Dependence of Microstructures and Mechanical Properties on the Growth Rate and Composition in Directionally Solidified Mg-Gd Alloys

Microstructures and mechanical properties of directionally solidified Mg-xGd (5.21, 7.96 and 9.58 wt.%) alloys were investigated at a wide range of growth rates (V = 10-200 μm/s) under the constant temperature gradient (G = 30 K/mm). The results showed that when the growth rate was 10 μm/s, different interface morphologies were observed in three tested alloys: cellular morphology for Mg-5.21Gd alloy, a mixed morphology of cellular structure and dendritic structure for Mg-7.96Gd alloy and dendrite morphology for Mg-9.58Gd alloy, respectively. Upon further increasing the growth rate, only dendrite morphology was exhibited in all experimental alloys. The microstructural parameters (λ1, λ2) decreased with increasing the growth rate for all the experimental alloy, and the measured λ1 and λ2 values were in good agreement with Trivedi model and Kattamis-Flemings model, respectively. Vickers hardness and the ultimate tensile strength increased with the increase of the growth rate and Gd content, while the elongation decreased gradually. Furthermore, the relationships between the hardness, ultimate tensile strength, the growth rate and the microstructural parameters were discussed and compared with the previous experimental results.

Semisolid Casting and Die Casting of Al-4.8%Mg-2%Si Alloy

An aluminum alloy, Al–4.8%Mg–2%Si, was cast by die casting and thixocasting, and the properties of the cast specimens were investigated. When the poured molten metal temperature was lower than 640 °C during die casting, it was lower than the liquidus temperature, and the metal became a semisolid slurry in the sleeve of the die casting machine; this fulfills the conditions for rheocasting. A tension test was conducted to investigate the effects of semisolid casting on the mechanical properties of Al–4.8%Mg–2%Si. The ultimate tensile strength and elongation of the ingots cast by die casting and rheocasting were affected by the size of ingot. When the ingot had a circular base of 4.5 mm diameter, the ultimate tensile strength and elongation were excellent; however, when the cross section of the ingot was a square with a side length of 20 mm, the tensile strength and elongation were inferior. The thixocasting was conducted using square ingots with a side length of 20 mm, and the tensile strength and elongation were poor in this case as well. The results of this study demonstrate that semisolid casting cannot improve the mechanical properties of Al–4.8%Mg–2%Si ingots with a high thickness. Semisolid casting cannot produce fine-grained Mg2Si, and the mechanical properties of the material could not be improved by this casting method.

Fatigue Performance of Natural and Synthetic Rattan Strips Subjected to Cyclic Tensile Loading

Tensile fatigue performances of selected natural rattan strips (NRSs) and synthetic rattan strips (SRSs) were evaluated by subjecting them to zero-to-maximum constant amplitude cyclic tensile loading. Experimental results indicated that a fatigue life of 25,000 cycles began at the stress level of 50% of rattan material ultimate tensile strength (UTS) value for NRSs evaluated. Rattan core strips’ fatigue life of 100,000 cycles started at the stress level of 30% of its UTS value. Rattan bast strips could start a fatigue life of 100,000 cycles at a stress level below 30% of material UTS value. SRSs didn’t reach the fatigue life of 25,000 cycles until the applied stress level reduced to 40% of material UTS value and reached the fatigue life of 100,000 cycles at the stress level of 40% of material UTS value. It was found that NRSs’ S-N curves (applied nominal stress versus log number of cycles to failure) could be approximated by S=σou(1−H×log10⋅Nf). The constant H values in the equation were 0.10 and 0.08 for bast and core materials, respectively.

