Fracture Resistance of AAAS Composites with Ceramic Precursor

2021 ◽  
Vol 322 ◽  
pp. 54-59
Author(s):  
Iva Rozsypalová ◽  
Petr Daněk ◽  
Pavla Rovnaníková ◽  
Zbyněk Keršner

The paper deals with selected alkali-activated aluminosilicate (AAAS) composites based on ceramic precursors in terms of their characterization by mechanical fracture parameters. Composites made of brick dust as a precursor and an alkaline activator with a silicate modulus of Ms = 0.8, 1.0, 1.2, 1.4 and 1.6 were investigated. The filler employed with one set of composites was quartz sand, while for the other set it was crushed brick. The test specimens had nominal dimensions of 40 × 40 × 160 mm and were provided with notches at midspan of up to 1/3 of the height of the specimens after 28 days. 6 samples from each composite were tested. The specimens were subjected to three-point bending tests in which force vs. displacement (deflection at midspan) diagrams (F–d diagrams) and force vs. crack mouth opening (F–CMOD) diagrams were recorded. After the correction of these diagrams, static modulus of elasticity, effective fracture toughness, effective toughness and specific fracture energy values were determined using the Effective Crack Model and the Work-of-Fracture method. After the fracture experiments, informative compressive strength values were determined from one of the parts. All of the evaluations included the determination of arithmetic means and standard deviations. The silicate modulus values and type of filler of the AAAS composites significantly influenced their mechanical fracture parameters.

2021 ◽  
Vol 322 ◽  
pp. 66-71
Author(s):  
Martin Lipowczan ◽  
David Lehký ◽  
Iva Rozsypalová ◽  
Petr Daněk ◽  
Pavla Rovnaníková ◽  
...  

The paper deals with selected alkali-activated aluminosilicate (AAAS) composites based on ceramic precursors in terms of characterization by mechanical fracture parameters. Two composites made of brick dust as a precursor and an alkaline activator with a silicate modulus Ms = 1.0 were investigated. The composites differed in the fineness of grinding of the precursor – in the first set it was 0 to 1 mm, in the second set 0 to 0.3 mm. The filler was crushed brick. The test specimens had nominal dimensions of 40 × 40 × 160 mm and were provided with notches in the middle of the span up to 1/3 of the depth of the specimens after 28 days of hardening. Five to six specimens from each composite set were tested. The specimens were subjected to three-point bending tests, in which force vs. displacement (deflection in the middle of the span) diagrams (F–d diagrams) and force vs. crack mouth opening displacement (F–CMOD) diagrams were recorded. After correction of these diagrams, the values of static modulus of elasticity, effective fracture toughness, effective toughness and specific fracture energy were determined using the Effective Crack Model and the Work-of-Fracture method. After the fracture experiments, the values of informative compressive strength were determined on one of the fractured parts. At the same time, the values of static modulus of elasticity, tensile strength and specific fracture energy were identified using artificial neural networks and F–d diagrams measured and simulated in the ATENA FEM software. All evaluations included the determination of basic statistics of parameters.


2018 ◽  
Vol 272 ◽  
pp. 220-225 ◽  
Author(s):  
Hana Šimonová ◽  
Tomáš Trčka ◽  
Michal Bejček ◽  
Iva Rozsypalová ◽  
Petr Daněk ◽  
...  

The aim of this paper is to describe the procedure of determining the mechanical fracture parameters of selected concrete specimens taken from panels after the fire experiments. The records (in form load vs displacement diagrams) of three-point bending fracture tests of these specimens with initial stress concentrators was first advanced corrected and subsequently evaluated using the Effective Crack Model and the work-of-fracture method. The increasing temperatures during the fire experiments ranging between 550 to 1000 °C led to a decrease of modulus of elasticity and fracture toughness values and to the increase of fracture energy value. The 2D laser profile scanner was used to estimate the degree of complexity of fracture surfaces; its statistical dependence on the mechanical fracture parameters proved to be moderate – the absolute value of the correlation coefficient was about 0.5°[–].


