Strain Scan and Texture of an Anhydrite-Dolomite Rock from the Piora-Syncline (Switzerland)

2006 ◽  
Vol 524-525 ◽  
pp. 633-638
Author(s):  
Christian Scheffzük ◽  
Kurt Walther ◽  
Alexander Frischbutter ◽  
Rudolf Naumann

An anhydrite-dolomite rock was investigated in order to find correlations between intracrystalline strain and texture. The sample represents a composite rock, called Zuckerdolomit, occurring for instance in the central Alps. Zuckerdolomit may occasionally respond to mechanical impulses with a complete break down of its structure. Residual strain was scanned at the strain/stress diffractometer EPSILON-MDS and the crystallographic texture was obtained by neutron time-of-flight diffraction at the texture diffractometer SKAT at the pulsed neutron source IBR-2 in Dubna, Russia. Texture was additionally determined by the U-stage microscopy. The texture of the rock could be derived from the main constituents: anhydrite and dolomite. The anhydrite texture appears to be characterised by an orthorhombic symmetry. One plane of the symmetry trends parallel to the rock’s foliation plane, with basal planes subparallel to and a small circle distribution within the foliation plane. There is a subordinated small circle orientation pattern relating in 45° to the rock’s foliation plane. On the other hand, the subordinated regulation pattern of anhydrite is fixed to the orientation of the foliation plane. The determined residual strain data for anhydrite and dolomite reflect a generally opposed directed state, regarding both, compression and dilatation. Moreover, taking into account the elastic constants for both minerals, which differ approximately by the factor two, the special geomechanical behaviour of the studied Zuckerdolomit appears to be considerably determined by interactions between its residual strain and textural properties. This may be of particular importance for underground activities (mining, tunnelling etc.). The dangerous geomechanical behaviour of the rock seems to be determined by its residual straintexture relations more than so far believed (anhydrite hydration).

2006 ◽  
Vol 524-525 ◽  
pp. 781-786
Author(s):  
Christian Scheffzük ◽  
Petra Kluge-Weiss ◽  
Felix Greuter

Strain/stress experiments for characterization of micro- and macro-strain distribution and texture experiments were carried out on a varistor ceramic using neutron-TOF-diffraction. By a radial strain scan, residual strain has been determined on the (1010 ), (0002), (1012), and (1120 ) Bragg reflections of the hexagonal ZnO as well as on the (400) reflections of the cubic spinel Zn7Sb2O12. Residual strain values in the range of -1.5x10-4 (contraction) and 4x10-4 (dilatation) were observed for ZnO, with indications of macro-strains across the cylindrical sample and substantial micro-strains between the different phases. The texture on both phases (ZnO, Zn7Sb2O12) is characterized by a weak, non-ideal fibre texture around the cylinder axis. The results indicate that the texture pattern might coincide with the strain. To our knowledge, these are the first texture and residual strain investigations in metal oxide varistor elements and they will be discussed in detail.


2005 ◽  
Vol 369 (1-4) ◽  
pp. 1-7 ◽  
Author(s):  
Myung-Kook Moon ◽  
Chang-Hee Lee ◽  
Vyacheslav T. Em ◽  
Pavol Mikula ◽  
Kwang-Pyo Hong ◽  
...  

2012 ◽  
Vol 152-154 ◽  
pp. 1406-1412
Author(s):  
Yan Li Song ◽  
Lin Hua

In this paper, the rule of mixture, which is often used to derive the weld properties from the uniaxial tension test of a subsize welded specimen, was improved by taking the residual welding strain/stress into account and assuming iso-strain increment across the welded specimen. Based on this improved method, hardening data of two different tailor welded blanks were determined. Erichsen cupping tests were performed experimentally and numerically to evaluate the effects of welding residual strain and stress on TWB formability. The results indicate that: (1) the residual strain and stress affect the formality of TWBs to some extent and (2) neglecting the welding residual strain and stress may predict a delayed crack onset and relatively large values in the maximum punch load and Erichsen index.


2006 ◽  
Vol 321-323 ◽  
pp. 1663-1666 ◽  
Author(s):  
Yoshiaki Kiyanagi ◽  
Takashi Kamiyama ◽  
Toshiyuki Nagata ◽  
F. Hiraga

Neutron imaging using a pulsed neutron time-of-flight method can give an energy dependent transmission image, namely, spectroscopic image. This image includes the structure information if the sample is coherent scatterer. Here, two examples are introduced. First, we obtained the transmission image of a welded sample of SS304 and 308. Change of the crystal structure depending on the position was observed. Furthermore, we measured spatial dependent transmission of SS samples treated in different ways, surface treatment and whole body treatment. There were almost no spatial dependent change, but the cross section change was found between surface and whole body treatment samples. It was suggested that this might be due to the difference of a grain size. These results demonstrated that the spectroscopic imaging using a pulsed neutron source is a useful tool for material characterization.


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