Effect of thermal cycling on mechanical and microstructural properties of heat-treated Ti-6Al-4V alloy

Titanium (Ti-6Al-4V) is an α+β phase-field alloy utilized in many industries due to its high strength-to-weight ratio and near-net shaping capability. Solution treated & aging, and stress relief annealing processes were performed on the samples to increase the strength and % of elongation. The heat-treated samples then thermally cycled for 500 cycles, 1000 cycles, and 1500 cycles to evaluate the microhardness and tensile properties. The presence of martensite and α2 precipitates in the thermally cycled samples was confirmed by scanning electron microscopy (SEM) and X-ray diffraction analysis (XRD). In this investigation, at 1000 thermal cycles, all specimens show improvement in both hardness and strength when compared within the cycles. Solution-treated and aging (STA), stress relief annealing (SRA), and without any heat-treatment (WHT) processes have their highest hardness values recorded for 1000 thermal cycles, and the values are 471 HV0.5, 381 HV0.5, and 374.6HV0.5, respectively. For the SRA process, ultimate tensile strength (UTS) of 925 MPa and yield strength (YS) of 896 MPa have resulted in 1000 cycles. Similarly, at 1000 thermal cycle WHT processed samples yielded UTS of 920 MPa and YS of 885 MPa. STA process samples that are heat-treated for 1000 thermal cycles have better strength properties than SRA and WHT and had a UTS of 1530MPa and YS of 1420MPa. From a ductility point of view, a maximum elongation of 29% for the STA process has resulted. Compared to forged titanium alloy (base metal), an increase of 31% elongation and 41% ultimate tensile strength for solution treated and aging process at 1000 cycles has resulted in this investigation.

Process Parameters Optimization for GMA Welding of AISI 1008 Steel Joints for Optimal Tensile Strength

Parameters optimization has become a gateway to achieving quality welds with improved properties desirable for construction and industrial applications. The complex interaction of welding input parameters requires process optimization to achieve optimal responses (s). This study reports the optimization of input parameters for Gas Metal Arc Welding (GMAW) for optimal ultimate tensile strength in AISI 1008 steel joints. Three levels of arc voltage, welding current, and gas flow rate were selected as input parameters, while the targeted output response is the ultimate tensile strength. Taguchi’s method with an L-9 orthogonal matrix was adopted for the process optimization. The MINITAB 17 software was used to analyze the response through analysis of variance and signal-to-noise ratio. The result revealed that the parameter settings for optimal tensile strength for the GMA welding of 6 mm thick AISI 1008 steel joint are arc voltage set at 30 V, current at 180 A, and gas flow rate set at 17 L/mm. The analysis of variance showed that the arc voltage had the most significant influence on the ultimate tensile strength with a 39.76% contribution, followed by the gas flow rate with 31.15%, while the welding current had 6.28% contributions. The surface plots show that a lower-level voltage, higher-level welding current, and higher-level gas flow rate favoured maximum ultimate tensile strength.

Effect of heat treatment on crystallinity and mechanical properties of flexible structures 3D printed with fused deposition modeling

Fused Deposition Modeling (FDM) is a widely used 3D printing technique, which works based on the principle of melted polymer extrusion through nozzle(s) and depositing them on a build plate layer by layer. However, products manufactured with this method lack proper mechanical strength. In this work, 2/1 twill weave fabric structures are 3D printed using poly (lactic) acid (PLA). The ultimate tensile strength in the warp and weft directions and the modulus (stiffnesses) are measured for non-heat-treated (NHT) samples. The printed samples were heat-treated (HT) to improve the strength and stiffness. The variation in ultimate tensile strength is statistically insignificant in warp direction at all temperatures; however, the tensile strength in weft direction decreased after heat treatment. The modulus in warp direction increased by 31% after heat treatment while in the weft direction it decreased after heat treatment. Differential scanning calorimetry (DSC) tests showed the highest crystallinity at 125°C. The properties of the twill fabrics were compared with a standard dog-bone (DB) specimen using uniaxial tensile tests, Differential scanning calorimetry tests, and optical microscope (OM). For dog-bone specimens, the maximum values of crystallinity, ultimate tensile strength, and modulus were found to be at 125°C. The maximum crystallinity percentages are higher than that of the NHT samples. The ultimate tensile strength of NHT DB specimen 3D printed in horizontal orientation improved after heat treatment. The ultimate tensile strength of DB samples in vertical directions increased after heat treatment as well. The stiffness increased in both directions for DB samples.

