scholarly journals Synthesis of LiNi0.85Co0.14Al0.01O2 Cathode Material and its Performance in an NCA/Graphite Full-Battery

Energies ◽  
2019 ◽  
Vol 12 (10) ◽  
pp. 1886 ◽  
Author(s):  
Cornelius Satria Yudha ◽  
Soraya Ulfa Muzayanha ◽  
Hendri Widiyandari ◽  
Ferry Iskandar ◽  
Wahyudi Sutopo ◽  
...  
Keyword(s):  
Cathode Material ◽  
Solid State Reaction Method ◽  
Electrochemical Performances ◽  
Sem Images ◽  
Voltage Range ◽  
Reaction Method ◽  
Artificial Graphite ◽  
Synthesis Routes ◽  
Xrd Patterns ◽  
Co Precipitation

Nickel-rich cathode material, NCA (85:14:1), is successfully synthesized using two different, simple and economical batch methods, i.e., hydroxide co-precipitation (NCA-CP) and the hydroxides solid state reaction method (NCA-SS), followed by heat treatments. Based on the FTIR spectra, all precursor samples exhibit two functional groups of hydroxide and carbonate. The XRD patterns of NCA-CP and NCA-SS show a hexagonal layered structure (space group: R_3m), with no impurities detected. Based on the SEM images, the micro-sized particles exhibit a sphere-like shape with aggregates. The electrochemical performances of the samples were tested in a 18650-type full-cell battery using artificial graphite as the counter anode at the voltage range of 2.7–4.25 V. All samples have similar characteristics and electrochemical performances that are comparable to the commercial NCA battery, despite going through different synthesis routes. In conclusion, the overall results are considered good and have the potential to be adapted for commercialization.

Synthesis and Electrochemical Properties of 0.5Li2MnO3•0.5LiMn0.5Ni0.5O2

2010 ◽  
Vol 105-106 ◽  
pp. 664-667
Author(s):  
Sheng Wen Zhong ◽  
Wei Hu ◽  
Qian Zhang
Keyword(s):  
Cathode Material ◽  
Electrochemical Properties ◽  
Specific Capacity ◽  
Precipitation Method ◽  
Electrochemical Performances ◽  
Discharge Specific Capacity ◽  
Xrd Patterns ◽  
Co Precipitation ◽  
Two Stages ◽  
Calcined Temperature

The precursor of Mn0.75Ni0.25CO3 is prepared by carbonate co-precipitation method. And the cathode material 0.5Li2MnO3•0.5LiMn0.5Ni0.5O2 is synthesized with two stages calcining temperatures T1 and T2. T1 represents 400°C, 500°C, 600°C and T2 is selected at 750°C, 850°C, 950°C respectively. XRD Patterns shows that the cathode material has the integrated structures of Li2MnO3 and LiMO2, and it has better crystallization during the rise of calcined temperature at 950°C. The electrochemical performances tests indicates that the initial discharge specific capacity are greater than 220mAh/g at the current density 0.2 mA/cm2 in 2.5-4.6V at room temperature. When cathode material is calcined at 750°C, its discharge specific capacity even reach to 248mAh/g, but the cathode material has more perfect general electrochemical properties during calcined temperature at 950°C.

scholarly journals Studies on Highly Dense Pure YIG Polycrystalline Ceramics Fabricated by Tape-casting Method

2020 ◽  
Author(s):  
Chong Zhao ◽  
Yingkui Li ◽  
Xiaofei Shen ◽  
Zhijun Cao ◽  
Zhiquan Cao ◽  
...  
Keyword(s):  
Tape Casting ◽  
Solid State Reaction Method ◽  
Grain Structure ◽  
Casting Method ◽  
Forming Process ◽  
Sem Images ◽  
Polycrystalline Ceramics ◽  
Pure Phase ◽  
One Step ◽  
Xrd Patterns

Abstract Pure phase Y3Fe5O12 (YIG) ceramics was successfully produced by tape-casting forming process and one-step solid-state reaction method. With the sintering temperature above 1100 ºC, the pure phase YIG ceramics was synthesized with no YIP or Fe2O3 phase in XRD patterns. YIG ceramic sintering at 1400 ºC for 10 h showed a clear grain structure with an obvious grain boundary, and no pores were observed in the SEM images. YIG ceramics in this paper has a high relative density which was 99.8% and the saturation magnetization was 28.2 emu/g at room temperature. The hysteresis loss at temperatures of 230-360 K was smaller than 10 mJ/kg. The tan Se was nearly zero at 6~7 GHz and 11~12 GHz, showing that it can be used as a good material for microwave applications. In addition, the low values of tan and tan indicates that it may have a good electromagnetic wave absorption ability.

scholarly journals Synthesis and electrochemical performances of Na3V2(PO4)2F3/C composites as cathode materials for sodium ion batteries

