Effect of Double-layer Application on Dentin Bond Durability of One-step Self-etch Adhesives

2014 ◽  
Vol 39 (4) ◽  
pp. 416-426 ◽  
Author(s):  
M Taschner ◽  
M Kümmerling ◽  
U Lohbauer ◽  
L Breschi ◽  
A Petschelt ◽  
...  
Keyword(s):  
Bond Strength ◽  
Double Layer ◽  
Artificial Saliva ◽  
In Vitro Study ◽  
Adhesive Systems ◽  
Microtensile Bond Strength ◽  
Application Technique ◽  
One Step ◽  
Self Etch

SUMMARY Purpose The aim of this in vitro study was 1) to analyze the influence of a double-layer application technique of four one-step self-etch adhesive systems on dentin and 2) to determine its effect on the stability of the adhesive interfaces stored under different conditions. Materials and Methods Four different one-step self-etch adhesives were selected for the study (iBondSE, Clearfil S3 Bond, XenoV+, and Scotchbond Universal). Adhesives were applied according to manufacturers' instructions or with a double-layer application technique (without light curing of the first layer). After bonding, resin-dentin specimens were sectioned for microtensile bond strength testing in accordance with the nontrimming technique and divided into 3 subgroups of storage: a) 24 hours (immediate bond strength, T0), b) six months (T6) in artificial saliva at 37°C, or c) five hours in 10 % NaOCl at room temperature. After storage, specimens were stressed to failure. Fracture mode was assessed under a light microscope. Results At T0, iBond SE showed a significant increase in microtensile bond strength when the double-application technique was applied. All adhesive systems showed reduced bond strengths after six months of storage in artificial saliva and after storage in 10% NaOCl for five hours; however at T6, iBond SE, Clearfil S3 Bond, and XenoV+ showed significantly higher microtensile bond strength results for the double-application technique compared with the single-application technique. Scotchbond Universal showed no difference between single- or double-application, irrespective of the storage conditions. Conclusion The results of this study show that improvements in bond strength of one-step self-etch adhesives by using the double-application technique are adhesive dependent.

scholarly journals Effect of Different Application Techniques of Universal Bonding System on Microtensile Bond Strength of Bulk-Fill Composites to Primary and Permanent Dentin

2020 ◽  
Author(s):  
Masoud Fallahinejad Ghajari ◽  
Mahsa Sheikholeslamian ◽  
Amir Ghasemi ◽  
Leila Simaei
Keyword(s):  
Bond Strength ◽  
Failure Modes ◽  
In Vitro Study ◽  
Permanent Teeth ◽  
Microtensile Bond Strength ◽  
Universal Adhesive ◽  
Bonding System ◽  
The Mean ◽  
Self Etch

Objectives: This study aimed to determine the microtensile bond strength (μTBS) of a bulk-fill composite to permanent and primary coronal dentin using a universal adhesive in self-etch and total-etch modes. Materials and Methods: This in-vitro study was performed on 52 occlusal dentinal surfaces of human primary and permanent teeth. The crowns were cut to the gingival level. The 48 prepared dentin sections were randomly assigned to the following groups (n=13): A: Primary/Total-etch, B: Primary/Self-etch, C: Permanent/Total-etch, and D: Permanent/Self-etch. In groups A and C, after etching for 15 seconds, two layers of a universal bonding (Futurabond U) were applied and cured for 10 seconds. All samples were filled with a bulk-fill composite (x-trafil; VOCO) and cured for 40 seconds. The samples were cut to a bar-shaped dentin block with the dimensions of 1×1×1 mm3, and after 10,000 thermocycles, the μTBS test was accomplished at a crosshead speed of 1 mm/minute. The mean and standard deviation (SD) of μTBS were calculated, and the data were analyzed using two-way analysis of variance (ANOVA) and Fisher's exact test. Results: The mean μTBS was as follows: A: 15.03±2.0279, B: 11.11±2.4423, C: 23.50±4.8165, and D: 16.26±6.3200 MPa. Futurabond U showed a higher μTBS in the total-etch mode (P<0.001). The permanent teeth had greater μTBS than the primary teeth (P<0.001). Similar percentages of failure modes were observed in the total-etch groups but in the self-etch groups, most failures were in the form of adhesive and mixed. Conclusion: Greater μTBS was observed in the permanent teeth with the total-etch technique.

scholarly journals Analysis of micro-shear bond strength of self-etch adhesive systems with dentine: An in vitro study

