In situ synthesis of silver nanoparticles on dialdehyde cellulose as reliable SERS substrate

Cellulose ◽  
2021 ◽  
Author(s):  
Qiutian She ◽  
Jie Li ◽  
Yudong Lu ◽  
Shan Lin ◽  
Ruiyun You
2014 ◽  
Vol 53 (11) ◽  
pp. 4147-4155 ◽  
Author(s):  
Anna Bacciarelli-Ulacha ◽  
Edward Rybicki ◽  
Edyta Matyjas-Zgondek ◽  
Aleksandra Pawlaczyk ◽  
Malgorzata I. Szynkowska

2016 ◽  
Vol 87 (19) ◽  
pp. 2407-2419 ◽  
Author(s):  
Qingqing Zhou ◽  
Jingchun Lv ◽  
Yu Ren ◽  
Jiayi Chen ◽  
Dawei Gao ◽  
...  

This study presented a simple and environmentally friendly method of in situ synthesis of silver nanoparticles (AgNPs) on cotton fabrics for durable ultraviolet (UV) protection and antibacterial activity using Aloe vera leaf extraction (AVE) as a reducing and stabilizing agent. Cotton fabrics were pretreated in water, and then immersed in AgNO3 and AVE, respectively. Cotton fabrics were characterized by small angle X-ray diffraction (XRD), scanning electron microscopy (SEM), thermogravimetric analysis, UV protection, antibacterial activity, and laundering durability. Comparing with the smooth surface of the control cotton fabric, SEM and energy dispersive X-ray spectrometry (EDX) results showed that there were a considerable number of Ag2O and AgNPs loading on the surface of the pretreated and Ag loaded cotton fabrics. The XRD pattern indicated, respectively, the existence of Ag2O and AgNPs, the structures of which were similar to JCPDS File No.65-3289 and JCPDS File No. 01-071-4613 on the pretreated and Ag loaded cotton fabrics. The pretreated and Ag loaded cotton fabrics showed excellent UV protection, antibacterial activity, and laundering durability, especially the Ag loaded cotton fabric, of which the UV protection factor value and transmission of UVA were 148 and 1.11%, respectively, after 20 washing cycles, and the clear zone width was more than 4 mm against E. coli or S. aureus. AgNPs facilitated the improvement of the thermal property of the cotton fabrics. Thus this facile in situ reduction of AgNPs with AVE may bring a promising and green strategy to produce functional textiles.


Nanomaterials ◽  
2019 ◽  
Vol 9 (3) ◽  
pp. 384 ◽  
Author(s):  
Zhiliang Zhang ◽  
Tiantian Si ◽  
Jun Liu ◽  
Guowei Zhou

The rapid sampling and efficient collection of target molecules from a real-world surface is fairly crucial for surface-enhanced Raman scattering (SERS) to detect trace pesticide residues in the environment and in agriculture fields. In this work, a versatile approach was exploited to fabricate a flexible SERS substrate for highly sensitive detection of carbaryl pesticides, using in-situ grown silver nanoparticles (AgNPs)on non-woven (NW) fabric surfaces based on mussel-inspired polydopamine (PDA) molecules. The obtained NW@PDA@AgNPs fabrics showed extremely sensitive and reproducible SERS signals toward crystal violet (CV) molecules, and the detection limit was as low as 1.0 × 10−12 M. More importantly, these NW@PDA@AgNPs fabrics could be directly utilized as flexible SERS substrates for the rapid extraction and detection of trace carbaryl pesticides from various fruit surfaces through a simple swabbing approach. It was identified that the detection limits of carbaryl residues from apple, orange, and banana surfaces were approximately decreased to 4.02 × 10−12, 6.04 × 10−12, and 5.03 × 10−12 g, respectively, demonstrating high sensitivity and superior reliability. These flexible substrates could not only drastically increase the collection efficiency from multifarious irregular-shaped matrices, but also greatly enhance analytical sensitivity and reliability for carbaryl pesticides. The fabricated flexible and multifunctional SERS substrates would have great potential to trace pesticide residue detection in the environment and bioscience fields.


2020 ◽  
Vol 208 (1) ◽  
pp. 10-16
Author(s):  
Zhenming Qi ◽  
Ruizhi Zhang ◽  
Jingchun Lv ◽  
Dawei Gao ◽  
Chunxia Wang

2011 ◽  
Vol 364 ◽  
pp. 439-443 ◽  
Author(s):  
Soon Wei Chook ◽  
Chin Hua Chia ◽  
Zakaria Sarani ◽  
Mohd Khan Ayob ◽  
Kah Leong Chee ◽  
...  

Graphene oxide (GO) sheets, a single layer of carbon atoms which can be served as substrates for fabricating metallic nanoparticles-GO nanocomposites. In this study, the nanocomposite of silver nanoparticles and graphene oxide were produced via in-situ synthesis and with the addition of chitosan to investigate the formation of silver nanoparticles on the graphene oxide sheets. XRD and UV-Vis studies confirmed the formation of silver nanoparticles on GO sheets, while TEM and FESEM images presented the loading of silver nanoparticles on the GO sheets. The degree of loading and distribution of the silver nanoparticles on the graphene oxide were depend on the method during the formation of silver nanoparticles. The nanocomposites can be potentially used in food packaging and biomedical applications.


Sign in / Sign up

Export Citation Format

Share Document