Elastoplastic Deformation and Damage Process in Duplex Steel Studied Using Synchrotron and Neutron Diffraction

2017 ◽  
Vol 905 ◽  
pp. 9-16
Author(s):  
Yu Chen Zhao ◽  
Léa Le Joncour ◽  
Andrzej Baczmański ◽  
Manuel François ◽  
Sebastian Wroński ◽  
...  
Keyword(s):  
Neutron Diffraction ◽  
Synchrotron Diffraction ◽  
X Ray ◽  
Slip Mechanism ◽  
Lattice Strains ◽  
Duplex Steel ◽  
Consistent Model ◽  
Damage Process ◽  
Crystallographic Planes

In the present work, the mechanical behavior of phases in duplex steel during tensile test was studied. Special interest was taken in the analysis of damage process just before failure. In this aim two diffraction methods: in-situ time of flight neutron diffraction and X-ray synchrotron diffraction were applied. Using diffraction data, the slip mechanism on crystallographic planes during plastic deformation was investigated. In the case of aged UR45N steel, it was found that significant softening caused by damage process was initiated in the ferritic phase. The lattice strains measured in situ by two above mentioned diffraction methods were compared with prediction of the self-consistent model.

Localization of Stresses in Polycrystalline Grains Measured by Neutron Diffraction and Predicted by Self-Consistent Model

2011 ◽  
Vol 681 ◽  
pp. 103-108
Author(s):  
Anita Gaj ◽  
Lea le Joncour ◽  
Andrzej Baczmanski ◽  
Sebastian Wroński ◽  
Benoit Panicaud ◽  
...  
Keyword(s):  
Neutron Diffraction ◽  
Load Transfer ◽  
Diffraction Method ◽  
Lattice Strains ◽  
Consistent Model ◽  
Self Consistent ◽  
Main Component ◽  
Critical Resolved Shear Stress ◽  
Elastic Lattice

Time of flight neutron diffraction method was applied to measure elastic lattice strains in austenitic steel during "in situ" tensile test. Comparing experimental data with self-consistent model, the critical resolved shear stress and hardening parameters were determined for polycrystalline grains. The result allowed us to determine the main component of the stress localization tensor, relating the rate of grain stress with the applied macrostress rate. The evolution of concentration tensor in function of the applied macrostress was analyzed. Finally, the load transfer between grains during yielding of the sample was studied.

On the Development of Grain-Orientation-Dependent and Inter-Phase Stresses in a Super Duplex Stainless Steel under Uniaxial Loading

2006 ◽  
Vol 524-525 ◽  
pp. 917-922 ◽  
Author(s):  
Ru Lin Peng ◽  
Yan Dong Wang ◽  
Guo Cai Chai ◽  
Nan Jia ◽  
Sten Johansson ◽  
...  
Keyword(s):  
Plastic Deformation ◽  
Stainless Steel ◽  
Neutron Diffraction ◽  
Grain Orientation ◽  
Super Duplex Stainless Steel ◽  
Lattice Strains ◽  
Duplex Steel ◽  
In Situ Neutron Diffraction ◽  
Phase Stresses

Microstresses due to intergranular and inter-phase interactions in an austenitic-ferritic super duplex steel (SAF 2507) under uniaxial compressive deformation have been studied by in-situ neutron diffraction experiments. Lattice strains of several hkl planes of austenite respective ferrite were mapped as a function of sample direction at a number of load levels during loading into the plastic regime and unloading. The analysis of the experimental results has shown that during loading both grain-orientation-dependent and inter-phase stresses were generated under plastic deformation that was inhomogeneous at the microstructural level. Residual stresses depending on the grain-orientation and phase have been found after unloading. The results also indicate stronger intergranular interactions among the studied hkl planes of austenite than those of ferrite.

scholarly journals Determination of Residual Stresses in an Oxidized Metallic Alloy under Thermal Loadings

Metals ◽  
2018 ◽  
Vol 8 (11) ◽  
pp. 913
Author(s):  
Zhimao Wang ◽  
Jean-Luc Grosseau-Poussard ◽  
Benoît Panicaud ◽  
Guillaume Geandier ◽  
Pierre-Olivier Renault ◽  
...  
Keyword(s):  
Residual Stresses ◽  
Correction Method ◽  
Lattice Parameter ◽  
European Synchrotron Radiation Facility ◽  
X Ray Diffraction ◽  
Synchrotron Diffraction ◽  
X Ray ◽  
Crystallographic Planes

