Effect of High Sintering Temperature on the Cobalt Ferrite Synthesized Via Co-precipitation Method

2020 ◽  
pp. 233-242
Author(s):  
Siti Maisarah Ahmad Tarmizi ◽  
Muhammad Amin Zamri ◽  
Nur Azmah Nordin ◽  
Rizuan Mohd Rosnan ◽  
Saiful Amri Mazlan ◽  
...  
Keyword(s):  
Cobalt Ferrite ◽  
Sintering Temperature ◽  
Precipitation Method ◽  
Co Precipitation

scholarly journals Structure, Luminescence, and Magnetic Properties of Crystalline Manganese Tungstate Doped with Rare Earth Ion

Materials ◽  
2021 ◽  
Vol 14 (13) ◽  
pp. 3717
Author(s):  
Jae-Young Jung ◽  
Soung-Soo Yi ◽  
Dong-Hyun Hwang ◽  
Chang-Sik Son
Keyword(s):  
Magnetic Field ◽  
Rare Earth ◽  
Sintering Temperature ◽  
Luminescent Properties ◽  
Concentration Quenching ◽  
Rare Earth Ions ◽  
Precipitation Method ◽  
Rare Earth Ion ◽  
Co Precipitation ◽  
Quenching Phenomenon

The precursor prepared by co-precipitation method was sintered at various temperatures to synthesize crystalline manganese tungstate (MnWO4). Sintered MnWO4 showed the best crystallinity at a sintering temperature of 800 °C. Rare earth ion (Dysprosium; Dy3+) was added when preparing the precursor to enhance the magnetic and luminescent properties of crystalline MnWO4 based on these sintering temperature conditions. As the amount of rare earth ions was changed, the magnetic and luminescent characteristics were enhanced; however, after 0.1 mol.%, the luminescent characteristics decreased due to the concentration quenching phenomenon. In addition, a composite was prepared by mixing MnWO4 powder, with enhanced magnetism and luminescence properties due to the addition of dysprosium, with epoxy. To one of the two prepared composites a magnetic field was applied to induce alignment of the MnWO4 particles. Aligned particles showed stronger luminescence than the composite sample prepared with unsorted particles. As a result of this, it was suggested that it can be used as phosphor and a photosensitizer by utilizing the magnetic and luminescent properties of the synthesized MnWO4 powder with the addition of rare earth ions.

scholarly journals Effect of Sintering Temperature on the Microstructure, Electrical and Magnetotransport Properties of La0.67Sr0.33MnO3 Compound

2014 ◽  
Vol 895 ◽  
pp. 319-322
Author(s):  
Lim Kean Pah ◽  
Abdul Halim Shaari ◽  
Chen Soo Kien ◽  
Chin Hui Wei ◽  
Albert Gan ◽  
...  
Keyword(s):  
Grain Size ◽  
Single Phase ◽  
Sintering Temperature ◽  
Measurement Range ◽  
Hexagonal Structure ◽  
Precipitation Method ◽  
Metal Insulator ◽  
Higher Temperature ◽  
Co Precipitation ◽  
Grain Surface

In this work, we report the effect of sintering temperature (900°C, 1000°C, 1100°C and 1200°C) on the electrical and magnetotransport properties of polycrystalline La0.67Sr0.33MnO3 (LSMO). Single phase of LSMO hexagonal structure (R-3c) accompanied with minor phases was successfully synthesized by co-precipitation method. With increasing sintering temperature, grain growth was promoted and grain connectivity was improved. It was found that an enhancement of resistivity on smaller grain size was due to larger grain surface over volume (grain boundaries effect). The shifting of the metal-insulator transition (TMI) to higher temperature was also responsible for observed changes in physical properties. TMI of 900°C, 1000°C and 1100°C were 232 K, 278 K and 298 K respectively however 1200°C was out of measurement range (higher than 300 K). In summary, CP900 with smaller grain size distribution (~200 nm) displayed the highest resistivity and MR% of -19.2% (at 80 K, 10 kG).

Composition and magnetic properties of cobalt ferrite nano-particles prepared by the co-precipitation method

2010 ◽  
Vol 322 (21) ◽  
pp. 3470-3475 ◽  
Author(s):  
Yue Zhang ◽  
Zhi Yang ◽  
Di Yin ◽  
Yong Liu ◽  
ChunLong Fei ◽  
...  
Keyword(s):  
Magnetic Properties ◽  
Cobalt Ferrite ◽  
Nano Particles ◽  
Precipitation Method ◽  
Co Precipitation

PREPARING DOUBLE-BASE THERMO-SENSITIVE CERAMICS WITH NANOPOWDERS

2006 ◽  
Vol 05 (02n03) ◽  
pp. 265-271
Author(s):  
MENG KUI WANG ◽  
YU QIANG YANG
Keyword(s):  
Ceramic Material ◽  
Thick Film ◽  
Production Cost ◽  
Sintering Temperature ◽  
Precipitation Method ◽  
Sensitive Material ◽  
Surface Active Agents ◽  
Surface Active ◽  
Co Precipitation ◽  
Double Base

The preparing process and the properties of thick-film double-based thermo-sensitive material were studied. The preparing steps were as follows: (i) preparing Ba 1-x Sr x TiO 3 micro-powders with chemical co-precipitation method; (ii) adding dispersants and surface active agents into crushing medium powders to prepare Ba 1-x Sr x TiO 3 nanopowders; (iii) preparing V 2 O 3-based micro-powders; (iv) mixing Ba 1-x Sr x TiO 3 nanopowders, V 2 O 3-based micro-powders, donor impurities, acceptor impurities and micro additives according to a certain ratio to make thick-film thermo-sensitive ceramic material. The presintering and sintering temperature of the prepared PTC ceramics were both reduced, which is very meaningful in using cheaper SiC instead of more expensive MoSi 2, prolonging the kiln's life, and lowering the production cost. The samples we prepared did not contain PbO , so they are safe to the environment.

Sign in / Sign up

Export Citation Format

Share Document