2020 ◽  
Vol 309 ◽  
pp. 73-79
Author(s):  
Hana Šimonová ◽  
Ivana Kumpová ◽  
Iva Rozsypalová ◽  
Patrik Bayer ◽  
Petr Frantik ◽  
...  

This paper deals with selected alkali-activated aluminosilicate composites with a ceramic precursor in terms of their characterization using mechanical fracture parameters. Three composites were studied. They were manufactured using brick powder as a precursor and an alkaline activator with a dimensionless silicate modulus of Ms = 1.0, 1.2 and 1.4. The test specimens were nominally 40 × 40 × 160 mm in size and had a central edge notch with a depth of 1/3 of the specimen’s height. At least 6 specimens made of each composite were tested at the age of 28 days. The specimens were subjected to three-point bending tests, during which diagrams showing force vs. deflection at midspan (F–d diagrams) and force vs. crack mouth opening displacement (F–CMOD diagrams) were recorded. After the processing of these diagrams, values were determined for the static modulus of elasticity, effective fracture toughness (including its initiation component from the analysis of the first part of the F–CMOD diagrams), effective toughness and specific fracture energy using the effective crack model, Work-of-Fracture method, and Double-K fracture model. After the fracture experiments had been performed, compressive strength values were determined for informational purposes from one part of each specimen that remained after testing. In order to obtain visual information about the internal structure of the composites before and after the mechanical testing, the selected specimen was examined via X-ray microtomography. Tomographic measurements and image processing were performed for the qualitative and quantitative evaluation of internal structural changes with an emphasis on the calculation of porosimetry parameters as well as the visualization of the fracture process zone. The fractal dimension of the fracture surface and fracture process zone was determined. The porosity and microstructure images of selected samples taken from specimens were assessed.


2019 ◽  
Vol 9 (9) ◽  
pp. 1754 ◽  
Author(s):  
Hana Šimonová ◽  
Petr Frantík ◽  
Zbyněk Keršner ◽  
Pavel Schmid ◽  
Pavel Rovnaník

Knowledge of the mechanical and primarily fracture parameters of composites with a brittle matrix is essential for the quantification of their resistance to crack initiation and growth, and also for the specification of material model parameters employed for the simulation of the quasi-brittle behavior of structures made from this type of composite. Therefore, the main target of this paper is to quantify the mechanical fracture parameters of alkali-activated slag composites with steel microfibers and the contribution of the matrix to their fracture response. The first alkali-activated slag composite was a reference version without fibers; the others incorporated steel microfibers amounting to 5, 10, 15 and 20% by weight of the slag. Prism specimens with an initial central edge notch were used to perform the three-point bending fracture tests. Load vs. displacement (deflection at midspan) and load vs. crack mouth opening displacement diagrams were recorded during the fracture tests. The obtained diagrams were employed as inputs for parameter identification, the aim of which was to transfer the fracture test response data to the desired material parameters. Values were also determined for fracture parameters using the effective crack model, work-of-fracture method and double-K fracture model. All investigated mechanical fracture parameters were improved by the addition of steel microfibers to the alkali-activated matrix. Based on the obtained results, the addition of 10 to 15% of microfibers by weight is optimal from the point of view of the enhancement of the fracture parameters of alkali-activated slag composite.


2021 ◽  
Vol 1205 (1) ◽  
pp. 012019
Author(s):  
H Simonova ◽  
C Mizerova ◽  
P Rovnanik ◽  
M Lipowczan ◽  
P Schmid

Abstract In this study, the effect of carbon black and graphite filler on the crack initiation and fracture parameters of fly ash geopolymer mortar is investigated. The carbon black was added in the amount of 0.5 and 1.0% and graphite powder in the amount of 5 and 10% relative to the fly ash mass. The reference mixture without any filler was also prepared. The fracture characteristics were determined based on the results of the three-point bending test of prismatic specimens provided with an initial central edge notch. The fracture experiments were conducted at the age of 48 days. The vertical force (F), the displacement measured in the middle of the span length (d), and the crack mouth opening displacement (CMOD) were continuously recorded during the test. The records of fracture tests were subsequently evaluated using the effective crack model, work-of-fracture method, and double-K fracture model. The addition of both fine fillers led to a decrease in monitored mechanical fracture parameters in comparison with reference mortar.


