Deposition of Vanadium-Containing Yellow Pigment onto Marshalite Particles through Solution-Combustion Reaction

Author(s):  
N. I. Radishevskaya ◽  
A. Yu. Nazarova ◽  
O. V. Lvov ◽  
N. G. Kasatskii ◽  
R. V. Minin
2009 ◽  
Vol 24 (1) ◽  
pp. 245-252 ◽  
Author(s):  
Robert Ianoş

Single-phase nanocrystalline 4CaO·Al2O3·Fe2O3 powders were prepared directly from the combustion reaction using a new cost-effective, time-saving, and environmentally friendly version of solution combustion synthesis. Instead of a single fuel, a fuel mixture of urea and β-alanine was used. It was shown by x-ray diffraction, energy-dispersive x-ray analysis, thermogravimetric analysis, and optical microscopy that this new version of the solution combustion synthesis allows the maximization of the exothermic effect associated with the combustion reaction. On the other hand, it was shown that the traditional version of combustion synthesis involving the use of a single fuel, such as urea or β-alanine, does not ensure the formation of Ca4Al2Fe2O10 unless subsequent thermal treatments are applied. It was suggested that the occurrence of combustion reactions cannot be regarded only in terms of adiabatic temperature, as the kinetic aspects overrule the thermodynamic ones.


2010 ◽  
Vol 101 (3) ◽  
pp. 631-638 ◽  
Author(s):  
V. Singh ◽  
V. K. Rai ◽  
S. Watanabe ◽  
T. K. Gundu Rao ◽  
I. Ledoux-Rak ◽  
...  

2006 ◽  
Vol 21 (7) ◽  
pp. 1664-1673 ◽  
Author(s):  
Ranjan K. Sahu ◽  
A.K. Ray ◽  
S.K. Das ◽  
A.J. Kailath ◽  
L.C. Pathak

A novel microwave-assisted combustion method was used to prepare Ni powder. The method involves the combustion reaction of nickel nitrate and urea as a fuel in the microwave field. The initiation of the exothermic peak of the combustion reaction was found to vary as a function of urea content. The microwave-prepared Ni powder was characterized using x-ray diffraction (XRD), scanning electron microscopy, atomic force microscopy, Fourier transform infrared spectroscopy, thermogravimetric (TG) analysis, differential thermal analysis (DTA), and magnetic measurement. The XRD pattern revealed that the Ni powder crystallizes with the cubic phase when the molar ratio of fuel to nitrate is varied between 5:1 and 6:1. Above or below that molar ratio, NiO phase coexists as an impurity along with the Ni phase. The magnetization value of Ni measured at room temperature is 53.5 Am2/kg, which is close to the value observed for commercial Ni powder (55.0 Am2/kg). The mechanism for the formation of the Ni and NiO phase is discussed based on the infrared, TG, and DTA data. The method shows that highly pure Ni powder can be prepared using urea as a fuel and microwaves as a source of energy via the solution combustion method.


RSC Advances ◽  
2014 ◽  
Vol 4 (100) ◽  
pp. 56784-56790 ◽  
Author(s):  
G. P. Nagabhushana ◽  
D. Samrat ◽  
G. T. Chandrappa

Nanoparticles of ultra-porous MoO3 were synthesized in a single step by a solution combustion reaction using molybdenum metal powder for the first time as a precursor.


2015 ◽  
Vol 44 (8) ◽  
pp. 2736-2744 ◽  
Author(s):  
Vijay Singh ◽  
S. Watanabe ◽  
T. K. Gundu Rao ◽  
R. Senthil Kumaran ◽  
Hui Gao ◽  
...  

2008 ◽  
Author(s):  
Emilio Moran ◽  
Miguel ïngel. Alario-Franco ◽  
Marco L. Garcia-Guaderrama ◽  
Oscar Blanco

Sign in / Sign up

Export Citation Format

Share Document