Effect of Multiple Consecutive Applications of One-step Self-etch Adhesive on Microtensile Bond Strength

2009 ◽  
Vol 10 (2) ◽  
pp. 67-74 ◽  
Author(s):  
Hacer Deniz Arisu ◽  
Hüma Ömürlü ◽  
Evrim Eligüzeloğlu ◽  
Mine Üçtaşli
Keyword(s):  
Bond Strength ◽  
Adhesive System ◽  
Microtensile Bond Strength ◽  
One Step ◽  
Group 3 ◽  
Group 2 ◽  
Adhesive Application ◽  
Self Etch ◽  
Group 1

Abstract Aim The aim of this study was to evaluate the effects of multiple consecutive coatings of a one-step self-etch adhesive system (Clearfil Tri-S Bond) on the microtensile bond strength (MBS) to dentin. Methods and Materials Nine caries-free human lower third molars were sectioned perpendicular to the long axis to expose the mid-coronal dentin. The teeth were separated into three experimental groups (n=3) according to the number of adhesive resin coats applied. In Group 1 one layer of Clearfil Tri-S Bond was applied according to the manufacturer's instructions. In Group 2 and Group 3 the adhesive was applied in two and three layers, respectively. In these two groups the first layer was applied according to the manufacturer's instructions but the second and third layers of adhesive were not light cured after application. After the placement of the composite, the teeth were sectioned to obtain approximately 1 mm2 beams for testing. Eighteen beams were prepared for each group using the ‘non-trimming’ method. The MBS values of all specimens were tested, and fracture modes were then determined using a stereomicroscope. Results The mean MBS values (in MPa) of Group 1 (one coat of the adhesive) was significantly lower (p=0.04) than those of Group 3 (three applied coats of the adhesive). There were no statistically significant differences between Groups 1 and 2 and Groups 2 and 3. Conclusion Within the limitations of this in vitro study the application of multiple coats of a one-step self-etch adhesive may provide an increase in bond strength compared to the application of only one coat of adhesive. Clinical Significance Three consecutive coats of one-step self-etching adhesive application can improve MBS. Citation Arisu HD, Eligüzeloğlu E, Üçtaşli M, Ömürlü H. Effect of Multiple Consecutive Applications of One-step Self-etch Adhesive on Microtensile Bond Strength. J Contemp Dent Pract 2009 March; (10)2:067-074.

scholarly journals An Evaluation of Shear Bond Strength of Self-Etch Adhesive on Pre-etched Enamel: An in vitro Study

2013 ◽  
Vol 14 (6) ◽  
pp. 1036-1038
Author(s):  
Abdul Mujeeb ◽  
Bhadra Rao ◽  
Satti Narayana Reddy ◽  
Kanchan Mehta ◽  
G Saritha
Keyword(s):  
Statistical Analysis ◽  
Bond Strength ◽  
Shear Bond Strength ◽  
Occlusal Surfaces ◽  
Group 3 ◽  
The Mean ◽  
Group 2 ◽  
Self Etch ◽  
Group 1

ABSTRACT Aim To determine the shear bond strength of self-etch adhesive G-bond on pre-etched enamel. Materials and methods Thirty caries free human mandibular premolars extracted for orthodontic purpose were used for the study. Occlusal surfaces of all the teeth were flattened with diamond bur and a silicon carbide paper was used for surface smoothening. The thirty samples were randomly grouped into three groups. Three different etch systems were used for the composite build up: group 1 (G-bond self-etch adhesive system), group 2 (G-bond) and group 3 (Adper single bond). Light cured was applied for 10 seconds with a LED unit for composite buildup on the occlusal surface of each tooth with 8 millimeters (mm) in diameter and 3 mm in thickness. The specimens in each group were tested in shear mode using a knife-edge testing apparatus in a universal testing machine across head speed of 1 mm/ minute. Shear bond strength values in Mpa were calculated from the peak load at failure divided by the specimen surface area. The mean shear bond strength of all the groups were calculated and statistical analysis was carried out using one-way Analysis of Variance (ANOVA). Results The mean bond strength of group 1 is 15.5 Mpa, group 2 is 19.5 Mpa and group 3 is 20.1 Mpa. Statistical analysis was carried out between the groups using one-way ANOVA. Group 1 showed statistically significant lower bond strength when compared to groups 2 and 3. No statistical significant difference between groups 2 and 3 (p < 0.05). Conclusion Self-etch adhesive G-bond showed increase in shear bond strength on pre-etched enamel. How to cite this article Rao B, Reddy SN, Mujeeb A, Mehta K, Saritha G. An Evaluation of Shear Bond Strength of Self-Etch Adhesive on Pre-etched Enamel: An In vitro Study. J Contemp Dent Pract 2013;14(6):1036-1038.

