Microstructure and Mechanical Properties of Magnesium Prepared by Spark Plasma Sintering

2010 ◽  
Vol 129-131 ◽  
pp. 764-768 ◽  
Author(s):  
Wan Nur Azrina Wan Muhammad ◽  
Yoshiharu Mutoh ◽  
Yukio Miyashita

Magnesium powders were sintered by using spark plasma sintering (SPS) and conventional pressureless sintering (PLS) techniques at sintering temperatures ranged from 552°C to 605°C to investigate effect of sintering method on microstructure and mechanical properties of sintered magnesium. High densed magnesium could be obtained by using spark plasma sintering technique compared to conventional presureless sintering at the same sintering temperature. It was found that the ultimate tensile strength increased with increasing sintering temperature for both the materials sintered by PLS and SPS. The magnesium samples prepared by SPS showed better mechanical properties than those prepared by PLS. The microstructural observations revealed that the grain growth was not significant in SPS process compared to PLS, which would enhance the mechanical properties of the SPS sintered magnesium.

2018 ◽  
Vol 281 ◽  
pp. 125-130
Author(s):  
Nan Lu ◽  
Jia Xi Liu ◽  
Gang He ◽  
Jiang Tao Li

MgO/Graphene ceramic composites were fabricated by combining combustion synthesis with spark plasma sintering. MgO/Graphene mixture powders were prepared by the combustion reaction between Mg powders and CO2 gas. Dense MgO/Graphene composites were fabricated by spark plasma sintering (SPS) using LiF as the sintering additive. The effect of the sintering temperature on microstructure and mechanical properties of the prepared MgO/Graphene ceramics was discussed. The sintering temperature of the MgO/Graphene mixture powders increased from 900°C to 1300°C. The highest density of 3.43g/cm3 and hardness of 2133MPa were obtained at 1100°C. Compared with monolithic MgO ceramics, the hardness of MgO/Graphene ceramics at the same sintering temperature was increased from 840MPa to 2133MPa.


2007 ◽  
Vol 534-536 ◽  
pp. 833-836 ◽  
Author(s):  
J.K. Lee ◽  
Taek Soo Kim ◽  
Ha Guk Jeong ◽  
Jung Chan Bae

The microstructure and mechanical properties of the Mg97Zn1Y2 alloy prepared by spark plasma sintering of gas atomized powders have been investigated. After consolidation, precipitates were observed to form in the α-Mg solid solution matrix of the Mg97Zn1Y2 alloy. These precipitates consisted of Mg12YZn and Mg24Y5 phases. The density of the consolidated bulk Mg-Zn-Y alloy was 1.86 g/cm3. The ultimate tensile strength and elongation were dependent on the consolidation temperature, which were in the ranges of 280 to 293 MPa and 8.5 to 20.8 %, respectively.


2014 ◽  
Vol 682 ◽  
pp. 188-191 ◽  
Author(s):  
Lilia I. Shevtsova ◽  
T.S. Sameyshcheva ◽  
D.D. Munkueva

The structure and mechanical properties of materials fabricated by spark plasma sintering of mechanically activated mixture of nickel and aluminum nanopowders were investigated. On account of the elemental powders ratio formation of Ni3Al compound was expected. Relative density of sintered samples was equal to ~ 95 %, microhardness of materials was 6540 MPa. Ultimate tensile strength of samples tested according to three-point bending scheme exceed 1100 MPa.


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