Synthesis and Luminescent Properties of Porous YVO4:Sm Nanoplates

2009 ◽  
Vol 620-622 ◽  
pp. 541-544 ◽  
Author(s):  
Ju An Wang ◽  
Yun Hua Xu ◽  
Qihong Cen ◽  
Xiao Man Zhang ◽  
Ya Ru Cui
Keyword(s):  
Low Temperature ◽  
Ethylene Glycol ◽  
Luminescence Intensity ◽  
Annealing Temperature ◽  
Luminescent Properties ◽  
Precipitation Method ◽  
Low Temperature Synthesis ◽  
Temperature Synthesis ◽  
Preparation Methods ◽  
Co Precipitation

The present research describes a simple low-temperature synthesis route of fabricating porous YVO4:Sm nanoplates via a chemical co-precipitation method using commercially available Y2O3, NH4VO3, Sm2O3 and ethylene glycol as the reacting precursors. The as-synthesized YVO4:Sm was thermally treated at 300°C and 600°C for 2 h which is much lower than that of the conventional preparation methods. The obtained samples were characterized by FTIR, XRD, TEM and PL. The photoluminescence measurement revealed that the luminescence intensity was significantly increased with increasing annealing temperature.

Modified Synthesis Temperature of Ba3 Co1.7 Ni0.1 Cu0.1 Mn0.1 Fe24 O41 Z-Type Ferrite Nanoparticles Prepared by Co-Precipitation Method

2013 ◽  
Vol 829 ◽  
pp. 737-741 ◽  
Author(s):  
Mohammad Javad Pourhosseini Asl ◽  
Ali Ghasemi ◽  
Gholam Reza Gordani
Keyword(s):  
Low Temperature ◽  
Synthesis Temperature ◽  
Precipitation Method ◽  
Diffraction Field ◽  
X Ray Diffraction ◽  
Low Temperature Synthesis ◽  
Temperature Synthesis ◽  
Optimum Synthesis ◽  
Different Temperatures ◽  
Co Precipitation

In this study, the low temperature synthesis of barium-Z type hexaferrite nanoparticles was considered. In this manner, the Z-type hexaferrite with the chemical composition of Ba3 Co1.7 Ni0.1 Cu0.1 Mn0.1 Fe24 O41 was synthesized at different temperatures of 900, 1000 and 1100 0C for 3hr. An X-Ray diffraction, field emission scanning electron microscopy (FE-SEM) and a vibrating sample magnetometer (VSM) analysis were carried out to investigate structural and magnetic properties of samples. XRD results showed that the Z-type ferrite phase was formed in all samples. However, At the low temperature synthesis (T=900 0C), the Ba2Me2Fe12O22 and BaFe2O4 phases were also detected. FE-SEM micrographs showed that with increasing the synthesis temperature, the particle size was increased. It was found that the saturation of magnetization was slightly increased from 54 to 55. 5emugr with an increase in synthesis temperature from 900 to 11000C, while the coercivity increased initially from 670 Oe to 860 Oe and then decreased to 488 Oe. The results also indicated that the temperature of 10000C was the optimum synthesis temperature of Ba-Z type hexaferrite nanoparticles, which was much lower than that of Z-type hexaferrite produced by previous researchers.

scholarly journals LOW-TEMPERATURE SYNTHESIS OF SUPERPARAMAGNETIC Zn0.8Ni0.2Fe2O4 FERRITE NANOPARTICLES

2018 ◽  
Vol 56 (1) ◽  
pp. 31
Author(s):  
Luong Thi Quynh Anh ◽  
Nguyen Van Dan ◽  
Do Minh Nghiep
Keyword(s):  
Particle Size ◽  
Magnetic Properties ◽  
Oleic Acid ◽  
Low Temperature ◽  
Coercive Force ◽  
Saturation Magnetization ◽  
Ferrite Nanoparticles ◽  
Low Temperature Synthesis ◽  
Temperature Synthesis ◽  
Co Precipitation

The crystalline nanoparticles of Ni0.2Zn0.8Fe2O4 ferrite were synthesized by chemical co-precipitation with precursor concentration of 0.1M, then modified by 0.25M solution of oleic acid in pentanol, finally heated at temperatures 120, 140, 160 and 180oC for 6h in autoclave. The XRD, EDS and TEM confirmed that all of samples are crystalline and their particle size are 6, 6.5, 7 and 8 nm. The magnetic properties showed that the coercive force, the remanence of samples are about zero, the saturation magnetization Ms has values from 14.20 to 27.12 emu/g.

scholarly journals Ethylene glycol assisted low-temperature synthesis of boron carbide powder from borate citrate precursors

2014 ◽  
Vol 2 (3) ◽  
pp. 268-274 ◽  
Author(s):  
Rafi-ud-din ◽  
G.H. Zahid ◽  
Z. Asghar ◽  
Muhammad Maqbool ◽  
Ejaz Ahmad ◽  
...  
Keyword(s):  
Low Temperature ◽  
Ethylene Glycol ◽  
Boron Carbide ◽  
Carbide Powder ◽  
Low Temperature Synthesis ◽  
Temperature Synthesis ◽  
Citrate Precursors

Low Temperature Synthesis and Luminescent Properties of Ca2SnO4: Eu3

2010 ◽  
Vol 136 ◽  
pp. 14-17 ◽  
Author(s):  
Yu Zhong Li ◽  
Xiao Chun Zhou
Keyword(s):  
Low Temperature ◽  
Spherical Shape ◽  
Luminescent Properties ◽  
Xrd Analysis ◽  
Electric Dipole Transition ◽  
Low Temperature Synthesis ◽  
Temperature Synthesis ◽  
X Ray ◽  
Emission Transition ◽  
Red Emitting Phosphor

A novel red emitting phosphor, Ca2SnO4: Eu3+, was prepared by the low temperature solid state reaction. X-ray powder diffraction (XRD) analysis confirmed the formation of Ca2SnO4: Eu3+. Scanning electron-microscopy (SEM) observation indicated a narrow size distribution of about 500 nm for the particles with spherical shape. Under 396 nm excitation, the Ca2SnO4: Eu3+ phosphor exhibits novel red emission at about 613 nm which is assigned to the 5D0→7F2 electric-dipole transition. Furthermore, the emission transition 5D0→7F2 has been found to be more prominent over the normal orange emission transition 5D0→7F1.

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