scholarly journals Comparative Evaluation of Self-etching Primers and Phosphoric Acid Effectiveness on Composite to Enamel Bond: An in vitro Study

2013 ◽  
Vol 14 (5) ◽  
pp. 790-795 ◽  
Author(s):  
G Vinay Kumar ◽  
Basanagouda S Patil ◽  
BK Raghavendra Rao ◽  
SM Sharathchandra ◽  
Reshma Hegde
Keyword(s):  
Phosphoric Acid ◽  
Bond Strength ◽  
Comparative Evaluation ◽  
In Vitro Study ◽  
Vitro Study ◽  
One Step ◽  
Group 3 ◽  
Group 2 ◽  
Group 1

ABSTRACT Aim The aim of the present study was to investigate the effectiveness of the one total-etch self-priming adhesive, one two-step self-etching primer adhesive, and one ‘all-in-one’ selfetching adhesive system on the adhesion of a resin composite to enamel. Materials and methods Thirty-six freshly extracted human mandibular molars were selected for this study. A flat area about 5 mm in diameter was created on the exposed mesial surface of enamel of each tooth by moist grinding with 320, 420 and 600 grit silicon carbide paper. Twelve teeth were randomly assigned into three groups. In group 1, Adper Easy One (3M ESPE), a one step self-etching primer adhesive was applied and light curing unit for 10 seconds. In group 2, Adper SE Plus, a twostep self-etching primer with bottle A containing the aqueous primer and bottle B containing the acidic adhesive was applied and light cured for 10 seconds. Group 3 (control)—etchant 37% phosphoric acid is applied to the surface for 15 seconds and rinsed with water and air dried and adhesive (single bond 2) is applied to the surface and tube is placed and light cured for 20 seconds. Composite material (Z350) was placed in the tube and light cured for 40 seconds in all the groups. Bond strength testing was done using universal testing machine at the enamel-composite interface. The debonded enamel surface was evaluated in stereomicroscope to assess the cohesive, adhesive or mixed fracture. Data was statistically analyzed by one way analysis of variance (ANOVA). Results Group 1 performed least among all groups with a mean score of 19.46 MPa. Group 2 had a mean score of 25.67 MPa. Group 3 had a mean score of 27.16 MPa. Conclusion Under the conditions of this in vitro study, the bond strength values of the two-step self-etching primer systems tested were similar to the total-etch. And, one step self-etching primers have lower bond strength compared to the total-etch. How to cite this article Patil BS, Rao BKR, Sharathchandra SM, Hegde R, Kumar GV. Comparative Evaluation of Selfetching Primers and Phosphoric Acid Effectiveness on Composite to Enamel Bond: An in vitro Study. J Contemp Dent Pract 2013;14(5):790-795.

scholarly journals The Effects of Prophylactic Ozone Pretreatment of Enamel on Shear Bond Strength of Orthodontic Brackets Bonded with Total or Self-Etch Adhesive Systems

2010 ◽  
Vol 04 (04) ◽  
pp. 367-373 ◽  
Author(s):  
Sevi Burcak Cehreli ◽  
Asli Guzey ◽  
Neslihan Arhun ◽  
Alev Cetinsahin ◽  
Bahtiyar Unver
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Orthophosphoric Acid ◽  
Ozone Treatment ◽  
Bond Failure ◽  
Group 4 ◽  
Group 3 ◽  
Group 2 ◽  
Self Etch ◽  
Group 1