Investigation of microstructure and mechanical characteristic of underwater friction stir welding for Aluminum 6061 alloy – Silicon carbide (SiC) metal matrix composite

Demand for metal matrix composites (MMCs) is expected to increase in these applications, such as ‎in the aerospace and automotive sectors. Adequate joining techniques, which are important for ‎structural materials, have not yet been developed for Metal Matrix Composite (MMCs), however. ‎This work aimed to demonstrate the feasibility of ‎friction stir welding (FSW) and ‎underwater friction stir welding (UFSW) for joining Al 6061/5, Al 6061/10, and Al ‎‎6061/18 wt. %SiC composites have been produced by utilizing reinforce stir casting technique. Two ‎rotational ‎speeds,1000and 1800 rpm, and traverse speed 10mm \ min were examined. Specimen ‎composite plates 10 mm thick have been successfully welded by FSW. For FSW and UFSW, a tool ‎made of high-speed steel (HSS) with a conical pin shape was used. The result revealed that the ‎ultimate tensile strength of the welded joint by FSW and UFSW at rotation speed 1800 rpm for (Al ‎‎6061/18 wt. ‎‎% SiC composites) was 195 MPa and 230 MPa respectively. The ultimate ‎tensile ‎strength of the welded joint by FSW and UFSW (Al 6061/18 wt.% SiCe composites) was 165 MPa ‎and 180 MPa at rotation speed ‎‎1000 rpm respectively. The microstructural assessment showed that due ‎to larger grain sizes at FSW and UFSW, most of the fractures are located in the thermal ‎mechanically affected zone (TMAZ) adjacent to the weld nugget zone (WNZ). It is observed that in ‎failure, most of the joints show ductile features. As the volume fraction of SiC (18 wt.%) increases, ‎the friction stir welded and underwater friction stir welded efficiency decreases.

Enhanced Strength and Plasticity of CoCrNiAl0.1Si0.1 Medium Entropy Alloy via Deformation Twinning and Microband at Cryogenic Temperature

The synthesis of lightweight yet strong-ductile materials has been an imperative challenge in alloy design. In this study, the CoCrNi-based medium-entropy alloys (MEAs) with added Al and Si were manufactured by vacuum arc melting furnace subsequently followed by cool rolling and anneal process. The mechanical responses of CoCrNiAl0.1Si0.1 MEAs under quasi-static (1 × 10−3 s−1) tensile strength showed that MEAs had an outstanding balance of yield strength, ultimate tensile strength, and elongation. The yield strength, ultimate tensile strength, and elongation were increased from 480 MPa, 900 MPa, and 58% at 298 K to 700 MPa, 1250 MPa, and 72% at 77 K, respectively. Temperature dependencies of the yield strength and strain hardening were investigated to understand the excellent mechanical performance, considering the contribution of lattice distortions, deformation twins, and microbands. Severe lattice distortions were determined to play a predominant role in the temperature-dependent yield stress. The Peierls barrier height increased with decreasing temperature, owing to thermal vibrations causing the effective width of a dislocation core to decrease. Through the thermodynamic formula, the stacking fault energies were calculated to be 14.12 mJ/m2 and 8.32 mJ/m2 at 298 K and 77 K, respectively. In conclusion, the enhanced strength and ductility at cryogenic temperature can be attributed to multiple deformation mechanisms including dislocations, extensive deformation twins, and microbands. The synergistic effect of multiple deformation mechanisms lead to the outstanding mechanical properties of the alloy at room and cryogenic temperature.

The microstructure evolution and mechanical properties improvement of the AZ61 alloy by adding Sc

The improvement of mechanical properties and the microstructure evolution through adding Sc to AZ61magnesium alloy were studied. The results indicated that the Mg17Al12 phase in the extruded AZ61 alloy was mainly distributed around the sub-structured and fine deformed grains, resulting in the nonuniform microstructure. The addition of Sc could effectively suppress the band-like precipitation of Mg17Al12 phase and improve the uniformity of microstructure. The grain sizes of the extruded alloys showed a trend of first decreasing and then increasing with the increase of Sc, which was mainly attributed to the secondary phase. The AZ61-0.5Sc alloy exhibited the best mechanical properties, its ultimate tensile strength and yield strength were 14.8MPa and 40.8MPa higher than those of the extruded AZ61 alloy, respectively, which was ascribed to the fine grains and abundant secondary phase in the alloy.