Effect of powder morphology on the microstructure and mechanical property gradients in stainless steels induced by thermal gradients in spark plasma sintering

MRS Advances ◽  
2021 ◽  
Author(s):  
Alexander D. Preston ◽  
Kaka Ma
Nanomaterials ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 1150
Author(s):  
Nicolás A. Ulloa-Castillo ◽  
Roberto Hernández-Maya ◽  
Jorge Islas-Urbano ◽  
Oscar Martínez-Romero ◽  
Emmanuel Segura-Cárdenas ◽  
...  

This article focuses on exploring how the electrical conductivity and densification properties of metallic samples made from aluminum (Al) powders reinforced with 0.5 wt % concentration of multi-walled carbon nanotubes (MWCNTs) and consolidated through spark plasma sintering (SPS) process are affected by the carbon nanotubes dispersion and the Al particles morphology. Experimental characterization tests performed by scanning electron microscopy (SEM) and by energy dispersive spectroscopy (EDS) show that the MWCNTs were uniformly ball-milled and dispersed in the Al surface particles, and undesirable phases were not observed in X-ray diffraction measurements. Furthermore, high densification parts and an improvement of about 40% in the electrical conductivity values were confirmed via experimental tests performed on the produced sintered samples. These results elucidate that modifying the powder morphology using the ball-milling technique to bond carbon nanotubes into the Al surface particles aids the ability to obtain highly dense parts with increasing electrical conductivity properties.


2021 ◽  
Vol 1033 ◽  
pp. 93-97
Author(s):  
Tanapon Tansiranon ◽  
Katsuyoshi Kondoh ◽  
Kazuhiro Ishikawa ◽  
Yoji Miyajima ◽  
Anak Khantachawana

This paper aims to investigate effect of spark plasma sintering temperature on mechanical property of Ti + ZrO2. The samples were prepared by SPS system with the different sintering temperature containing 900, 1,000, and 1,100 oC under the pressing pressure of 30 MPa in vacuum. The results show that hardness of Ti + 2 wt.% ZrO2 alloy increases with increasing sintering temperature. The highest hardness was 363 HV while suitable temperature for sintering Ti + 2 wt.% ZrO2 alloy was 1,100 oC. Further, the microstructure and crystal structure of all samples were single-α-phase structure with different in elements dispersion, which was related to amount of lattice expansion in the HCP structure.


Author(s):  
Rayappa Shrinivas Mahale ◽  
V. Shamanth ◽  
P.C. Sharath ◽  
R. Shashanka ◽  
K. Hemanth

2009 ◽  
Vol 2009.6 (0) ◽  
pp. 277-278
Author(s):  
Michiya MURAKAMI ◽  
Taku WATANABE ◽  
Haruka TSURUTA ◽  
Hiroshi IZUI ◽  
Michiharu OKANO

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