Objectives: The aim of this in vitro study is to determine (1) shear bond strength (SBS) of brackets bonded with self-etch and total-etch adhesive after ozone treatment (2) bond failure interface using a modified Adhesive Remnant Index (ARI).Methods: 52 premolars were randomly assigned into four groups (n=13) and received the following treatments: Group 1: 30 s Ozone (Biozonix, Ozonytron, Vehos Medikal, Ankara, Turkey) application + Transbond Plus Self-Etching Primer (SEP) (3M) + Transbond XT (3M), Group 2: Transbond Plus SEP + Transbond XT, Group 3: 30 s Ozone application + 37% orthophosphoric acid + Transbond XT Primer (3M) + Transbond XT, Group 4: 37% orthophosphoric acid + Transbond XT Primer + Transbond XT. All samples were stored in deionised water at 37oC for 24 hours. Shear debonding test was performed by applying a vertical force to the base of the bracket at a cross-head speed of 1 mm/min.Results: The mean SBS results were Group 1: 10.48 MPa; Group 2: 8.89 MPa; Group 3: 9.41 MPa; Group 4: 9.82 MPa. One-Way Variance Test revealed that the difference between the groups was not statistically significant (P=0.267). Debonded brackets were examined by an optical microscope at X16 magnification to determine the bond failure interface using a modified ARI. The results were (mean) Group 1: 2.38; Group 2: 1.31; Group 3: 3.00; Group 4: 1.92. Multiple comparisons showed that Groups 1 and 2, 2 and 3, 3 and 4 were statistically different (P=0.014, P<.001 and P=0.025).Conclusions: Ozone treatment prior to bracket bonding does not affect the shear bond strength. (Eur J Dent 2010;4:367-373)

scholarly journals Shear Bond Strength Comparison between Two Orthodontic Adhesives and Self-Ligating and Conventional Brackets

2007 ◽  
Vol 77 (4) ◽  
pp. 701-706 ◽  
Author(s):  
Rodney G. Northrup ◽  
David W. Berzins ◽  
Thomas Gerard Bradley ◽  
William Schuckit
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Orthodontic Adhesives ◽  
Significant Difference ◽  
Conventional Brackets ◽  
Group 3 ◽  
Group 2 ◽  
Post Hoc ◽  
Group 1

Abstract Objective: To evaluate and compare the shear bond strengths of two adhesives using two types of brackets: a conventional and a self-ligating bracket system. Materials and Methods: Sixty extracted human premolars were collected. The premolars were randomly divided into three groups of 20 teeth. All three groups were direct bonded. Groups 1 and 2 used light-cured adhesive and primer (Transbond XT) with a conventional (Orthos) and a self-ligating bracket (Damon 2), respectively. Group 3 used a light-cured primer (Orthosolo) and a light-cured adhesive (Blūgloo) with a self-ligating bracket (Damon 2). The specimens were stored in distilled water at 37°C for 40 ± 2 hours, after which they were debonded and inspected for Adhesive Remnant Index (ARI) scoring. Results: The mean shear bond strength was 15.2 MPa for group 1, 23.2 MPa for group 2, and 24.8 MPa for group 3. A one-way analysis of variance and post hoc Tukey test showed significant differences in bond strength (P &lt; .001) between group 1 and groups 2 and 3 but no significant difference (P &gt; .05) between groups 2 and 3. A Weibull analysis demonstrated that all three groups provided sufficient bond strength with over 90% survival rate at normal masticatory and orthodontic force levels. A Kruskal-Wallis test showed no significant difference (P &gt; .05) in ARI scores among all three groups. Conclusions: All three groups demonstrated clinically acceptable bond strength. The Damon 2 self-ligating bracket exhibited satisfactory in vitro bond strength with both adhesive systems used.

scholarly journals A Comparative Evaluation of Three Commercially Available Dentin Desensitizers on the Shear Bond Strength of Composite Resins: An in vitro Study

