Complex Study of Eutectoidal Phase Transformation of 2507-Type Super-Duplex Stainless Steel

The aim of this work was to study expansively the process of the eutectoidal phase transformation of 2507-type super-duplex stainless steel. Three sample sets were prepared. The first sample set was made to investigate the effect of the previous cold rolling and heat treatment for the eutectoidal phase transformation. Samples were cold rolled at seven different rolling reductions which was followed by heat treatment at five different temperatures. The second sample set was prepared to determine the activation energy of the eutectoidal decomposition process using the Arrhenius equation. Samples were cold rolled at seven different rolling reductions and were heat treated at the same temperature during eight different terms. A third sample set was made to study how another plastic-forming technology, beside the cold rolling, can influence the eutectoidal decomposition. Samples were elongated by single axis tensile stress and were heat treated at the same temperature. The results of the first and the third sample sets were compared. The rest δ-ferrite contents were calculated using the results of AC and DC magnetometer measurements. DC magnetometer was used as a feritscope device in this work. Light microscope and electron back scattering diffraction (EBSD) images demonstrated the process of the eutectoidal decomposition. The thermoelectric power and the hardness of the samples were measured. The results of the thermoelectric power measurement were compared with the results of the δ-ferrite content measurement. The accurate value of the coercive field was determined by a Foerster-type DC coercimeter device.

Plastic Deformation and Thermal Induced Phase Transformation in 2507 Type Super Duplex Stainless Steel

The aim of this study was to investigate the effect of the previously applied cold rolling and the latter heat treatment for the eutectoidal decomposition of δ-ferrite in 2507 type superduplex stainless steel (SDSS). The samples were cold rolled at seven different deformation rates which was followed by heat treatment at were 20, 700, 750, 800 and 850 °C temperatures. The rolled and heat treated samples were investigated by hardness tester, AC magnetometer and thermoelectric power measurement. The activation energy of the decomposition was determined by the Arrhenius equation through the results of the AC magnetometer measurement.

The Microstructure and Mechanical Properties of the Ni-Al-V Alloys Prepared by Levitation and Crystallization in Copper Mould

Microstructure and mechanical properties of NiAlV alloys of the composition belonging to the pseudo-binary Ni3Al-Ni3V cross-section were investigated. The samples were prepared by the cold crucible levitation melting (CCLM) and by re-melting and crystallizing in the small volume copper mould. The phase composition of the samples, with should result from the eutectoidal decomposition was not found. Instead the Ni3(Al,V) and Ni(Al,V) solid solution or seldom disordered solid solution were retained due to the relatively high cooling rates. In the compression test the NiAlV alloys crystallized in the copper mould revealed high ductility and strength.

Phase Transformations in Co5Sm

Much higher magnetic coercivities than were previously available have been attained with the compound Co5Sm. However, coercivity is very sensitive to heat treatment; in particular, annealing near 750°C substantially reduces coercivity. This has been attributed to a possible eutectoidal decomposition of Co5Sm into CO17Sm12 and CO7Sm12 on the basis of optical metallography. This possibility makes it necessary to obtain basic electron microstructural information from CO5Sm heat treated in this temperature range.High quality Co5Sm crystals were annealed in sealed Mo bombs at 750°C for 10 days. Electron transparent specimens were prepared by ion thinning in a commercialion milling apparatus.