scholarly journals Quantitative Mapping of Strains and Young Modulus Based on Phase-Sensitive OCT

Author(s):  
Vladimir Y. Zaitsev ◽  
Lev A. Matveev ◽  
Alexander A. Sovetsky ◽  
Alexander L. Matveyev

Author(s):  
D.J. Eaglesham

Convergent Beam Electron Diffraction is now almost routinely used in the determination of the point- and space-groups of crystalline samples. In addition to its small-probe capability, CBED is also postulated to be more sensitive than X-ray diffraction in determining crystal symmetries. Multiple diffraction is phase-sensitive, so that the distinction between centro- and non-centro-symmetric space groups should be trivial in CBED: in addition, the stronger scattering of electrons may give a general increase in sensitivity to small atomic displacements. However, the sensitivity of CBED symmetry to the crystal point group has rarely been quantified, and CBED is also subject to symmetry-breaking due to local strains and inhomogeneities. The purpose of this paper is to classify the various types of symmetry-breaking, present calculations of the sensitivity, and illustrate symmetry-breaking by surface strains.CBED symmetry determinations usually proceed by determining the diffraction group along various zone axes, and hence finding the point group. The diffraction group can be found using either the intensity distribution in the discs



Author(s):  
Camila Ranucci de Luca ◽  
João Fellipe Souza ◽  
Paulo Torres ◽  
Heraldo da Costa Mattos


2002 ◽  
Vol 66 (1) ◽  
pp. 235 ◽  
Author(s):  
A. N. Kravchenko ◽  
G. A. Bollero ◽  
R. A. Omonode ◽  
D. G. Bullock


1979 ◽  
Vol 44 (6) ◽  
pp. 1942-1948 ◽  
Author(s):  
Jaroslav Hrouz ◽  
Michal Ilavský ◽  
Ivan Havlíček ◽  
Karel Dušek

The viscoelastic penetration and tensile behaviour of poly(methyl acrylate) and poly(ethyl acrylate) in the main transition region have been investigated. It was found that the time-temperature superposition could be carried out in the case of the penetration viscoelastic behaviour; the temperature dependence of the penetration and tensile shift factors was the same. The superimposed curves of the penetration and Young modulus allowed us to calculate the dependence of the Poisson ratio and thus to characterize the change in sample volume with deformation. It was demonstrated that the penetration method of determination of the viscoelastic behaviour is equivalent to the tensile method.



1997 ◽  
Vol 62 (11) ◽  
pp. 1747-1753 ◽  
Author(s):  
Radek Marek

Determination of 15N chemical shifts and heteronuclear coupling constants of substituted 2,2-dimethylpenta-3,4-dienal hydrazones is presented. The chemical shifts were determined by gradient-enhanced inverse-detected NMR techniques and 1H-15N coupling constants were extracted from phase-sensitive gradient-enhanced single-quantum multiple bond correlation experiments. Stereospecific behaviour of the coupling constants 2J(1H,15N) and 1J(1H,13C) has been used to determine the configuration on a C=N double bond. The above-mentioned compounds exist predominantly as E isomers in deuteriochloroform.



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