2015 ◽  
Vol 5 (2) ◽  
pp. 65-68
Author(s):  
Shruti Patil ◽  
Prajna Shetty
Keyword(s):  
Bond Strength ◽  
Comparative Evaluation ◽  
Shear Bond Strength ◽  
In Vitro Study ◽  
Composite Resins ◽  
Group 4 ◽  
Group 3 ◽  
Group 2 ◽  
Group 1

ABSTRACT Background The dentin desensitizers available for in-office application for prevention and/or treatment of post restorative dentinal hypersensitivity, act by blocking the open dentinal tubules. In doing so, they may influence the bond strength of the restorative resins. Thus, the aim of the study was to evaluate the effect of desensitizers on the shear bond strength of dentin adhesives and to check the extent of dentinal tubule occlusion caused by these desensitizers. Materials and Methods Sixty-four premolars were randomly divided into four groups of sixteen each. The middle depth dentin was exposed by on the buccal surface and was etched using 37% phosphoric acid and rinsed. They were assigned to, Group 1: Gluma desensitizer, Group 2: Vivasens desensitizer, Group 3: Gluma Comfort Bond and desensitizer, and Group 4: Adper Single Bond 2. Composite resin post of 2 mm in height and width were built on these specimens. The samples were then mounted in acrylic resin blocks. Universal testing machine was used to test the shear bond strength. The data were analyzed using one-way analysis of variance (ANOVA) and post hoc Tukey's test. Results The mean values of the shear bond strength were for: Group 1—18.61 ± 1.03 MPa, Group 2—17.53 ± 1.36 MPa, Group 3—22.63 ± 1.61 MPa and Group 4—23.12 ± 1.02 MPa. There was a statistically significant difference (p < 0.05) among the groups. Conclusion The use of dentin desensitizers’ influences bond strength between the tooth and the adhesive. Among the various agents, the single bottle system containing Gluma comfort bond and desensitizer had the best adhesion among the desensitizer groups. How to cite this article Patil S, Naik B, Shetty P. A Comparative Evaluation of Three Commercially Available Dentin Desensitizers on the Shear Bond Strength of Composite Resins: An in vitro Study. J Contemp Dent 2015;5(2):65-68.

scholarly journals Resin Bonding of Self-Etch Adhesives to Bovine Dentin Bleached from Pulp Chamber

2016 ◽  
Vol 2016 ◽  
pp. 1-7
Author(s):  
Akiko Haruyama ◽  
Atsushi Kameyama ◽  
Junji Kato ◽  
Shinji Takemoto ◽  
Yutaka Oda ◽  
...  
Keyword(s):  
Bond Strength ◽  
Resin Composite ◽  
Adhesive System ◽  
Unit Group ◽  
Tooth Bleaching ◽  
Pulp Chamber ◽  
Halogen Light ◽  
Group 2 ◽  
Self Etch ◽  
Group 1

This study evaluated the microtensile bond strength (μTBS) of 1-step self-etch adhesives (1-SEAs) and 2-step self-etch adhesives (2-SEAs) to pulp chamber dentin immediately after bleaching with 2 types of common bleaching techniques. Pulp chamber dentin of bovine teeth was bleached using 30% hydrogen peroxide (H2O2) solution with quartz-tungsten-halogen light-curing unit (Group 1) and 3.5% H2O2-containing titanium dioxide (TiO2) (Pyrenees®) activated with 405-nm violet diode laser for 15 min (Group 2). Unbleached specimens were placed in distilled water for 15 min and used as controls. After treatment, dentin was bonded with resin composite using 1-SEA or 2-SEA and stored in water at 37°C for 24 h. Each specimen was sectioned and trimmed to an hourglass-shape andμTBS was measured. Fractured specimens were examined under a scanning electron microscope to determine fracture modes. All specimens in Group 1 failed before proper bonding tests. In Group 2, theμTBS of 2-SEA was significantly greater (with no failed specimens) than 1-SEA (where 21 out of 36 failed). These results indicate that 2-SEA is a better adhesive system than 1-SEA on bleached dentin. Our results also demonstrated that application of H2O2significantly decreases bond strength of resin to dentin; however, in the case of nonvital tooth bleaching, Pyrenees® is a better alternative to the conventional 30% H2O2bleaching.

