scholarly journals Effect of Heat Treatment of Si3N4 on Grain Growth Behavior and Grain Boundary Structure

1997 ◽  
Vol 105 (1219) ◽  
pp. 218-222
Author(s):  
Naoto HIROSAKI ◽  
Hideaki MATSUBARA
2013 ◽  
Vol 753 ◽  
pp. 377-382 ◽  
Author(s):  
Suk Joong L. Kang

This paper reviews our recent investigations on grain growth in ceramics. Grain growth behavior has been found to be governed by the grain boundary structure: normal growth with a stationary relative grain size distribution for rough boundaries and non-normal (nonstationary) growth for faceted boundaries. Based on the concept of nonlinear migration of faceted boundaries, the mixed control model of grain growth is introduced and the principle of microstructural evolution is deduced. This principle states that various types of grain growth behavior are predicted as a result of the coupling effect between the maximum driving force for growth and the critical driving force for appreciable migration of the boundary. A wealth of experimental results supports the theoretical predictions of grain growth behavior, showing the generality of the suggested principle of microstructural evolution. Application of this principle is also demonstrated for the fabrication of single crystals as well as polycrystals with desired microstructures.


1998 ◽  
Vol 13 (12) ◽  
pp. 3449-3452 ◽  
Author(s):  
Takahisa Yamamoto ◽  
Yuichi Ikuhara ◽  
Katsuro Hayashi ◽  
Taketo Sakuma

Grain boundary structure was examined in 0.1 mol% TiO2-excess BaTiO3 by high-resolution electron microscopy (HRTEM) and electron energy loss spectroscopy (EELS). Their grain boundaries were mostly faceted with {210} type habit. The faceted boundaries were characterized to be associated with an extra Ti–O2 bond with the rutile-like structure. The grain growth behavior in a small TiO2-excess BaTiO3 is discussed from the viewpoint of grain boundary structure.


2007 ◽  
Vol 539-543 ◽  
pp. 4087-4092 ◽  
Author(s):  
Won Bae Lee ◽  
Chang Yong Lee ◽  
Yun Mo Yeon ◽  
Jong Bong Lee ◽  
Shur Chang Chae ◽  
...  

The grain growth behavior and mechanical properties in the friction stir weld zone after post weld heat treatment (PWHT) have been investigated. As PWHT temperature increased, a normal grain growth of as-welded equaxied grains ceased and abnormally grown grains with elongated shape coarsened. Huge elongated grains changed into smaller equaxied grains at 500°C. In case of lower heat input condition, abnormal grain growth initiated faster due to smaller initial grain size. The weld zone with bigger initial grains had advantages to maintain the thermal stability at high temperature. The hardness near the weld zone was almost recovered to the 95% of the unaffected base metal at 500 °C and the weld zone under lower heat input condition resulted in the homogeneous recovery through the whole weld zone.


1999 ◽  
Vol 32 (1-4) ◽  
pp. 187-195 ◽  
Author(s):  
V. Sursaeva ◽  
U. Czubayko ◽  
A. Touflin

Changes of the grain boundary character distribution and texture during normal grain growth have been investigated using the SAC-SEM based method and a 4 circle X-ray texture goniometer on A1 strips with columnar structure. The microstructure of the strips consists of regions with oriented (clusters) and randomly oriented grains. All changes of microstructure are outside the clusters during normal grain growth and consequently no texture change was observed.


2020 ◽  
Vol 321 ◽  
pp. 03004
Author(s):  
Jinghao Li ◽  
Manuel Sage ◽  
Xianglin Zhou ◽  
Mathieu Brochu ◽  
Yaoyao Fiona Zhao

Metal additive manufacturing (MAM) technology is now changing the pattern of the high-end manufacturing industry, among which MAM fabricated Ti6Al4V has been far the most extensively investigated material and attracts a lot of research interests. This work established a deep neural network (DNN) to investigate the grain boundary in competitive grain growth for a bi-crystal system, the column β grains of Ti6Al4V as an example. Because of the limited number of experimental samples, the DNN is trained based on the data coming from the Geometrical Limited criterion. A series of direct energy deposition experiment using Ti6Al4V is carried out under the Taguchi experimental design. The grain boundary angles between the column grains are measured in the experiment and used to evaluate the accuracy of DNN.


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