A Cu(ii) Schiff base complex immobilized on graphene oxide has been synthesized and characterized by FTIR, FT-RAMAN, XRD, UV, TEM, FE-SEM, EDAX, TGA, N2 adsorption–desorption and AAS analysis.
This study including prepared new colored esters containing heterocyclic with high molecular weights. In the first part of work we synthesized azo dyes [1,2] from the reaction p-toluidine with β-naphthol and o-nitro phenol, thin we synthesized Schiff bases [3,4] by the reaction anthranilic acid with benzaldehyde and dimethyl benzaldehyde. The reaction azo dyes (contain OH group) with Schiff base (contain COOH group) these led to produce the new colored esters [A1-A4]. The second part of work was modification the (C=N-) group in esters to heterocyclic compounds by reacting with phenyl iso cyanide to produce new β-lactam [B1-B4] and with anthranilic acid to get new hydroquinazoline [C1-C4]. All these compounds were characterized by physical properties and spectral methods FTIR, 1H-NMR and 13C-NMR.
Synthesis and Characterization of Graphene Oxide Supported Schiff Base Palladium Catalyst and Its Catalytic Performance to Suzuki Reaction