Oxidative regeneration study of spent V2O5 catalyst from sulfuric acid manufacture

Converter was one tool unit that consisting 4 beds in the production process of sulfuric acid. The performance of this converter was supported by the addition of a vanadium pentaoxide (V2O5) catalyst. The process that occurring in the converter was double contacts – double absorbers. The purpose of this case was converter performance evaluation that using by SO2 conversion parameter to SO3. Primary data was the dry air flow rate that entering the burner, the SO2 gas content that be into the converter, the catalyst temperature of each converter bed, and the catalyst pressure in each bed converter. Data on the field showed that activity on bed I was 72,96%, and theoretical was 60%. Then, bed II gave 91,22%; 87%; on bed III was 96,85%; 94%; and bed IV was 99,9%; 99,73% as respectively. From these experiments could be concluded that result data was greater than the theoretical. The difference of this conversion indicated that the performance of the converter did not increase

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Preparation of Thin Cadmium Telluride Samples for Electron Microscope Studies

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100052754 ◽

1974 ◽

Vol 32 ◽

pp. 548-549

Author(s):

T. J. Magee ◽

J. Peng ◽

J. Bean

Keyword(s):

Electron Microscope ◽

Sulfuric Acid ◽

Solid State ◽

Sample Preparation ◽

Cadmium Telluride ◽

Potassium Dichromate ◽

Optical Components ◽

The Past ◽

Solid State Devices

Cadmium telluride has become increasingly important in a number of technological applications, particularly in the area of laser-optical components and solid state devices, Microstructural characterizations of the material have in the past been somewhat limited because of the lack of suitable sample preparation and thinning techniques. Utilizing a modified jet thinning apparatus and a potassium dichromate-sulfuric acid thinning solution, a procedure has now been developed for obtaining thin contamination-free samples for TEM examination.

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Physical, Chemical, and Crystallographic Characterization of Anodic Coatings on High Strength Aluminum Base Alloys

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100093146 ◽

1976 ◽

Vol 34 ◽

pp. 636-637

Author(s):

R. E. Herfert ◽

N. T. McDevitt

Keyword(s):

Sulfuric Acid ◽

Salt Spray ◽

High Strength ◽

Environmental Stability ◽

Anodic Films ◽

Sodium Dichromate ◽

Corrosion Resistant ◽

Aerospace Applications ◽

Bond Strengths ◽

Adhesive Bonded Joints

Durability of adhesive bonded joints in moisture and salt spray environments is essential to USAF aircraft. Structural bonding technology for aerospace applications has depended for many years on the preparation of aluminum surfaces by a sulfuric acid/sodium dichromate (FPL etch) treatment. Recently, specific thin film anodizing techniques, phosphoric acid, and chromic acid anodizing have been developed which not only provide good initial bond strengths but vastly improved environmental durability. These thin anodic films are in contrast to the commonly used thick anodic films such as the sulfuric acid or "hard" sulfuric acid anodic films which are highly corrosion resistant in themselves, but which do not provide good initial bond strengths, particularly in low temperature peel.The objective of this study was to determine the characteristics of anodic films on aluminum alloys that make them corrosion resistant. The chemical composition, physical morphology and structure, and mechanical properties of the thin oxide films were to be defined and correlated with the environmental stability of these surfaces in humidity and salt spray. It is anticipated that anodic film characteristics and corrosion resistance will vary with the anodizing processing conditions.

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