scholarly journals Determination of boron in cordierite base composite ceramic powders by ICP-AES after acid decomposition using a microwave oven.

1994 ◽  
Vol 43 (4) ◽  
pp. 351-354 ◽  
Author(s):  
Toshihisa MARUTA ◽  
Shigeru YOKOYAMA ◽  
Koichi NINOMIYA ◽  
Takeshi YAMANE
Keyword(s):  
Composite Ceramic ◽  
Microwave Oven ◽  
Ceramic Powders ◽  
Acid Decomposition ◽  
Base Composite

Decomposition of peroxobenzoic acid in benzene catalyzed by transition metal 2,4-pentanedionates

1984 ◽  
Vol 49 (3) ◽  
pp. 673-679 ◽  
Author(s):  
Pavel Lederer ◽  
Eva Mácová ◽  
Josef Vepřek-Šiška
Keyword(s):  
Transition Metal ◽  
Reaction Rate ◽  
Reaction Products ◽  
Acid Decomposition ◽  
Analogous Experiment ◽  
Catalytic Effects

The decomposition of peroxobenzoic acid in benzene was studied, and catalytic effects of Fe(III), Mn(III), Co(II), Co(III), and Cr(III) on the reaction rate and the composition of the reaction mixture were investigated. An analogous experiment carried out in perdeuterobenzene and determination of the distribution of deuterium in the reaction products provided evidence for the participation of the solvent in peroxobenzoic acid decomposition.

scholarly journals Determination of Arsenic, Chromium and Lead in titanium dioxide pigments by ICP- OES with Concomitant Metals Analyser

2019 ◽  
pp. 296-305
Author(s):  
Beena Sunilkumar ◽  
S. B. Singh
Keyword(s):  
Titanium Dioxide ◽  
Matrix Effects ◽  
Mineral Acid ◽  
Icp Oes ◽  
Acid Decomposition ◽  
Simple Method ◽  
Sample Dissolution ◽  
The Matrix ◽  
Generating System

A simple method has been developed for the determination of trace toxic elements like arsenic, lead and chromium in titanium dioxide pigment samples by ICP OES attached with a Concomitant Metals Analyser. Open mineral acid decomposition was used for sample dissolution employing a mixture of nitric and hydrofluoric acids. The continuous online generation of hydrides into the plasma was achieved through a concomitant metals analyser. The recovery of arsenic, lead and chromium and the matrix effects of titanium on these elements have been studied with spiking experiments. The proposed method has been successfully applied to the determination of arsenic and other elements in titanium pigment samples. The continuous hydride generating system, Concomitant Metals Analyser (CMA) improved the sensitivity of analysis nearly five times in pigment samples. The precision of the measurements was found to be less than 10% RSD.

The Study on Organic Acid Detection Using Lon Chromatography

2012 ◽  
Vol 424-425 ◽  
pp. 923-926
Author(s):  
Xiao Jian Hu ◽  
Wen Chen ◽  
Li Li ◽  
Jin Ping Zhou ◽  
Bao Shou Guo ◽  
...  
Keyword(s):  
Drinking Water ◽  
Convenient Method ◽  
High Sensitivity ◽  
Microwave Oven ◽  
Good Recovery ◽  
Microwave Technology ◽  
Trace Level ◽  
Recovery Treatment ◽  
Technology Foundation

A simple and convenient method for the determination of μ g/l level in the real drinking water bromate overcome traditional methods of defects. Argentina by electrolyzing the smallest electrode interference and then focus on extra chlorine use microwave technology foundation evaporation and concentration, the proposed method is very sensitive to the determination of trace level of the sales of the drinking water. And a microwave oven, drinking water ten times the sample can be concentrated in 10 minutes can get and good recovery. Treatment of the silver electrode, the method of interference, and can effectively eliminate the Cl- This method is successfully applied to the detection in water sample level in the trace. It is the advantage of the operation is simple, fast, high sensitivity, accurate results. This method can be applied widely, suitable for trace analysis of water samples.

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