An ASM Recommended Practice for Modified Layer Removal Method (MLRM) to Evaluate Residual Stress in Thermal Spray Coatings

Author(s):  
E.F. Rybicki ◽  
J.R. Shadley ◽  
R.T.R. McGrann ◽  
A.C. Savarimuthu ◽  
D. Graving

Abstract Thermal spray coatings are subjected to mechanical loadings in many applications, and there is a need to evaluate the mechanical properties of these coatings. Mechanical properties of interest in the performance of thermal spray coatings include fatigue life, wear resistance, bond strength. Young's modulus, Poisson's ratio, and residual stresses. One property that has a large effect on the performance of thermal spray coated parts is the residual stress distribution in the thermal spray coating and in the substrate. Thus, it is important to have (1) a fundamentally sound method for evaluating residual stresses and (2) a written recommended procedure for applying the method. ASM International is not a standard writing organization. Yet, the increased use of thermal spray coatings and the need for documentation on methods for evaluating mechanical properties of thermal spray coatings have generated a need to prepare Recommended Practices. To meet this need, the ASM International Thermal Spray Society has formed three subcommittees to prepare Recommended Practices for thermal spray coatings. This paper describes a draft form of a Recommended Practice for evaluating residual stresses in thermal spray coatings. This Recommended Practice is being developed by the Subcommittee on "Evaluating of Mechanical Properties of Thermal Spray Coatings". The method, called the Modified Layer Removal Method, has been presented in several papers and has been used for a variety of different coatings. The paper describes the dimensions of the test specimen, the equipment needed, the procedure for removing layers, and the methods for collecting and interpreting the data to evaluate through thickness residual stresses. The Recommended Practice (RP) is in Draft form, but is presented to let the thermal spray community know about the RP effort and invite comments and volunteers to write other RP's.

Author(s):  
S. Tobe ◽  
Y. Andou ◽  
M. Ando ◽  
S. Kuroda ◽  
K. Akita

Abstract Microscopic and macroscopic residual stress measurements and a finite element method (FEM) for stress analysis of thermal spray coatings have been carried out to investigate the residual stress generation mechanism. The residual stresses of one splat, laminated two splats and coatings were measured by a micro-beam x-ray stress measurement system and the macroscopic residual stresses were measured in-situ by the curvature change of the thin substrate plate during and after spraying. Two coating materials were employed in this study to deposit the coatings. One is molybdenum of which the coefficient of thermal expansion (CTE) is smaller than that of steel substrate and the other is 80%Ni-20%Cr alloy which has higher CTE than steel. The substrate was preheated up to 550°C just before spraying. The residual stresses of the splat and a coating are fundamentally the same level. The FEM analysis on the residual stress was also useful and by the comparison of two measurement results of microscopic and macroscopic residual stresses, the generation mechanism was discussed.


1989 ◽  
Vol 153 ◽  
Author(s):  
P.C. Chen ◽  
Yoshiki Oshida

AbstractMulti-layer thin film which has structure of Cu/Cr/K/Cr/Cu prepared by sputtering process was analyzed for interfacial stresses for as-deposited conditions. This structure was also annealed at 150°C, 250°C, and 350°C for around 15 min. in a vacuum and cooled slowly down for stress analyses.Equations derived by Osgood [1] for residual stress estimations for homogeneous material system using layer removal technique (stress relief) is now applied for inhomogeneous system (multilayer structure). The results are compared with the data obtained from x-ray diffraction technique by using sin2Ψ-2θ method, for Cu layer.From the present analyses, the data obatined using layer removal seem to be qualitatively consistent with but not quantitatively in agreement with x-ray method. Data obtained using the layer removal method have some overlaps with those obtained from x-ray technique. However, in details, data from the curvature method present different scattering band from the x-ray method. It is suggested that the layer removal method is more practical to be used to estimate the average residual stress of the multi-layer system not only because the layer removal method estimates the bulk behavior but also when the metal film is thin (e.g., 200A for Cr layer), x-ray technique becomes impractical. By annealing the sputtered structure up to 250°C, the residual stresses, in particularly Cu layer, decreased on both sides in x- and y-directions.From the main results drawn from the present studies, the layer removal sequence for the curvature method shows significant affects on the obtained results of residual stresses. Minimizing influences caused by layer removal sequences as well as removing duration and temperature provides the most accurate results on residual stress measurements.


2011 ◽  
Vol 519 (10) ◽  
pp. 3249-3253 ◽  
Author(s):  
L.M. Jiang ◽  
J. Peng ◽  
Y.G. Liao ◽  
Y.C. Zhou ◽  
J. Liang ◽  
...  

2008 ◽  
Vol 24 (5) ◽  
pp. 374-382 ◽  
Author(s):  
Y. Y. Santana ◽  
La J. G. Barbera-Sosa ◽  
J. Caro ◽  
E. S. Puchi-Cabrera ◽  
M. H. Staia

2018 ◽  
Vol 284 ◽  
pp. 1151-1156
Author(s):  
Lenar N. Shafigullin ◽  
A.R. Ibragimov ◽  
A.I. Saifutdinov

C. C. Berndt advanced investigations of mechanical properties of thermal spray coatings under 4-point bending. He found that this investigation method is sensitive to the mechanical properties of thermal spray coatings.This paper contains the detailed investigation results for thermal spray coatings of zirconium dioxide under 4-point bending, i.e. tests of the specimens subjected to spraying at varying conditions and pre-test soaking with the various duration at 1100 °С.It was established how the mechanical properties of thermal spray coatings changed depending on the spraying mode and high temperature soaking. The test results show that the double heat treatment of coatings is more preferable than one-time heat treatment as it make the properties change linearly. It is more easily controllable during operation of the components with thermal spray coating.


2017 ◽  
Vol 26 (6) ◽  
pp. 1115-1145 ◽  
Author(s):  
Abba A. Abubakar ◽  
Abul Fazal M. Arif ◽  
Khaled S. Al-Athel ◽  
S. Sohail Akhtar ◽  
Javad Mostaghimi

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