Thermal Polycondensation Process and Oil Furnace Production

2021 ◽  
Vol 624 (2) ◽  
pp. 7-11
Author(s):  
N. R. Mikhailets ◽  
◽  
S. A. Sinitsin ◽  
E. A. Danilov ◽  
◽  
...  

The article discusses the methods of obtaining petroleum pitch of thermal polycondensation. The main attention is paid to the characteristics of petroleum pitch, its properties, its comparison with coal-tar pitch, the advantages of petroleum pitch in comparison to coal-tar pitch, the processes of production of petroleum pitch by thermal polycondensation are given. Three promising technologies for the production of petroleum pitch have been identified: thermal polycondensation of cracking residue, high-temperature thermal polycondensation of petroleum feedstock and thermal polycondensation of pyrolysis resin according to a two-stage scheme. Methods of obtaining petroleum pitch in laboratory conditions, such as thermal polycondensation under pressure and heat treatment under reduced pressure, are presented. The urgency and feasibility of developments for the creation of petroleum pitch and the introduction of thermopoly-condensation processes in Russia is emphasized.

Carbon ◽  
2019 ◽  
Vol 153 ◽  
pp. 805
Author(s):  
Ya-wei Dong ◽  
Guo-zheng Xing ◽  
Li-e Jin ◽  
Ping Li ◽  
Qing Cao

Fuel ◽  
2008 ◽  
Vol 87 (6) ◽  
pp. 751-760 ◽  
Author(s):  
K. Mokoena ◽  
T.J. Van der Walt ◽  
T.J. Morgan ◽  
A.A. Herod ◽  
R. Kandiyoti

2021 ◽  
Vol 63 (11) ◽  
pp. 56-59
Author(s):  
The Nam Dao ◽  
◽  
Minh Thanh Vu ◽  
Tuan Anh Doan ◽  
Thi Thao Vu ◽  
...  

Using differential scanning calorimetry and thermogravimetric analysis showed the marking temperature of coal tar pitch is 107.8°C. The thermal decomposition of the pitch is divided into three main stages, corresponding to three phases α, β, γ, with a coke yield of 47% at 800°C. The change in the XRD diagram showed a clear transition from the amorphous state of carbon to the highly ordered crystalline structure of graphite after treatment at 2,200 and 2,700°С. The purity of the pitch sample and the structure of the CCC carbon-carbon composite material after heat treatment at 2,700°C were studied using scanning electron microscopy and energy-dispersive X-ray spectroscopy methods. The results showed that after heat treatment, the C content in the sample reached more than 99.5%, and the coke residues after graphitization were bound and connected to the carbon fabric into a mass of graphite material.


2019 ◽  
Vol 34 (3) ◽  
pp. 258-266 ◽  
Author(s):  
Ya-wei Dong ◽  
Guo-zheng Xing ◽  
Li-e Jin ◽  
Ping Li ◽  
Qing Cao

2021 ◽  
Vol 137 (6) ◽  
pp. 16-19
Author(s):  
N. R. Mikhailets ◽  
◽  
S. A. Sinitsin ◽  
E. A. Danilov ◽  
◽  
...  

The article emphasizes the relevance and expediency of developments for the creation of petroleum pitch and the introduction of thermal polycondensation processes in Russia. The possibility of producing petroleum pitches from vacuum-distilled cracking residue is considered. It is shown that to obtain a petroleum pitch suitable for carbon materials, it is necessary to carry out the process of thermal polycondensation in two stages: at elevated pressure, and then at reduced pressure. The physicochemical properties of the obtained petroleum pitches and intermediate products of the process have been investigated. The possibility of obtaining petroleum pitches with a yield of 35-38% wt. from the vacuum distilled cracking residue at the thermal polycondensation unit.


2008 ◽  
Vol 23 (1) ◽  
pp. 75-80 ◽  
Author(s):  
Yun-wei XUE ◽  
Chang-ling YANG ◽  
Yong-gen LU ◽  
Hai-qin RONG ◽  
Peng WANG ◽  
...  

Sign in / Sign up

Export Citation Format

Share Document