Thermal degradation and evolved gas analysis of some vegetable oils using TG/FT-IR/MS technique

2014 ◽  
Vol 119 (3) ◽  
pp. 1703-1711 ◽  
Author(s):  
N. Tudorachi ◽  
F. Mustata
The Analyst ◽  
2019 ◽  
Vol 144 (18) ◽  
pp. 5589-5599 ◽  
Author(s):  
Filip Kunc ◽  
Vinod Balhara ◽  
Ying Sun ◽  
Malgosia Daroszewska ◽  
Zygmunt J. Jakubek ◽  
...  

Thermogravimetric analysis (TGA) coupled with evolved gas analysis-FT-IR has been examined as a potential method to study the functional group content for surface modified silica nanoparticles.


2014 ◽  
Vol 120 (1) ◽  
pp. 789-794 ◽  
Author(s):  
Fabio Sonvico ◽  
Victoria Coleman ◽  
Daniela Traini ◽  
Paul M. Young

2017 ◽  
Vol 68 (11) ◽  
pp. 2734-2738
Author(s):  
Mihai Dumitras ◽  
Dan Maftei ◽  
Anton Airinei ◽  
Nita Tudorachi ◽  
Alin Constantin Dirtu

This study aims to investigate the thermal degradation behavior of decabromodiphenyl ether (BDE 209) by simultaneous TG/DTA under various conditions. Due to low volatility, high elution temperatures are needed when applying chromatographic techniques for this class of flame retardants (FR), resulting in thermal degradation affecting analysis results, but no systematic study has been reported. Kinetic analysis was performed by the non-parametric (NPK) method, and in correlation with evolved gas analysis (EGA) information and molecular modeling results, provided valuable insight into the kinetics and mechanism of BDE 209 thermal degradation. The conclusions were aimed at designing proper specific GC analytical methods for the selected FRs and serving for a better estimation of the human exposure to such compounds.


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