scholarly journals Influence of adhesive system in bond strength of fiber glass posts to radicular dentin using dual cure resin cement

2014 ◽  
Vol 17 (1) ◽  
pp. 4 ◽  
Author(s):  
Daphne Camara Barcellos ◽  
Maria Filomena Rocha Lima Huhtala ◽  
Melissa Aline Silva ◽  
Ana Paula Martins Gomes ◽  
Lucas Teixeira Franco
Keyword(s):  
Bond Strength ◽  
Glass Fiber ◽  
Adhesive System ◽  
Single Bond ◽  
Pull Out ◽  
Fiber Posts ◽  
Glass Fiber Posts ◽  
Group 2 ◽  
Self Etch ◽  
Group 1

<p>The purpose of this study was to evaluate the bond strength between root dentin and glass fiber posts cemented with dual cure resinous cement associated with the conventional and self-etching adhesive systems. Twenty-four single-rooted human teeth were selected, and the crowns were removed at the cement enamel junction. The roots received biomechanical preparation and obturation followed by the intraradicular preparation compatible with a drill diameter of the glass fiber posts. The roots were divided into two groups, according to cementation protocol (n-12): Group 1 - etched with 37% phosphoric acid for 30 seconds, total-etch adhesive system Single Bond (3M ESPE)  and Enforce  resinous cement (Dentsply); Group 2 – self-etch adhesive system One Up Bond F (Tokuyama)  and Enforce  resinous cement (Dentsply). After the posts cementation, the roots were kept at 37<sup>0</sup> C for one week, and submitted to pull out test on the universal testing machine Emic to a traction speed of 1 mm/min. Data in MPa were submitted to the statistical <em>t</em>-test (5%). The <em>t</em>-test showed significant differences between the two groups (p=0.003). The average values in MPa (±standard-deviation) were: Group 1: 5.28(±3.25), Group 2: 10.05(±3.78). Enforce associated with the self-etch adhesive system One Up Bond F showed significantly higher bond strength values than Group 1 - Enforce associated with the total-etch adhesive system Single Bond.</p>

scholarly journals Effect of Ozone Application on the Resin-dentin Microtensile Bond Strength

2011 ◽  
Vol 36 (5) ◽  
pp. 537-544 ◽  
Author(s):  
PCF Rodrigues ◽  
JB Souza ◽  
CJ Soares ◽  
LG Lopes ◽  
C Estrela
Keyword(s):  
Bond Strength ◽  
Sodium Ascorbate ◽  
Acid Etching ◽  
Microtensile Bond Strength ◽  
Group 4 ◽  
Caries Treatment ◽  
Antioxidant Agents ◽  
Group 3 ◽  
Group 2 ◽  
Group 1

SUMMARY When ozone is used during caries treatment, bond strength can be compromised by the release of oxygen. The use of antioxidant agents neutralizes the free oxygen. The aim of this study was to evaluate the effects of ozone and sodium ascorbate on resin-dentin microtensile bond strength (μTBS). Forty human third molars were divided into four groups: Group 1, not treated with ozone; Group 2, ozone application followed by acid etching; Group 3, acid etching followed by ozone application; and Group 4, ozone and application of sodium ascorbate. Bonded beams (1.0 mm2) were tested under tension (0.5 mm min−1). The μTBS values were analyzed using one-way analysis of variance (ANOVA) and the Tukey test (p=0.05). All beams that fractured were analyzed under stereomicroscopy (40×). Group 1 had significantly higher μTBS values than Group 2 or 3. The μTBS values of Groups 1 and 4 were similar and higher than those of Group 2. The use of ozone in Group 2 resulted in lower values of μTBS in all conditions evaluated. The predominant failure mode was adhesive. The application of ozone decreased the μTBS of the dentin-composite resin interface. These values were reversed when compared with Groups 1 and 2 when sodium ascorbate was used.

