Recycling of Aluminum Salt Cake: Utilization of Evolved Ammonia

2012 ◽  
Vol 44 (1) ◽  
pp. 16-19 ◽  
Author(s):  
Peng Li ◽  
Mei Zhang ◽  
Lidong Teng ◽  
Seshadri Seetharaman
Keyword(s):  
Molecules ◽  
2021 ◽  
Vol 26 (7) ◽  
pp. 2040
Author(s):  
Zsolt Fülöp ◽  
Péter Bana ◽  
István Greiner ◽  
János Éles

A new, continuous-flow consecutive reduction method was developed for the C-N bond formation in the synthesis of the key intermediate of the antipsychotic drug cariprazine. The two-step procedure consists of a DIBAL-H mediated selective ester reduction conducted in a novel, miniature alternating diameter reactor, followed by reductive amination using catalytic hydrogenation on 5% Pt/C. The connection of the optimized modules was accomplished using an at-line extraction to prevent precipitation of the aluminum salt byproducts.


Langmuir ◽  
2003 ◽  
Vol 19 (22) ◽  
pp. 9155-9161 ◽  
Author(s):  
Daniel Angelescu ◽  
Ali Khan ◽  
Horia Caldararu

2007 ◽  
Vol 96 (9) ◽  
pp. 2375-2389 ◽  
Author(s):  
Christina Vessely ◽  
Tia Estey ◽  
Theodore W. Randolph ◽  
Ian Henderson ◽  
Rajiv Nayar ◽  
...  

1978 ◽  
Vol 48 (6) ◽  
pp. 320-324 ◽  
Author(s):  
Russell M.H. Kullman ◽  
Robert M. Reinilardt

JOM ◽  
1996 ◽  
Vol 48 (8) ◽  
pp. 32-37 ◽  
Author(s):  
A. C. Sheth ◽  
K. D. Parks ◽  
S. Parthasarathy
Keyword(s):  

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