scholarly journals MICROSCOPIC DIAGNOSTIC FEATURES OF WHOLE, MILLED AND POWDERED PLANT MATERIAL “RHIZOMES OF COMMON TURMERIC”

2016 ◽  
Vol 1 (1) ◽  
pp. 62-66
Author(s):  
VA A Kurkin ◽  
VM M Ryzhov ◽  
TK K Ryazanova ◽  
LV V Tarasenko ◽  
MYu Yu Borisov ◽  
...  

Aim - the determination of microscopic diagnostic features of rhizomes of common turmeric (Curcuma longa L.), ginger family (Zingiberaceae). Materials and methods. We have studied whole, milled and powdered plant material of turmeric from different manufactures. The study was carried out with the use of the digital microscopes “Motic DM111” (Korea) and “Motic DM-39C-N9GO-A” (Korea). Results. It was determined that the microscopic diagnostic features of rhizomes of turmeric include the presence of cells with sinuous walls and structured content in the form of colored folding in the parenchyma; closed collateral vascular bundles lie scattered in the parenchyma, their conductive elements have narrow lumen. Vascular bundles contain pigment cells considerably smaller in comparison with the size of vessels. Pigment cells with drops of orange-red essential oil are also found in the parenchyma. In milled and powdered plant material, the fragments of all these elements are observed. In the fragments of powdered rhizomes of turmeric, numerous cells with yellow content are found; the parenchyma cells have less expressed folded structure. Fragments of vessels are found both in milled and powdered material. Conclusion. The results of this study were included in the section “Microscopy” of the project of pharmacopoeial monograph “Curcuma longa L. rhizomes”.

2018 ◽  
Vol 8 (4) ◽  
pp. 42-47
Author(s):  
Tien Nguyen Huu ◽  
Tram Le Thi Bao ◽  
Ngoc Nguyen Thi Nhu ◽  
Thang Phan Phuoc ◽  
Khan Nguyen Viet

Background: Curcumin is a major ingredient in turmeric (Curcuma longa L., Zingiberaceae), which has important activities such as anti-tumor, anti-inflammatory, antioxidant, anti-ischemia, protection of gastric mucosa etc,. Curcumin can be considered as a biological marker of turmeric and turmeric products. Objectives: Developing an HPLC method for quantification of curcumin in turmeric powder and turmeric - honey ball pills; applying this method for products on the market. Materials and methods: turmeric powder and turmeric - honey ball pills collected in Thua Thien Hue province. After optimization process, the method was validated and applied to evaluate the content of curcumin. Results: The chromatography analysis was performed with: Zorbaz Eclipse XDB-C18 (150 × 4.6 nm; 5 µm); Mobile phase: acetonitril: 2% acetic acid (45:55), Flow rate was kept constant at 1.0 ml/min; Detector PDA (420 nm). The method was validated for the HPLC system compatibility, specificity, linearity range, precision and accuracy; the recovery greater than 98%. Conclusion: The developed HPLC method can determine curcumin in turmeric powder and turmeric - honey ball pills. Key words: Curcumin, turmeric powder, turmeric-honey ball pills, quantitative determination, HPLC


2019 ◽  
Vol 70 (6) ◽  
pp. 2015-2020
Author(s):  
Silvia Robu ◽  
Aurelia Romila ◽  
Olimpia Dumitriu Buzia ◽  
Adrian Florin Spac ◽  
Camelia Diaconu ◽  
...  

Numerous articles on Salvia officinalis L. have been published regarding the composition of their essential oil. The considerable variation found may be due to the quality of the plant material as well as to the methods used for analysis. A simple GC-MS method was developed and optimized in the QbD approach, for the determination of sage essential oils. The optimization of GC-MS analysis was performed using different mobile phase flows, injection volumes, split ratios and temperature programs. The optimized method proved to be simple and can be successfully applied for the determination of sage essential oils.


Author(s):  
Dayani Pavalakumar ◽  
Madhura Jayasinghe ◽  
Maharsha Edirisinghe ◽  
Isuru Wijesekara ◽  
Subhashinie Senadheera

1945 ◽  
Vol 157 (1) ◽  
pp. 161-167
Author(s):  
Willard L. McRary ◽  
Marion C. Slattery

2012 ◽  
Vol 722 ◽  
pp. 8-20 ◽  
Author(s):  
Víctor Matamoros ◽  
Diana Calderón-Preciado ◽  
Carmen Domínguez ◽  
Josep M. Bayona

2010 ◽  
Vol 46 (2) ◽  
pp. 265-272 ◽  
Author(s):  
Paula Cristina Rezende Enéas ◽  
Renata Barbosa de Oliveira ◽  
Gerson Antônio Pianetti

Oxcarbazepine (OXC) is an important anticonvulsant and mood stabilizing drug. A pharmacopoeial monograph for OXC is not yet available and therefore the development and validation of a new analytical method for quantification of this drug is essential. In the present study, a UV spectrophotometric method for the determination of OXC was developed. The various parameters, such as linearity, precision, accuracy and specificity, were studied according to International Conference on Harmonization Guidelines. Batches of 150 mg OXC capsules were prepared and analyzed using the validated UV method. The formulations were also evaluated for parameters including drug-excipient compatibility, flowability, uniformity of weight, disintegration time, assay, uniformity of content and the amount of drug dissolved during the first hour.


The Analyst ◽  
1953 ◽  
Vol 78 (931) ◽  
pp. 614 ◽  
Author(s):  
W. A. Forster

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