Textures and Local Textures in Severely Cold-Rolled and Annealed Ultra-Fine-Grained FeCo Alloy

2005 ◽  
Vol 495-497 ◽  
pp. 731-736 ◽  
Author(s):  
J.N. Deng ◽  
Emmanuel Bouzy ◽  
Jean-Jacques Fundenberger ◽  
Ru Lin Peng ◽  
Chang Shu He ◽  
...  

We find that a severely rolled FeCo alloy has anomalous enhancement of the rotated-cube {100}<011> texture component and a decrease of the {111} components after annealing, which is contrast to the recrystallization behaviors reported in traditional BCC metals and alloys. The local texture measurements show that two kinds of grains with obviously different orientations, i.e. {100} and {111}, are heterogeneously distributed in the deformed specimen and the migration of high-angle grain boundaries is observed after annealing in the disordering temperature region.

2009 ◽  
Vol 618-619 ◽  
pp. 551-554 ◽  
Author(s):  
O. Al-Buhamad ◽  
M. Zakaria Quadir ◽  
Michael Ferry

A multilayered sheet composite of commercial purity Al and Al-0.3%Sc alloys was produced by accumulative roll bonding. The final sheet material consisted of 64 ultra fine grained layers, each of ~7.8mm in thickness. The as-deformed material was annealed at temperatures ranging from 250 to 350°C to study the changes in microstructure and their associated influence on mechanical properties. The as-deformed structures largely comprised of high angle grain boundaries in the Al layers and low angle grain boundaries in the Al(Sc) layers. During annealing, the structures in the Al(Sc) layers remained unaltered, whereas the Al layers recrystallized rapidly to the full layer thickness. The mechanical properties of the Al-Al(Sc) composite were measured and found to be unique in strength and ductility with annealing temperature having a significant influence on these properties.


2016 ◽  
Vol 873 ◽  
pp. 43-46
Author(s):  
Tao Xiong ◽  
Gang Zhao ◽  
Jian Wen Gao

Research object of this article is a type of oriented silicon steel in 3.07% silicon content. By comparing samples under normalization and non-normalization respectively after primary recrystallizing annealing and secondary recrystallizing annealing, we have figured out how normalization influenced the recrystallizing behavior. The EBSD data of samples showed that normalization can half the grain size after primary recrystallizing, raise the percentage content of favored grain boundaries and high-angle grain boundaries, increase the content of Goss orientation grains by 5 times. And normalization coarsens the secondary recrystallizing grains, triples the magnetic induction and reduces the iron loss by half.


2002 ◽  
Vol 396-402 ◽  
pp. 1061-1066 ◽  
Author(s):  
Takeshi Fujita ◽  
Z. Horita ◽  
Terence G. Langdon

Author(s):  
Eswarahalli Venkatesh ◽  
L.E. Murr

In recent years, many researchers have shown great interest in understanding the structure of grain boundaries and their influence on the mechanical properties in metals and alloys. In recent years, the structure of grain boundaries and their control have been considered as a means of understanding the strengthening mechanisms in metals and alloys. There are many ways by which the grain boundary structure can be changed both in pure metals and alloys. One such means considered here is the thermomechanical treatment of pure metals.In the present work, high purity (99.9999%) aluminum sheet, mill rolled to 0.004 in. thick, is used. The as-received condition of the sample was flash-annealed at 903°K in an argon atmosphere. Batch specimens from this stock were cold rolled to 50% reduction in thickness and annealed in air at 903°K followed by either furnace cooling or air cooling to room temperature.


