Experimental Study of Silica Nano-Powder Synthesis Using a Diffusion Flame Reactor
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A chemical reactor is designed and developed to synthesize silica nano-powders by oxidation of tetraethyl orthosilicate (TEOS) using a three-port diffusion flame burner. Nano-silica powders were successfully synthesized. The particle size of the silica powders were confirmed by AFM and TEM techniques. Scanning electron microscopy (SEM) reveals that as-synthesized silica powders are in agglomerated condition. Phase analysis using XRD shows that the nano-silica in as-prepared condition is in amorphous form. However, during subsequent heat-treatment, it becomes crystalline.
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2008 ◽
Vol 34
(4)
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pp. 319-329
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2015 ◽
Vol 787
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pp. 732-735
2018 ◽
Vol 86
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pp. 128-138
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2008 ◽
Vol 28
(14)
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pp. 2731-2737
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