In order to clarify the mechanical features of a metal under thermal cyclic loading for the system Ni30Cr-Cr2O3, a specific study has been carried out. In the present work, the residual stresses in both the metal and the oxide layer have been investigated. An adapted method is applied to process the experimental results that were obtained by using in-situ high temperature synchrotron diffraction at European Synchrotron Radiation Facility. The sin2ψ analysis provides information about the stress in metal and oxide. X-ray diffraction provides also the lattice parameter between crystallographic planes in the metal. To obtain correct stress values, a correction method is also proposed taking into account different discrepancies sources to ensure the equation of mechanical balance.

Study of Stresses in Texture Components Using Neutron Diffraction

2013 ◽  
Vol 768-769 ◽  
pp. 289-295
Author(s):  
Andrzej Baczmański ◽  
Elżbieta Gadalińska ◽  
Sebastian Wroński ◽  
Léa Le Joncour ◽  
Benoit Panicaud ◽  
...  
Keyword(s):  
Experimental Data ◽  
Neutron Diffraction ◽  
Tensile Load ◽  
Group Method ◽  
Model Calculations ◽  
Lattice Strains ◽  
Consistent Model ◽  
Self Consistent ◽  
Full Stress Tensor

In this work a new method for analysis of neutron diffraction results obtained during “in situ” tensile load is proposed and tested. The methodology is based on the measurements of lattice strains during “in situ” tensile test for several hkl reflections and for different orientations of the sample with respect to the scattering vector. As the result the full stress tensor for preferred texture orientations in function of applied stress can be determined with help of crystallite group method. The experimental data are presented and compared with self-consistent model calculations performed for groups of grains corresponding to the measured hkl reflections.

scholarly journals Following Microstructures during Deformation: In situ X-ray/Neutron Diffraction and HRDIC

2019 ◽  
Vol 580 ◽  
pp. 012010
Author(s):  
E Polatidis ◽  
K Sofinowski ◽  
W-N Hsu ◽  
H Van Swygenhoven
Keyword(s):  
Neutron Diffraction ◽  
X Ray

scholarly journals The migration mechanism of transition metal ions in LiNi0.5Mn1.5O4

2015 ◽  
Vol 3 (24) ◽  
pp. 13031-13038 ◽  
Author(s):  
Gui-Liang Xu ◽  
Yan Qin ◽  
Yang Ren ◽  
Lu Cai ◽  
Ke An ◽  
...  
Keyword(s):  
Transition Metal ◽  
Neutron Diffraction ◽  
Metal Ions ◽  
Transition Metal Ions ◽  
High Energy ◽  
X Ray Diffraction ◽  
X Ray ◽  
Migration Mechanism

In situ high-energy X-ray diffraction and neutron diffraction were deployed to trace the migration of transition metal ions in LiNi0.5Mn1.5O4.

Lattice Strain Pole Figures Analysis in Titanium during Uniaxial Deformation

2017 ◽  
Vol 905 ◽  
pp. 74-80
Author(s):  
David Gloaguen ◽  
Baptiste Girault ◽  
Jamal Fajoui ◽  
Vincent Klosek ◽  
Marie José Moya
Keyword(s):  
Experimental Data ◽  
Neutron Diffraction ◽  
Lattice Strain ◽  
Pure Titanium ◽  
Tensile Load ◽  
Uniaxial Tensile ◽  
Lattice Strains ◽  
Pole Figures ◽  
In Situ Neutron Diffraction

A theoretical and experimental study was carry out to investigate deformation mechanisms in a textured titanium alloy. In situ neutron diffraction measurements were performed to analyze different {hk.l} family planes ({10.0}, {10.1}, {11.0} and {00.2}) and determine the corresponding internal strain pole figures. This method was applied to a pure titanium (a-Ti) submitted to a uniaxial tensile load up to 2 %. The experimental data was then used to validate the EPSC model in order to predict the distribution of lattice strains determined by neutron diffraction for various diffraction vector directions. This comparison reveals that the model results were in good agreement with the experimental data and the simulations reproduced the lattice strain development observed on the strain pole figures determined by neutron diffraction.

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