2015 ◽  
Vol 5 (3) ◽  
pp. 185-188 ◽  
Author(s):  
Vijay Kumar Shakya ◽  
Rajeev Kumar Singh ◽  
Anjani Kumar Pathak ◽  
Balendra Pratap Singh ◽  
Anil Chandra ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
In Vitro Study ◽  
Vitro Study ◽  
Adhesive Systems ◽  
Self Etch

scholarly journals Aging Protocols and Their Effects on Bond Strength of Total-Etch and Self-Etch Adhesive Systems to Dentin

2020 ◽  
Vol 14 (1) ◽  
pp. 408-415
Author(s):  
Isabella A. Gomes ◽  
Mário G. N. Gomes ◽  
Flávia L. B. Amaral ◽  
Fabiana M. G. França ◽  
Roberta T. Basting ◽  
...  
Keyword(s):  
Bond Strength ◽  
Failure Mode ◽  
Failure Modes ◽  
Resin Composite ◽  
Artificial Saliva ◽  
Mixed Data ◽  
Adhesive Systems ◽  
One Step ◽  
Self Etch ◽  
Conventional Type

Objective: This study investigated whether different aging protocols have effects on the bond strength of total-etch and self-etch adhesive systems to dentin substrate. Methods: Molars were sectioned exposing the dentin, which was submitted to restorative procedures using two-step total-etch (ASB, Adper SingleBond2), two-step self-etch (CLF, Clearfil SEBond), or one-step self-etch (OPT, Optibond All-in-One) system and resin composite. The obtained blocks were sectioned to result in sticks to be submitted to bond strength and failure mode tests after 24h storage in distilled water (DW), or 180-day aging protocols in DW, artificial saliva (AS), citric acid (CA), or thermal cycling (TC). The types of failures were classified as adhesive, cohesive in dentin, cohesive in composite resin, and mixed. Data were analyzed using ANOVA followed by Tukey’s test (α=5%). The failure modes were descriptive under the relative frequencies form. Results: It was observed that ASB presented the higher bond strength(p<0.05), while CLF and OPT did not demonstrate differences between them(p>0.05) after 24h. The bond strength obtained with ASB significantly overcame that of OPT when stored in DW or AS for 180 days (p<0.001). In these storing mediums, ASB did not differ from CLF(p>0.05), while in CA or TC the values of CLF were significantly lower (p<0.001). In TC aging, the values presented by OPT did not differ from ASB(p>0.05), both of which had higher values than CLF(p<0.05). The predominant failure mode was adhesive. Conclusion: For the two-step total-etch and two-step self-etch adhesives, the influence of aging in AS and TC was equivalent to that of storage in DW. The most deleterious effects occurred in CA, a situation in which self-etch adhesives displayed worse performance than the conventional type.

scholarly journals Effect of Salivary Contamination on the Bond Strength of Total-etch and Self-etch Adhesive Systems: An in vitro Study

2012 ◽  
Vol 13 (5) ◽  
pp. 655-660 ◽  
Author(s):  
LM Ranganath ◽  
AG Rajesh ◽  
Robert M Justin ◽  
Hemalatha Paranthaman ◽  
Ranjith P Varghese
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
In Vitro Study ◽  
Single Bond ◽  
Adhesive Systems ◽  
Bonding Agents ◽  
Dentin Bonding ◽  
Etched Surface ◽  
Self Etch

ABSTRACT Aim To evaluate the influence of salivary contamination during dentin bonding procedures on shear bond strength and to investigate the effect of contaminant-removing treatments on the recovery of bond strength for two dentin-bonding agents. Materials and methods Seventy-seven human maxillary and mandibular molars were randomly divided into two groups for total-etch adhesive (Single bond-3M ESPE, USA) and self-etch primer (UniFil Bond-GC, Tokyo, Japan) and subjected to contamination with saliva. The data for each group were subjected to one-way analysis of variance (ANOVA) followed by the Student Newman-Keuls test to make comparisons among the groups (p < 0.05). Results Salivary contamination had less adverse effect on the shear bond strength of single bond total-etch adhesive when it was blot dried or washed. UniFil bond was tolerant of salivary contamination, except when contamination occurred after application of the primer. Conclusion In single bond adhesive, when the etched surface is contaminated by saliva, blotting the surface and applying the primer can recover the bond strength. Complete drying of the salivary contaminated surface should be avoided. In the UniFil bond groups, the repriming treatment (UF-V and UF-VI) resulted in the recovery of shear bond strength in the specimens contaminated after priming. Clinical significance The results of this study showed that total- etch adhesive (single bond) was not affected by salivary contamination on the etched surface when the bonding surface was kept moist. Self-etch adhesive (UniFil bond) also tolerated salivary contamination except when the contamination occurred after application of the primer. How to cite this article Justin RM, Paranthaman H, Rajesh AG, Varghese RP, Ranganath LM. Effect of Salivary Contamination on the Bond Strength of Total-etch and Selfetch Adhesive Systems: An in vitro Study. J Contemp Dent Pract 2012;13(5):655-660.

