Effect of Annealing Temperature on the Structural and Magnetic Properties of Terbium Iron Garnet Thin Films Prepared by Sol-Gel Method

Author(s):  
Ftema W. Aldbea ◽  
N. B. Ibrahim
2013 ◽  
Vol 756 ◽  
pp. 91-98 ◽  
Author(s):  
Ftema W. Aldbea ◽  
Noor Bahyah Ibrahim ◽  
Mustafa Hj. Abdullah

Terbium –substituted yttrium iron garnet (Tb1.5Y1.5Fe5O12) films nanoparticles were successfully prepared by a sol-gel method. The films were deposited on the quartz substrate using spin coating technique. To study effect of annealing temperature, the annealing process was executed at 700, 800 and 900 °C in air for 2 hours. The X-ray diffraction (XRD) proved that the pure phase of garnet structure was detected for the film annealed at 900 °C. The lattice parameter increased with the increment of annealing temperature and the highest value of 12.35 Å was obtained at 900 °C. Field Emission Scanning Electron Microscope (FE-SEM) results showed that the particle size increased from 43nm to 56nm as annealing temperature increased from 700 to 900°C. The film’s thickness also affected by increasing of annealing temperature and become thin at 900 °C due to densification process occurred at high annealing temperature. The elemental compositions of the Tb1.5Y1.5Fe5O12 film were detected using an Energy Dispersive X-raySpectroscopy (EDX). Magnetic properties at room temperature were measured using a Vibrating Sample Magnetometer (VSM).The saturation magnetization Ms increased with the annealingtemperature and showed a high value of 104emu/cm3, but the coercivity Hc of the film was decreased due to the increment of the particle size. Normal 0 21 false false false MS X-NONE X-NONE MicrosoftInternetExplorer4 Terbium –substituted yttrium iron garnet (Tb1.5Y1.5Fe5O12) films nanoparticles were successfully prepared by a sol-gel method. The films were deposited on the quartz substrate using spin coating technique. To study effect of annealing temperature, the annealing process was executed at 700, 800 and 900°C in air for 2 hours. The X-ray diffraction (XRD) proved that the pure phase of garnet structure was detected for the film annealed at 900 °C. The lattice parameter increased with the increment of annealing temperature and the highest value of 12.35 Å was obtained at 900 °C. Field Emission Scanning Electron Microscope (FE-SEM) results showed that the particle size increased from 43nm to 56nm as annealing temperature increased from 700 to 900 °C. The film’s thickness also affected by increasing of annealing temperature and become thin at 900 °C due to densification process occurred at high annealing temperature. The elemental compositions of the Tb1.5Y1.5Fe5O12 film were detected using an Energy Dispersive X-ray Spectroscopy (EDX). Magnetic properties at room temperature were measured using a Vibrating Sample Magnetometer (VSM).The saturation magnetization Ms increased with the annealing temperature and showed a high value of 104emu/cm3, but the coercivity Hc of the film was decreased due to the increment of the particle size. st1\:*{behavior:url(#ieooui) } /* Style Definitions */ table.MsoNormalTable {mso-style-name:"Table Normal"; mso-tstyle-rowband-size:0; mso-tstyle-colband-size:0; mso-style-noshow:yes; mso-style-priority:99; mso-style-qformat:yes; mso-style-parent:""; mso-padding-alt:0cm 5.4pt 0cm 5.4pt; mso-para-margin:0cm; mso-para-margin-bottom:.0001pt; mso-pagination:widow-orphan; font-size:11.0pt; font-family:"Calibri","sans-serif"; mso-ascii-font-family:Calibri; mso-ascii-theme-font:minor-latin; mso-fareast-font-family:"Times New Roman"; mso-fareast-theme-font:minor-fareast; mso-hansi-font-family:Calibri; mso-hansi-theme-font:minor-latin; mso-bidi-font-family:"Times New Roman"; mso-bidi-theme-font:minor-bidi;}


2002 ◽  
Vol 189 (3) ◽  
pp. 883-887
Author(s):  
Sam Jin Kim ◽  
Woo Chul Kim ◽  
In Bo Shim ◽  
Chul Sung Kim ◽  
Seung Wha Lee

2019 ◽  
Vol 45 (6) ◽  
pp. 6906-6911 ◽  
Author(s):  
Q.S. Fu ◽  
C.L. Li ◽  
B. Meng ◽  
C. Chakrabarti ◽  
R. Zhang ◽  
...  

2019 ◽  
Vol 236 ◽  
pp. 547-549 ◽  
Author(s):  
L.R.F. Leal ◽  
Y. Guerra ◽  
E. Padrón-Hernández ◽  
A.R. Rodrigues ◽  
F.E.P. Santos ◽  
...  

2012 ◽  
Vol 12 (2) ◽  
pp. 950-954 ◽  
Author(s):  
Masoud Karimipour ◽  
J. Magnus Wikberg ◽  
Nasser Shahtahmasebi ◽  
Mahmood Rezaee Rokn Abad ◽  
M. M. Bagheri-Mohagheghi ◽  
...  

2016 ◽  
Vol 34 (2) ◽  
pp. 362-367 ◽  
Author(s):  
I. Yarici ◽  
M. Erol ◽  
E. Celik ◽  
Y. Ozturk

AbstractCerium substituted yttrium iron garnet (Ce0.2Y2.8Fe5O12; Ce-YIG) nanoparticles were produced via the sol-gel method from solutions of Ce-, Y- and Fe-based precursors, a solvent and a chelating agent. The solutions were dried at 200°C and heat treated at temperatures between 800 °C and 1400°C for 3 h in air. The effects of pH and annealing temperature on the structure, phase formation, magnetic properties and crystallite size were investigated. A cubic YIG phase was obtained for the sample annealed at 1400 °C. The presented results showed that the pH value of the starting solution affects the crystal size and consequently, the saturation magnetization.


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