Author(s):  
J.N. Deng ◽  
Emmanuel Bouzy ◽  
Jean-Jacques Fundenberger ◽  
Ru Lin Peng ◽  
Chang Shu He ◽  
...  
Keyword(s):  

Author(s):  
J. W. Matthews ◽  
W. M. Stobbs

Many high-angle grain boundaries in cubic crystals are thought to be either coincidence boundaries (1) or coincidence boundaries to which grain boundary dislocations have been added (1,2). Calculations of the arrangement of atoms inside coincidence boundaries suggest that the coincidence lattice will usually not be continuous across a coincidence boundary (3). There will usually be a rigid displacement of the lattice on one side of the boundary relative to that on the other. This displacement gives rise to a stacking fault in the coincidence lattice.Recently, Pond (4) and Smith (5) have measured the lattice displacement at coincidence boundaries in aluminum. We have developed (6) an alternative to the measuring technique used by them, and have used it to find two of the three components of the displacement at {112} lateral twin boundaries in gold. This paper describes our method and presents a brief account of the results we have obtained.


Author(s):  
C. W. Price

Little evidence exists on the interaction of individual dislocations with recrystallized grain boundaries, primarily because of the severely overlapping contrast of the high dislocation density usually present during recrystallization. Interesting evidence of such interaction, Fig. 1, was discovered during examination of some old work on the hot deformation of Al-4.64 Cu. The specimen was deformed in a programmable thermomechanical instrument at 527 C and a strain rate of 25 cm/cm/s to a strain of 0.7. Static recrystallization occurred during a post anneal of 23 s also at 527 C. The figure shows evidence of dissociation of a subboundary at an intersection with a recrystallized high-angle grain boundary. At least one set of dislocations appears to be out of contrast in Fig. 1, and a grainboundary precipitate also is visible. Unfortunately, only subgrain sizes were of interest at the time the micrograph was recorded, and no attempt was made to analyze the dislocation structure.


Author(s):  
D.R. Rasmussen ◽  
N.-H. Cho ◽  
C.B. Carter

Domains in GaAs can exist which are related to one another by the inversion symmetry, i.e., the sites of gallium and arsenic in one domain are interchanged in the other domain. The boundary between these two different domains is known as an antiphase boundary [1], In the terminology used to describe grain boundaries, the grains on either side of this boundary can be regarded as being Σ=1-related. For the {110} interface plane, in particular, there are equal numbers of GaGa and As-As anti-site bonds across the interface. The equilibrium distance between two atoms of the same kind crossing the boundary is expected to be different from the length of normal GaAs bonds in the bulk. Therefore, the relative position of each grain on either side of an APB may be translated such that the boundary can have a lower energy situation. This translation does not affect the perfect Σ=1 coincidence site relationship. Such a lattice translation is expected for all high-angle grain boundaries as a way of relaxation of the boundary structure.


Author(s):  
H. Lin ◽  
D. P. Pope

During a study of mechanical properties of recrystallized B-free Ni3Al single crystals, regularly spaced parallel traces within individual grains were discovered on the surfaces of thin recrystallized sheets, see Fig. 1. They appeared to be slip traces, but since we could not find similar observations in the literature, a series of experiments was performed to identify them. We will refer to them “traces”, because they contain some, if not all, of the properties of slip traces. A variety of techniques, including the Electron Backscattering Pattern (EBSP) method, was used to ascertain the composition, geometry, and crystallography of these traces. The effect of sample thickness on their formation was also investigated.In summary, these traces on the surface of recrystallized Ni3Al have the following properties:1.The chemistry and crystallographic orientation of the traces are the same as the bulk. No oxides or other second phases were observed.2.The traces are not grooves caused by thermal etching at previous locations of grain boundaries.3.The traces form after recrystallization (because the starting Ni3Al is a single crystal).4.For thicknesses between 50 μm and 720 μm, the density of the traces increases as the sample thickness decreases. Only one set of “protrusion-like” traces is visible in a given grain on the thicker samples, but multiple sets of “cliff-like” traces are visible on the thinner ones (See Fig. 1 and Fig. 2).5.They are linear and parallel to the traces of {111} planes on the surface, see Fig. 3.6.Some of the traces terminate within the interior of the grains, and the rest of them either terminate at or are continuous across grain boundaries. The portion of latter increases with decreasing thickness.7.The grain size decreases with decreasing thickness, the decrease is more pronounced when the grain size is comparable with the thickness, Fig. 4.8.Traces also formed during the recrystallization of cold-rolled polycrystalline Cu thin sheets, Fig. 5.


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