Influence of the Temperature on GZO Film Deposited by DC Magnetron Reactive Sputtering

2012 ◽  
Vol 446-449 ◽  
pp. 288-292
Author(s):  
Song Yu ◽  
H D Yang ◽  
B Huang ◽  
J S Zhang

GZO transparent conductive thin films were deposited by the direct current magnetron sputtering method from a ZnO target doped with Ga2O3 of 3wt% on glass slide substrates under high pressure of argon. The effect of substrate temperature on the GZO film’s morphology, optical and electrical properties is investigated by using scanning electron microscopy (SEM), UV spectrophotometer, four point probe and Spectroscopic Ellipsometer. The results showed that GZO thin films with high quality could be fabricated under the high pressure of argon.When substrate temperature is 250°C or below, surface morphology of thin films can be significantly improved.With the increase of substrate temperature, the crystal grain become larger, the crystal boundaries narrow and become clear, and reach a best case at 250°C. At the same time, the resistivity of GZO thin films decrease and reach the minimum which is 1.099×10-3 Ω•cm at 300°C while the average transmittance increase to 90%. Consequently, the properties of morphology began to get worse with the increase of temperature above 300°C.

2012 ◽  
Vol 602-604 ◽  
pp. 1503-1507
Author(s):  
Xia Wu ◽  
Hui Dong Yang ◽  
Ji Sen Zhang ◽  
Long Gu

The films were deposited on glass slide substrates by DC magnetron sputtering method by using a ZnO target doped with Ga2O3 of 3wt%, then annealing processing were implemented respectively under the temperature of 250 °C with the time of 0,30,60,90 and 120 minutes.Effects of sputtering on the structural and optical and electrical properties of GZO films had been investigated. The results showed that GZO films with high quality could be fabricated after vacuum-annealed. crystal face of GZO films had a good tendency of c axis. the (002) diffraction peak reached a maximum at the annealing time of 1.5 hours; at the same time ,crystal grain became larger and crystal boundaries narrow, film’s resident stress reduced to 0.5 Mpa.With the annealing time increasing, the resistivity of GZO films decreased and reached the minimum which was 9.1×10-4 Ω·cm at 1.5 hours. While the average transmittance decreased sharply after the time of 1.5 hours in visible region. Consequently, the best annealing time is 1.5 hours.


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