scholarly journals Microstructure and properties of a vacuum-tempered glass with low-temperature-sintered silver paste

Author(s):  
Qin Sun ◽  
Guoji Sun ◽  
Yihan Liu ◽  
Yufeng Li ◽  
Hongtao Chen ◽  
...  
2021 ◽  
Author(s):  
Qin Sun ◽  
Guoji Sun ◽  
Yihan Liu ◽  
Yufeng Li ◽  
Hongtao Chen ◽  
...  

Abstract A low-temperature sintered silver paste was used for metallization on tempered glass to prepare a vacuum tempered glass by soldering with Sn 96.5 Ag 3 Cu 0.5 paste (SAC305). The effects of the glass content and the sintering temperature on the microstructures, shear strengths, and fracture mechanisms of the bondlines were investigated in detail. The microstructure of the thick silver film and its interface with the tempered glass was characterized. The dissolution and precipitation behaviors of the silver in Bi-B-Zn glass were also analyzed. Bi 4 B 2 O 9 crystals were detected in the microstructure of the thick silver film when the joining temperature was increased above 450 °C, which can strengthen the silver film and the interface with the tempered glass. After soldering at 450 °C for 10 min, an excellent bondline was formed with a shear strength of 42.3 MPa and a leak rate of 7.2 × 10 -3 Pa.cm 3 /s by using the low-temperature sintered paste, which had a composition of 80 wt.% silver and 20 wt.% glass powder. Furthermore, heat transfer tests revealed that the vacuum tempered glass had excellent thermal insulation properties. The results showed that the low-temperature sintered silver paste combined with soldering was an effective method to prepare vacuum tempered glass.


2013 ◽  
Vol 2 (4) ◽  
pp. 166-172
Author(s):  
Shuji NISHIMOTO ◽  
Nobuyuki TERASAKI ◽  
Yoshiyuki NAGATOMO ◽  
Toshiyuki NAGASE ◽  
Yoshirou KUROMITSU

Author(s):  
Xinyue Wang ◽  
Zejun Zeng ◽  
Guoqi Q. Zhang ◽  
Jing Zhang ◽  
Pan Liu

Abstract Recent years, the sintered silver paste was introduced and further developed for power electronics packaging due to low processing temperature and high working temperature. The pressure-less sintering technology reduces the stress damage caused by the pressure to the chip, improves reliability, and is widely applied in manufacturing. Currently, most existed studies are focused on alcohol-based sintered silver pastes while resins have been demonstrated to improve the bonding properties of solder joints. Hence, the performance and sintering mechanisms with epoxy-based silver paste need to be further explored. In this work, a methodology for multi-factor investigation is settled on the epoxy-based silver paste to reveal the relationship between the strength and the different influence factors. We firstly analyzed the characteristics of commercialized epoxy-based silver paste samples, including silver content, silver particle size, organic paste composition, sample viscosity, and thermal conductivity. Samples were then prepared for shear tests and microstructure analysis under different pressure-less sintering temperatures, holding time, substrate surface, and chip size. Full factor analysis results were further discussed in detail for correlation. The influence factors were ranked from strong to weak as follows: sintering temperature, substrate surface, chip size, and holding time. Finally, a thermal cycling test was carried out for reliability analysis. Epoxy residues are one of the possible reasons which result in shear strength decreasing exponentially.


Coatings ◽  
2018 ◽  
Vol 8 (12) ◽  
pp. 451 ◽  
Author(s):  
Hongmei Zhu ◽  
Yongzuo Li ◽  
Baichun Li ◽  
Zhenyuan Zhang ◽  
Changjun Qiu

Post-treatment is crucial to improve the comprehensive performance of laser-cladded martensitic stainless steel coatings. In this work, a low-temperature tempering treatment (210 °C), for the first time, was performed on the laser-cladded AISI 420 martensitic stainless steel coating. The microstructure and properties of the pre- and post-tempering specimens were carefully investigated by XRD, SEM, TEM, a micro-hardness tester, a universal material testing machine and an electrochemical workstation. The results show that the as-cladded AISI 420 stainless steel coating mainly consisted of martensite, austenite, Fe3C and M23C6 carbides. The phase constituent of the coating remained the same, however, the martensite decomposed into finer tempered martensite with the precipitation of numerous nano-sized Fe3C carbides and reverted austenite in the as-tempered specimen. Moreover, a slight reduction was found in the micro-hardness and tensile strength, while a significant increase in elongation was achieved after tempering. The fractography showed a transition from brittle fracture to ductile fracture accordingly. The as-tempered coating exhibited a striking combination of mechanical properties and corrosion resistance. This work can provide a potential strategy to enhance the overall properties of the laser-deposited Fe-based coating for industrial applications.


2016 ◽  
Vol 42 (8) ◽  
pp. 10144-10150 ◽  
Author(s):  
Xiaoyu Cao ◽  
Xiaowei Yin ◽  
Xiaokang Ma ◽  
Xiaomeng Fan ◽  
Yanzhi Cai ◽  
...  

2007 ◽  
Vol 36 (10) ◽  
pp. 1333-1340 ◽  
Author(s):  
Tao Wang ◽  
Xu Chen ◽  
Guo-Quan Lu ◽  
Guang-Yin Lei

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