Preparation of Large Crystals of Photoactive Yellow Protein for Neutron Diffraction and High Resolution Crystal Structure Analysis†

2007 ◽  
Vol 83 (2) ◽  
pp. 336-338 ◽  
Author(s):  
Shigeo Yamaguchi ◽  
Hironari Kamikubo ◽  
Nobutaka Shimizu ◽  
Yoichi Yamazaki ◽  
Yasushi Imamoto ◽  
...  
Author(s):  
H. J. Berthold ◽  
E. Vonholdt ◽  
R. Wartchow ◽  
T. Vogt

AbstractNHA single crystal structure analysis of NThe deuterated compound NThe structures of the ordered low temperature phases will be reported separately.


2013 ◽  
Vol 53 (supplement1-2) ◽  
pp. S200
Author(s):  
Hiroshi Matsumoto ◽  
Yoichi Yamazaki ◽  
Hironari Kamikubo ◽  
Mariko Yamaguchi ◽  
Mikio Kataoka

2004 ◽  
Vol 37 (5) ◽  
pp. 786-790 ◽  
Author(s):  
Masatomo Yashima ◽  
Masahiko Tanaka

Accurate crystal structure analysis at high temperatures is an important challenge in science and technology. A new electric furnace for the measurement of high-resolution (δd/d= 0.03%) synchrotron radiation powder diffraction profiles from materials at high temperatures (up to 1900 K in air) has been designed and fabricated. This furnace consists of a ceramic refractory with MoSi2heaters, an aluminium body cooled by flowing water, and a sample stage with a spinner and a controller for sample-height adjustment.In situsynchrotron powder diffraction measurement for a calcium titanate perovskite specimen at 1674 K has been performed using the furnace at beamline 3A of the Photon Factory. The electron density distribution of the cubic perovskite at 1674 K was successfully obtained using a combination of Rietveld refinement, the maximum-entropy method (MEM) and MEM-based pattern-fitting techniques. The Ti atoms exhibit covalent bonding with the O atoms in the cubic CaTiO3perovskite at this temperature, while the Ca atoms are ionic. These results indicate that the new furnace yields high-quality data for accurate crystal structure analysis.


2011 ◽  
Vol 44 (16) ◽  
pp. 6441-6452 ◽  
Author(s):  
Kaewkan Wasanasuk ◽  
Kohji Tashiro ◽  
Makoto Hanesaka ◽  
Tokashi Ohhara ◽  
Kazuo Kurihara ◽  
...  

Sign in / Sign up

Export Citation Format

Share Document