"Synthesis and characterization of Ba0.8Sr0.2TiO3 perovskite thin films prepared by Sol Gel Technique "

2020 ◽  
Vol 7 (2) ◽  
pp. 1-11
Author(s):  
Hamed A. Gatea ◽  
Iqbal Nahi
Keyword(s):  
Thin Films ◽  
Strontium Titanate ◽  
Barium Strontium Titanate ◽  
Perovskite Structure ◽  
Sol Gel ◽  
X Ray Diffraction ◽  
Barium Strontium ◽  
Intermediate Phases ◽  
Gel Technique

"Barium strontium Titanate (BST) is a solid solution consist of BaTiO3 and SrTiO3 that mixed with suitable ratio. Barium strontium Titanate oxide (Ba0.8Sr0.2TiO3) thin films prepared by sol gel technique. Barium strontium Titanate thin films deposited on Si substrate and annealed at [400,500, 600 and 700] ºC. The characterization of BST films investigated by a different technique, the X-Ray Diffraction (XRD) and Scanning Electron Macroscopy (SEM) revealed the phases, crystal structure and surface topography of the films. XRD pattern shows tetragonal phase for Ba0.8Sr0.2TiO3 perovskite structure with many peaks for different plans. The films annealed at the different temperature that indicated intermediate phases on perovskite structure of Ba0.8Sr0.2TiO3.

Preparation and Characterization of Nanosized Barium-Strontium Titanate Immobilized on Aluminum Oxide and its Application in Separation of Cr(III) and Cr(VI)

2010 ◽  
Vol 152-153 ◽  
pp. 1013-1016
Author(s):  
Hong Wang ◽  
Jing Yang
Keyword(s):  
Aluminum Oxide ◽  
Strontium Titanate ◽  
Barium Strontium Titanate ◽  
Sol Gel ◽  
Complete Separation ◽  
X Ray Diffraction ◽  
X Ray ◽  
Ph Values ◽  
Barium Strontium

Nanometer barium-strontium titanate based coated aluminum oxide (ABST) was prepared by the sol–gel method and characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and Fourier transform infrared spectrophotometry (FTIR). Its application in speciation of Cr(III) and Cr(VI) from water were studied. The results showed that the nanometer barium-strontium titanate was immobilized on aluminum oxide firmly, becoming a new adsorbent. Two forms of chromium showed different exchange capacities at different pH values, viz. Cr (III) selectively retained at pH 10–13, whereas Cr (VI) retained at pH 1. Hence complete separation of the two forms of chromium is possible. Retained species were eluted with 5mL of 1 mol•L−1 HCl and 1 mol•L−1 NaOH. The Cr(III) and Cr(VI) concentration was measured by atomic absorption spectroscopy. The adsorbent had a promising prospect in the separation of Cr(III) and Cr(VI) in environment water.

Physical Characterization of BST with Different (x’) Ratios

2014 ◽  
Vol 487 ◽  
pp. 106-109
Author(s):  
Nurhafizah Ramli ◽  
Zaliman Sauli ◽  
Vithyacharan Retnasamy ◽  
They Yee Chin ◽  
K. Anwar ◽  
...  
Keyword(s):  
Thin Films ◽  
Surface Roughness ◽  
Strontium Titanate ◽  
Barium Strontium Titanate ◽  
Sol Gel ◽  
Force Microscopy ◽  
Atomic Force ◽  
Fields Of Study ◽  
Barium Strontium

Nowdays Barium strontium titanate (BST) can be applied into many fields of engineering. Its properties attracted more researchers to research and apply it into many fields of study. In this work, sol-gel method of preparing barium strontium titanate (BST) has been used. This work was done with 4 different ratio of x with 4 different deposition layers. The main purpose of this work is to investigate the relation between the ratio of barium (Ba) with different deposition layer and the surface of the substrate. Atomic force microscopy (AFM) was used in whole work to investigate the crystalline structure and surface roughness of the BST thin films.

Preparation and Characterization of Nanosized Barium-Strontium Titanate Immobilized on Aluminum Oxide and Its Application in Adsorption

2010 ◽  
Vol 26-28 ◽  
pp. 682-685 ◽  
Author(s):  
Dong Zhang ◽  
Chun Li Zhang
Keyword(s):  
Aluminum Oxide ◽  
Strontium Titanate ◽  
Barium Strontium Titanate ◽  
Sol Gel ◽  
X Ray Diffraction ◽  
Composite Adsorbent ◽  
Cadmium Ions ◽  
Lead And Cadmium ◽  
Barium Strontium

Nanometer barium-stroutium titanate immobilized on aluminum oxide (ABST) was prepared by the citric acid sol–gel method and characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and Fourier transform infrared spectrophotometry (FTIR). Its Pb2+ and Cd2+ adsorption properties from water were studied. Adsorption and elution were investigated under different conditions. The results showed that the nanometer barium-strontium titanate was immobilized on aluminum oxide firmly, becoming a composite adsorbent. The lead and cadmium ions were quantitatively retained at pH 5-8; their adsorption capacities of ABST were 70.28 mg•g－1 and 8.12 mg•g－1, respectively. The adsorbent of adsorped lead and cadmium ions were regenerated completely by elution with 1 mol•L－1 HNO3. The adsorbent had a promising prospect in analyticl chemistry and water treatment.

Characterization of SrBi2Nb2O9 Thin Films Prepared by Sol Gel Technique

1996 ◽  
Vol 459 ◽  
Author(s):  
E. Ching-Prado ◽  
W. Pérez ◽  
A. Reynés-Figueroa ◽  
R. S. Katiyar ◽  
D. Ravichandran ◽  
...  
Keyword(s):  
Thin Films ◽  
Raman Band ◽  
Sol Gel ◽  
Orthorhombic Symmetry ◽  
X Ray Diffraction ◽  
Ft Ir ◽  
Gel Technique ◽  
High Degree ◽  
First Time

ABSTRACTThin films of SrBi2Nb2O9 (SBN) with thicknesses of 0.1, 0.2, and 0.4 μ were grown by Sol-gel technique on silicon, and annealed at 650°C. The SBN films were investigated by Raman scatering for the first time. Raman spectra in some of the samples present bands around 60, 167, 196, 222, 302, 451, 560, 771, 837, and 863 cm−1, which correspond to the SBN formation. The study indicates that the films are inhomogeneous, and only in samples with thicknesses 0.4 μ the SBN material was found in some places. The prominent Raman band around 870 cm−1, which is the A1g mode of the orthorhombic symmetry, is assigned to the symmetric stretching of the NbO6 octahedrals. The frequency of this band is found to shift in different places in the same sample, as well as from sample to sample. The frequency shifts and the width of the Raman bands are discussed in term of ions in non-equilibrium positions. FT-IR spectra reveal a sharp peak at 1260 cm−1, and two broad bands around 995 and 772 cm−1. The bandwidths of the latter two bands are believed to be associated with the presence of a high degree of defects in the films. The experimental results of the SBN films are compared with those obtained in SBT (T=Ta) films. X-ray diffraction and SEM techniques are also used for the structural characterization.

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