ◽  
...  
Keyword(s):  
Thin Film ◽  
Raman Spectroscopy ◽  
Film Growth ◽  
Thin Film Growth ◽  
Tio3 Thin Film ◽  
X Ray Diffraction ◽  
X Ray

X-ray diffraction analysis of YBaCuO ultra-thin film growth

1997 ◽  
Vol 251 (1-2) ◽  
pp. 65-69 ◽  
Author(s):  
G. Linker ◽  
D. Hüttner ◽  
O. Meyer ◽  
M. Ohkubo ◽  
J. Reiner
Keyword(s):  
Thin Film ◽  
Diffraction Analysis ◽  
Film Growth ◽  
Thin Film Growth ◽  
X Ray Diffraction ◽  
X Ray ◽  
Ultra Thin Film

In-situ study of Ni–Ti thin film growth on a TiN intermediate layer by X-ray diffraction

2007 ◽  
Vol 126 (1) ◽  
pp. 332-337 ◽  
Author(s):  
R MARTINS ◽  
N SCHELL ◽  
R SILVA ◽  
L PEREIRA ◽  
K MAHESH ◽  
...  
Keyword(s):  
Thin Film ◽  
Intermediate Layer ◽  
Film Growth ◽  
Thin Film Growth ◽  
X Ray Diffraction ◽  
X Ray ◽  
In Situ Study

scholarly journals Epitaxial thin-film growth ofC60onVSe2studied with scanning tunneling microscopy and x-ray diffraction

1999 ◽  
Vol 59 (20) ◽  
pp. 13394-13400 ◽  
Author(s):  
R. Schwedhelm ◽  
J.-P. Schlomka ◽  
S. Woedtke ◽  
R. Adelung ◽  
L. Kipp ◽  
...  
Keyword(s):  
Thin Film ◽  
Scanning Tunneling Microscopy ◽  
Film Growth ◽  
Thin Film Growth ◽  
Scanning Tunneling ◽  
X Ray Diffraction ◽  
Tunneling Microscopy ◽  
Epitaxial Thin Film ◽  
X Ray ◽  
Epitaxial Thin Film Growth

scholarly journals Surface-Controlled Crystal Alignment of Naphthyl End-Capped Oligothiophene on Graphene: Thin-Film Growth Studied by in Situ X-ray Diffraction

Langmuir ◽  
2020 ◽  
Vol 36 (8) ◽  
pp. 1898-1906 ◽  
Author(s):  
Mathias K. Huss-Hansen ◽  
Martin Hodas ◽  
Nada Mrkyvkova ◽  
Jakub Hagara ◽  
Bjarke B. E. Jensen ◽  
...  
Keyword(s):  
Thin Film ◽  
Film Growth ◽  
Thin Film Growth ◽  
X Ray Diffraction ◽  
X Ray ◽  
Crystal Alignment

In SituReal-Time X-Ray Diffraction During Thin Film Growth of Pentacene

2012 ◽  
Vol 566 (1) ◽  
pp. 18-21 ◽  
Author(s):  
T. Watanabe ◽  
T. Hosokai ◽  
T. Koganezawa ◽  
N. Yoshimoto
Keyword(s):  
Thin Film ◽  
Film Growth ◽  
Thin Film Growth ◽  
X Ray Diffraction ◽  
X Ray

scholarly journals In Situ X-ray Measurements to Follow the Crystallization of BaTiO3 Thin Films during RF-Magnetron Sputter Deposition

2021 ◽  
Vol 11 (19) ◽  
pp. 8970
Author(s):  
Peter Walter ◽  
Markus Ilchen ◽  
JanTorben Roeh ◽  
Wiebke Ohm ◽  
Christian Bonar Zeuthen ◽  
...  
Keyword(s):  
Thin Film ◽  
Thin Films ◽  
Film Growth ◽  
Structural Evolution ◽  
Thin Film Growth ◽  
Structure Evolution ◽  
Special Focus ◽  
Time Resolved ◽  
X Ray

Here, we report on adding an important dimension to the fundamental understanding of the evolution of the thin film micro structure evolution. Thin films have gained broad attention in their applications for electro-optical devices, solar-cell technology, as well storage devices. Deep insights into fundamental functionalities can be realized via studying crystallization microstructure and formation processes of polycrystalline or epitaxial thin films. Besides the fundamental aspects, it is industrially important to minimize cost which intrinsically requires lower energy consumption at increasing performance which requires new approaches to thin film growth in general. Here, we present a state of the art sputtering technique that allows for time-resolved in situ studies of such thin film growth with a special focus on the crystallization via small angle scattering and X-ray diffraction. Focusing on the crystallization of the example material of BaTiO3, we demonstrate how a prototypical thin film forms and how detailed all phases of the structural evolution can be identified. The technique is shaped to enable a versatile approach for understanding and ultimately controlling a broad variety of growth processes, and more over it demonstrate how to in situ investigate the influence of single high temperature sputtering parameters on the film quality. It is shown that the whole evolution from nucleation, diffusion adsorption and grain growth to the crystallization can be observed during all stages of thin film growth as well as quantitatively as qualitatively. This can be used to optimize thin-film quality, efficiency and performance.

scholarly journals In-situ Observation of 2-Dimensional X-ray Diffraction of Organic Thin-film Growth by Synchrotron Radiation

Hyomen Kagaku ◽  
2014 ◽  
Vol 35 (4) ◽  
pp. 190-195 ◽  
Author(s):  
Noriyuki YOSHIMOTO ◽  
Takeshi WATANABE ◽  
Tomoyuki KOGANEZAWA ◽  
Mamoru KIKUCHI ◽  
Ichiro HIROSAWA
Keyword(s):  
Thin Film ◽  
Synchrotron Radiation ◽  
Film Growth ◽  
Thin Film Growth ◽  
In Situ Observation ◽  
Organic Thin Film ◽  
X Ray Diffraction ◽  
X Ray

In situenergy-dispersive x-ray diffraction system for time-resolved thin-film growth studies

2003 ◽  
Vol 14 (3) ◽  
pp. 336-345 ◽  
Author(s):  
K Ellmer ◽  
R Mientus ◽  
V Wei  ◽  
H Rossner
Keyword(s):  
Thin Film ◽  
Film Growth ◽  
Thin Film Growth ◽  
X Ray Diffraction ◽  
Time Resolved ◽  
X Ray ◽  
Growth Studies
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