RSC Advances ◽  
2019 ◽  
Vol 9 (53) ◽  
pp. 30628-30636 ◽  
Author(s):  
Mingxue Wang ◽  
Xiaobing Huang ◽  
Haiyan Wang ◽  
Tao Zhou ◽  
Huasheng Xie ◽  
...  
Keyword(s):  
Solid State ◽  
Carbon Source ◽  
Solid State Reaction ◽  
Solid State Reaction Method ◽  
Sodium Ion ◽  
Electrochemical Performances ◽  
Sodium Ion Batteries ◽  
Rate Performance ◽  
Cycle Stability ◽  
Reaction Method

Na3V2(PO4)2F3/C composites were synthesized by a solid-state reaction method using pitch as the carbon source, the as-prepared sample with the carbon content of 12.14% possesses an excellent rate performance and cycle stability.

scholarly journals Synthesis of Na-Doped Lithium Metatitanate and Its Absorption for Carbon Dioxide

2014 ◽  
Vol 2014 ◽  
pp. 1-5 ◽  
Author(s):  
Liu Zhirong ◽  
Zhang Huan ◽  
Wang Yun ◽  
Zhan Xinxing
Keyword(s):  
Carbon Dioxide ◽  
Solid State Reaction Method ◽  
Absorption Capacity ◽  
Absorption Kinetics ◽  
X Ray Diffraction ◽  
Carbon Dioxide Absorption ◽  
Reaction Method ◽  
X Ray ◽  
Xrd Patterns ◽  
The Relationship

Na-doped lithium metatitanate (Na-doped Li2TiO3) absorbent was doped with Na2CO3and lithium metatitanate (Li2TiO3) was prepared by a solid-state reaction method from mixture of TiO2and Li2CO3. The Na-doped lithium metatitanate was characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM) and surface area. Carbon dioxide absorption on Na-doped lithium metatitanate was investigated using TG-DTA. The results reveal an increase of the CO2absorption capacity of the Na-doped materials with respect to pure Li2TiO3. XRD patterns of the doped samples suggest a limited substitution of Li by Na atoms within the Li2TiO3structure. The results of experimental and modeling work were summarized to better understand the relationship between the sorbent microstructure and carbon dioxide absorption kinetics.

Surfactants assisted synthesis of nano-LiFePO4/C composite as cathode materials for lithium-ion batteries

2015 ◽  
Vol 3 (5) ◽  
pp. 2025-2035 ◽  
Author(s):  
Qingyu Li ◽  
Fenghua Zheng ◽  
Youguo Huang ◽  
Xiaohui Zhang ◽  
Qiang Wu ◽  
...  
Keyword(s):  
Solid State ◽  
Lithium Ion Batteries ◽  
Cathode Materials ◽  
Solid State Reaction ◽  
Lithium Ion ◽  
Solid State Reaction Method ◽  
Electrochemical Performances ◽  
Reaction Method

The solid state reaction method was applied to prepare a series of LiFePO4/C materials by adding various surfactants. The as-prepared LiFePO4/C particles using various surfactants show different electrochemical performances.

Synthesis and Luminescent Properties of Eu3+ Doped CaGd4O7 Phosphors by Solvothermal Reaction Method

2015 ◽  
Vol 15 (10) ◽  
pp. 8028-8033 ◽  
Author(s):  
Yeon Woo Seo ◽  
Mi Noh ◽  
Byung Kee Moon ◽  
Jung Hyun Jeong ◽  
Hyun Kyoung Yang ◽  
...  
Keyword(s):  
Broad Band ◽  
Luminescent Properties ◽  
Solvothermal Reaction ◽  
Sem Images ◽  
Reaction Method ◽  
X Ray ◽  
Chromaticity Coordinates ◽  
Potential Applications ◽  
Xrd Patterns ◽  
Cie Chromaticity

Eu3+ doped CaGd4O7 phosphors have been newly synthesized using a solvothermal reaction method and sintered at 1400 °C. The phase, composition, morphologies, and photoluminescent properties of the phosphors have been well characterized by means of the X-ray diffraction (XRD) patterns, energy dispersive X-ray spectroscopy (EDX), field emission scanning electron microscopy (FE-SEM), photoluminescence (PL) spectroscopy, and decay curves, respectively. The XRD patterns of the as-prepared phosphors confirm their monoclinic structure and the FE-SEM images reveal flower-like morphology, formed through agglomeration. The calculated size of the crystallites was approximately 83 nm. The photoluminescence excitation (PLE) spectra of CaGd4O7: Eu3+ phosphors consist of a broad band due to the charge transfer (CT) electronic transition, and several sharp peaks that can be attributed to the f–f transitions of Eu3+ and Gd3+. The PL spectra exhibited a stronger red emission corresponding to the 5D0→7F2 transition. The CIE chromaticity coordinates of the phosphors were calculated and all the chromaticity coordinates have been placed in the red spectral region. These luminescent powders are expected to have potential applications for white light-emitting diodes (WLEDs) and optical display systems.

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