2017 ◽  
Vol 259 ◽  
pp. 64-69
Author(s):  
Hana Šimonová ◽  
Petr Daněk ◽  
David Lehký ◽  
Zbyněk Keršner ◽  
Lubos Pazdera

In this paper, authors focus attention on mechanical fracture parameters obtained from records of three-point bending fracture tests on concrete specimens with initial notch. Total eight sets of specimens were tested. Three specimens at the age of 28 days were tested in each set. Concrete was different in dosage of Portland cement CEM I 42.5 R and amount of used superplasticizer. The Effective Crack Model (ECM) was used to evaluate the load vs deflection diagrams to obtain modulus of elasticity and effective fracture toughness; specific fracture energy was determined using work-of-fracture method. Modulus of elasticity, tensile strength and fracture energy were also subject of identification via inverse analysis based on artificial neural network, which aim is to transfer the input data obtained from the fracture test to the desired material parameters.


2020 ◽  
Vol 323 ◽  
pp. 01001 ◽  
Author(s):  
David Lehký ◽  
Hana Šimonová ◽  
Barbara Kucharczyková ◽  
Petr Daněk

The aim of the current research is to develop a complex multilevel approach for the experimental–computational determination of mechanical fracture parameters of concrete as a typical quasi-brittle material. This includes testing, advanced evaluation and soft computing-based identification of specimens of multiple sizes in multiple test configurations and analyses of fracture processes using multiscale modelling approaches. The evaluation of a part of an extensive experimental program is presented in this paper. The basic mechanical fracture parameters of the investigated concrete determined on standard test specimens with nominal dimensions of 100 × 100 × 400 mm subjected to the standard three-point bending fracture test are introduced. The results of three different sets of specimens provided with different depths of the initial notch are compared in terms of absolute values of the selected mechanical fracture parameters. The results indicate different sensitivity of particular mechanical fracture parameters in relation to the depth of the initial notch.


2021 ◽  
Vol 322 ◽  
pp. 3-8
Author(s):  
Iva Rozsypalová ◽  
Emília Bystrianska ◽  
Ondřej Koutný ◽  
Petr Daněk ◽  
Petr Frantík ◽  
...  

Mechanical fracture parameters were obtained for special fine-grained cement-based composites from three-point bending tests. A total of four sets of composite specimens were tested. All of the sets of composites were based on a general recipe and differ in the amount of high-strength aggregate and/or dispersed steel fibres present. Standardized prism specimens with a nominal size of 40 × 40 × 160 mm were used for the fracture tests after 131 days of curing. An initial notch was cut in the centre of the prisms with a depth approximately equal to one third of the specimen’s height. Three specimens from each set of composites were tested in the three-point bending fracture test configuration. Load versus midspan deflection diagrams were recorded. Experimentally obtained load vs displacement diagrams were corrected and analysed using the Effective Crack Model, the Work-of-Fracture method and an independent identification technique using numerical modelling. The most important mechanical fracture parameters, such as static modulus of elasticity, effective fracture toughness, specific fracture energy and effective tensile strength, were determined. Compressive and splitting tensile strength values were obtained from the halves of the specimens left over after the bending tests.


2018 ◽  
Vol 272 ◽  
pp. 185-188
Author(s):  
Barbora Svobodova ◽  
Hana Šimonová ◽  
Zbyněk Keršner

The structural concrete can be also characterized via parameters obtained by evaluation of fracture tests. Therefore, this paper presents software CheF developed in Java programming language, designed for evaluation of three-point bending fracture tests of core based concrete specimens with chevron type notch. The records of fracture tests in form load vs. displacement and load vs. crack mouth opening displacement diagrams are analysed by software CheF to obtain values of selected mechanical fracture parameters: modulus of elasticity E, fracture toughness KIc, and fracture energy GF, determined based on the linear elastic fracture mechanics approach and work-of-fracture method.


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