Vibrated Bulk Density using Semi-automated Device: Simplifying Sample Preparation while Improving Accuracy and Precision

2012 ◽  
pp. 1279-1281 ◽  
Author(s):  
Jignesh Panchal ◽  
Jeffrey Rolle
2011 ◽  
Vol 4 (4) ◽  
pp. 385-394 ◽  
Author(s):  
J. Meneely ◽  
F. Ricci ◽  
S. Vesco ◽  
M. Abouzied ◽  
M. Sulyok ◽  
...  

Many different immunochemical platforms exist for the screening of naturally occurring contaminants in food from the low cost enzyme linked immunosorbent assays (ELISA) to the expensive instruments such as optical biosensors based on the phenomenon of surface plasmon resonance (SPR). The primary aim of this study was to evaluate and compare a number of these platforms to assess their accuracy and precision when applied to naturally contaminated samples containing HT-2/T-2 mycotoxins. Other important factors considered were the speed of analysis, ease of use (sample preparation techniques and use of the equipment) and ultimately the cost implications. The three screening procedures compared included an SPR biosensor assay, a commercially available ELISA and an enzymelinked immunomagnetic electrochemical array (ELIME array). The qualitative data for all methods demonstrated very good overall agreements with each other, however on comparison with mass spectrometry confirmatory results, the ELISA and SPR assay performed slightly better than the ELIME array, exhibiting an overall agreement of 95.8% compared to 91.7%. Currently, SPR is more costly than the other two platforms and can only be used in the laboratory whereas in theory both the ELISA and ELIME array are portable and can be used in the field, but ultimately this is dependent on the sample preparation techniques employed. Sample preparative techniques varied for all methods evaluated, the ELISA was the most simple to perform followed by that of the SPR method. The ELIME array involved an additional clean-up step thereby increasing both the time and cost of analysis. Therefore in the current format, field use would not be an option for the ELIME array. In relation to speed of analysis, the ELISA outperformed the other methods.


1988 ◽  
Vol 32 ◽  
pp. 221-226
Author(s):  
Wayne Watson ◽  
Jim Parker ◽  
Anthony R. Harding

AbstractVarious sample preparation methods for Energy Dispersive X-ray Fluorescence (EDXRF) analysis of Portland cement were compared in order to evaluate improvement in analytical accuracy and precision. Sample preparation requirements for EDXRF are slightly different than for Wavelength Dispersive X-ray Fluorescence (WDXRF), and the methods commonly used in WDXRF are not optimized for EDXRF. Primarily, the work focuses on techniques for producing a fused sample with the lowest practical concentration of lithium borate flux. Determination of minimum detection limits were made from samples with varying proportions of flux in order to evaluate analytical optimization. Ease and reproducibility of preparation of the sample was also considered.


1986 ◽  
Vol 1 (2) ◽  
pp. 51-63 ◽  
Author(s):  
R. Jenkins ◽  
T. G. Fawcett ◽  
D. K. Smith ◽  
J. W. Visser ◽  
M. C. Morris ◽  
...  

The aim of any diffraction experiment is to obtain reproducible data of high accuracy and precision so that the data can be correctly interpreted and analyzed. Various methods of sample preparation have been devised so that reproducibility, precision and accuracy can be obtained. The success of a diffraction experiment will often depend on the correct choice of preparation method for the sample being analyzed and for the instrument being used in the analysis.A diffraction pattern contains three types of useful information: the positions of the diffraction maxima, the peak intensities, and the intensity distribution as a function of diffraction angle. This information can be used to identify and quantify the contents of the sample, as well as to calculate the material's crystallite size and distribution, crystallinity, and stress and strain. The ideal preparation for a given experiment depends largely on information desired.


2020 ◽  
Vol 8 (4) ◽  
pp. 995-1020
Author(s):  
Joel Mohren ◽  
Steven A. Binnie ◽  
Gregor M. Rink ◽  
Katharina Knödgen ◽  
Carlos Miranda ◽  
...  

Abstract. The quantification of soil bulk density (ρB) is a cumbersome and time-consuming task when traditional soil density sampling techniques are applied. However, it can be important for terrestrial cosmogenic nuclide (TCN) production rate scaling when deriving ages or surface process rates from buried samples, in particular when short-lived TCNs such as in situ 14C are applied. Here, we show that soil density determinations can be made using structure-from-motion multi-view stereo (SfM-MVS) photogrammetry-based volume reconstructions of sampling pits. Accuracy and precision tests as found in the literature and as conducted in this study clearly indicate that photographs taken from both a consumer-grade digital single-lens mirrorless (DSLM) and a smartphone camera are of sufficient quality to produce accurate and precise modelling results, i.e. to regularly reproduce the “true” volume and/or density by >95 %. This finding holds also if a freeware-based computing workflow is applied. The technique has been used to measure ρB along three small-scale (<1 km) N–S transects located in the semi-arid to arid Altos de Talinay, northern central Chile (∼30.5∘ S, ∼71.7∘ W), during a TCN sampling campaign. Here, long-term differences in microclimatic conditions between south-facing and north-facing slopes (SFSs and NFSs, respectively) explain a sharp contrast in vegetation cover, slope gradient and general soil condition patterns. These contrasts are also reflected by the soil density data, generally coinciding with lower densities on SFSs. The largest differences between NFSs and SFSs are evident in the lower portion of the respective slopes, close to the thalwegs. In general, field-state soil bulk densities were found to vary by about 0.6 g cm−3 over a few tens of metres along the same slope. As such, the dataset that was mainly generated to derive more accurate TCN-based process rates and ages can be used to characterise the present-day condition of soils in the study area, which in turn can give insight into the long-term soil formation and prevailing environmental conditions. This implies that the method tested in this study may also being applied in other fields of research and work, such as soil science, agriculture or the construction sector.


2008 ◽  
Author(s):  
J. Abrantes ◽  
N. R. Pinhão ◽  
J. Melo ◽  
M. J. Madruga ◽  
Emanuela Cincu ◽  
...  

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