scholarly journals Materials for Solid-Phase Extraction of Organic Compounds

Separations ◽  
2019 ◽  
Vol 6 (4) ◽  
pp. 56 ◽  
Author(s):  
Núria Fontanals ◽  
Rosa M. Marcé ◽  
Francesc Borrull

This review provides an overview of the most recent developments involving materials for solid-phase extraction applied to determine organic contaminants. It mainly concerns polymer-based sorbents that include high-capacity, as well as selective sorbents, inorganic-based sorbents that include those prepared using sol-gel technology along with structured porous materials based on inorganic species, and carbon nanomaterials, such as graphene and carbon nanotubes. Different types of magnetic nanoparticles coated with these materials are also reviewed. Such materials, together with their main morphological and chemical features, are described, as are some representative examples of their application as solid-phase extraction materials to extract organic compounds from different types of samples, including environmental water, biological fluids, and food.

1997 ◽  
Vol 786 (2) ◽  
pp. 259-268 ◽  
Author(s):  
Dianna L. Ambrose ◽  
James S. Fritz ◽  
Michael R. Buchmeiser ◽  
Norbert Atzl ◽  
Günther K. Bonn

2019 ◽  
Vol 15 (7) ◽  
pp. 788-800 ◽  
Author(s):  
Natasa P. Kalogiouri ◽  
Victoria F. Samanidou

Background:The sample preparation is the most crucial step in the analytical method development. Taking this into account, it is easily understood why the domain of sample preparation prior to detection is rapidly developing. Following the modern trends towards the automation, miniaturization, simplification and minimization of organic solvents and sample volumes, green microextraction techniques witness rapid growth in the field of food quality and safety. In a globalized market, it is essential to face the consumers need and develop analytical methods that guarantee the quality of food products and beverages. The strive for the accurate determination of organic hazards in a famous and appreciated alcoholic beverage like wine has necessitated the development of microextraction techniques.Objective:The objective of this review is to summarize all the recent microextraction methodologies, including solid phase extraction (SPE), solid phase microextraction (SPME), liquid-phase microextraction (LPME), dispersive liquid-liquid microextraction (DLLME), stir bar sorptive extraction (SBSE), matrix solid-phase dispersion (MSPD), single-drop microextraction (SDME) and dispersive solid phase extraction (DSPE) that were developed for the determination of hazardous organic compounds (pesticides, mycotoxins, colorants, biogenic amines, off-flavors) in wine. The analytical performance of the techniques is evaluated and their advantages and limitations are discussed.Conclusion:An extensive investigation of these techniques remains vital through the development of novel strategies and the implication of new materials that could upgrade the selectivity for the extraction of target analytes.


2008 ◽  
Vol 19 (6) ◽  
pp. 1136-1143 ◽  
Author(s):  
Eduardo J. Pilau ◽  
Raquel G. C. Silva ◽  
Isabel C. F. S. Jardim ◽  
Fabio Augusto

2019 ◽  
Vol 43 (43) ◽  
pp. 16950-16959 ◽  
Author(s):  
Ali Azadi ◽  
Shahin Ahmadi

In this study, a sensitive, rapid, accurate and practical procedure is established for determination of atorvastatin and valsartan from human biological fluids by dispersive micro solid phase extraction (D-μ-SPE) combined with HPLC-UV detector.


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