scholarly journals Effect of Casein Phosphopeptide Amorphous Calcium Phosphate Conditioning on Microtensile Bond Strength of Three Adhesive Systems to Deep Dentin

2021 ◽  
Author(s):  
Mohammad Ali Mohammadi Torkani ◽  
Sepideh Mesbahi ◽  
Amir Ardalan Abdollahi
Keyword(s):  
Calcium Phosphate ◽  
Bond Strength ◽  
Amorphous Calcium Phosphate ◽  
In Vitro Study ◽  
Adhesive Systems ◽  
Microtensile Bond Strength ◽  
Significant Difference ◽  
Bonferroni Test ◽  
Casein Phosphopeptide

Objectives: This study aimed to assess the effect of casein phosphopeptide amorphous calcium phosphate (CPP-ACP) on microtensile bond strength of three adhesive systems to deep dentin. Materials and Methods: In this in vitro study, the occlusal surface of 30 sound human third molars was sectioned at 2 mm below and above the cementoenamel junction. The samples were randomly divided into three groups of OptiBond Solo Plus, G-Bond, and Clearfil SE Bond. Before composite resin bonding, each group was divided into two subgroups with and without dentin preparation with CPP-ACP. The teeth were then sectioned into 1 mm rods (n=15), and their microtensile bond strength was measured at a crosshead speed of 0.5 mm/min. Data were analyzed using two-way ANOVA and post-hoc Bonferroni test. Results: There was no significant difference in bond strength of OptiBond Solo Plus (P=0.44) and Clearfil SE Bond (P=0.67) with/without CPP-ACP. A significant difference was found between the two subgroups of G-Bond in this respect (P<0.001). The differences in microtensile bond strength among all subgroups were significant (P<0.05). Conclusion: The microtensile bond strength in use of G-Bond is significantly higher following dentin treatment with CPP-ACP compared with no use of CPP-ACP.

Effect of Multiple Consecutive Applications of One-step Self-etch Adhesive on Microtensile Bond Strength

2009 ◽  
Vol 10 (2) ◽  
pp. 67-74 ◽  
Author(s):  
Hacer Deniz Arisu ◽  
Hüma Ömürlü ◽  
Evrim Eligüzeloğlu ◽  
Mine Üçtaşli
Keyword(s):  
Bond Strength ◽  
Adhesive System ◽  
Microtensile Bond Strength ◽  
One Step ◽  
Group 3 ◽  
Group 2 ◽  
Adhesive Application ◽  
Self Etch ◽  
Group 1

Abstract Aim The aim of this study was to evaluate the effects of multiple consecutive coatings of a one-step self-etch adhesive system (Clearfil Tri-S Bond) on the microtensile bond strength (MBS) to dentin. Methods and Materials Nine caries-free human lower third molars were sectioned perpendicular to the long axis to expose the mid-coronal dentin. The teeth were separated into three experimental groups (n=3) according to the number of adhesive resin coats applied. In Group 1 one layer of Clearfil Tri-S Bond was applied according to the manufacturer's instructions. In Group 2 and Group 3 the adhesive was applied in two and three layers, respectively. In these two groups the first layer was applied according to the manufacturer's instructions but the second and third layers of adhesive were not light cured after application. After the placement of the composite, the teeth were sectioned to obtain approximately 1 mm2 beams for testing. Eighteen beams were prepared for each group using the ‘non-trimming’ method. The MBS values of all specimens were tested, and fracture modes were then determined using a stereomicroscope. Results The mean MBS values (in MPa) of Group 1 (one coat of the adhesive) was significantly lower (p=0.04) than those of Group 3 (three applied coats of the adhesive). There were no statistically significant differences between Groups 1 and 2 and Groups 2 and 3. Conclusion Within the limitations of this in vitro study the application of multiple coats of a one-step self-etch adhesive may provide an increase in bond strength compared to the application of only one coat of adhesive. Clinical Significance Three consecutive coats of one-step self-etching adhesive application can improve MBS. Citation Arisu HD, Eligüzeloğlu E, Üçtaşli M, Ömürlü H. Effect of Multiple Consecutive Applications of One-step Self-etch Adhesive on Microtensile Bond Strength. J Contemp Dent Pract 2009 March; (10)2:067-074.

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