scholarly journals Evaluation of Microtensile Bond Strength of Universal Self-etch Adhesive System to Wet and Dry Dentin

2020 ◽  
Vol 8 (D) ◽  
pp. 77-81
Author(s):  
Mohamed Ahmed Wakwak ◽  
Eslam Hassan Gabr ◽  
Ahmed Mohamed Elmarakby
Keyword(s):  
Bond Strength ◽  
Adhesive System ◽  
Solvent Free ◽  
Microtensile Bond Strength ◽  
Universal Adhesive ◽  
Significance Level ◽  
Significant Difference ◽  
One Step ◽  
Storage Times ◽  
Self Etch

BACKGROUND: The durability of dentin-resin interfaces with the universal adhesive system is a crucial characteristic with chemical interactions between the exposed collagen and the adhesive monomers, but it is still compromised with wet and dry mode. AIM: The present study evaluated the effect of dentin wetness and solvents containing of one-step self-etch adhesives on the microtensile bond strength (μTBS) of dentin at different storage times. METHODS: Occlusal dentin of 54 extracted human molars was exposed. Each adhesive agent was applied according to manufacturer instructions to wet and dry dentin surfaces. Composite resin was incrementally built up. Bond strengths to dentin were determined using the μTBS test after water storage for 24 h, 1 month, and 6 months. One-way ANOVA was used to compare between more than two non-related samples. The significance level was set at p ≤ 0.05. RESULTS: Dryness of dentin increases the μTBS with solvent-containing adhesives while decrease the μTBS with solvent-free adhesive. There was an increase in microtensile bond strength values in the case of ethanol water-based self-etch adhesive over time. No statistically significant difference was found among different storage times regarding μTBS for solvent-free adhesive, while a statistically significant difference was found among different storage times in μTBS for solvent-containing adhesives. CONCLUSION: Universal adhesive systems improve the durability and stability of dentin bond strength.

Effect of Double-layer Application on Dentin Bond Durability of One-step Self-etch Adhesives

2014 ◽  
Vol 39 (4) ◽  
pp. 416-426 ◽  
Author(s):  
M Taschner ◽  
M Kümmerling ◽  
U Lohbauer ◽  
L Breschi ◽  
A Petschelt ◽  
...  
Keyword(s):  
Bond Strength ◽  
Double Layer ◽  
Artificial Saliva ◽  
In Vitro Study ◽  
Adhesive Systems ◽  
Microtensile Bond Strength ◽  
Application Technique ◽  
One Step ◽  
Self Etch

SUMMARY Purpose The aim of this in vitro study was 1) to analyze the influence of a double-layer application technique of four one-step self-etch adhesive systems on dentin and 2) to determine its effect on the stability of the adhesive interfaces stored under different conditions. Materials and Methods Four different one-step self-etch adhesives were selected for the study (iBondSE, Clearfil S3 Bond, XenoV+, and Scotchbond Universal). Adhesives were applied according to manufacturers' instructions or with a double-layer application technique (without light curing of the first layer). After bonding, resin-dentin specimens were sectioned for microtensile bond strength testing in accordance with the nontrimming technique and divided into 3 subgroups of storage: a) 24 hours (immediate bond strength, T0), b) six months (T6) in artificial saliva at 37°C, or c) five hours in 10 % NaOCl at room temperature. After storage, specimens were stressed to failure. Fracture mode was assessed under a light microscope. Results At T0, iBond SE showed a significant increase in microtensile bond strength when the double-application technique was applied. All adhesive systems showed reduced bond strengths after six months of storage in artificial saliva and after storage in 10% NaOCl for five hours; however at T6, iBond SE, Clearfil S3 Bond, and XenoV+ showed significantly higher microtensile bond strength results for the double-application technique compared with the single-application technique. Scotchbond Universal showed no difference between single- or double-application, irrespective of the storage conditions. Conclusion The results of this study show that improvements in bond strength of one-step self-etch adhesives by using the double-application technique are adhesive dependent.

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