Optical and Structural Characterization of Honeycomb-Like Ag2S Nanoparticles by a Simplified and Stable Wet Chemical Synthesis Method

2020 ◽  
Vol 49 (4) ◽  
pp. 2406-2410
Author(s):  
S. G. Ruvalcaba-Manzo ◽  
R. Ramírez-Bon ◽  
J. Tánori ◽  
R. Ochoa-Landin ◽  
S. J. Castillo
Keyword(s):  
Chemical Synthesis ◽  
Structural Characterization ◽  
Synthesis Method ◽  
Wet Chemical Synthesis ◽  
Wet Chemical ◽  
Ag2s Nanoparticles

scholarly journals Canted antiferromagnetism in high-purity NaFeF3 prepared by a novel wet-chemical synthesis method

2020 ◽  
Vol 4 (11) ◽  
Author(s):  
Fabian L. M. Bernal ◽  
Bruno Gonano ◽  
Fredrik Lundvall ◽  
David S. Wragg ◽  
Helmer Fjellvåg ◽  
...  
Keyword(s):  
Chemical Synthesis ◽  
High Purity ◽  
Synthesis Method ◽  
Wet Chemical Synthesis ◽  
Wet Chemical

scholarly journals Facile growth of high transmittance ZnO micro-rod clusters on indium tin oxide by a wet-chemical synthesis method

2021 ◽  
Vol 30 ◽  
pp. 263498332110389
Author(s):  
S Morkoç Karadeniz
Keyword(s):  
Chemical Synthesis ◽  
Tin Oxide ◽  
Indium Tin Oxide ◽  
Hexagonal Phase ◽  
Synthesis Method ◽  
Zinc Nitrate ◽  
Synthesis Process ◽  
Nitrate Hexahydrate ◽  
Wet Chemical Synthesis ◽  
Wet Chemical

A simple wet-chemical synthesis method was developed to fabricate Zinc oxide micro-rod clusters. The synthesis process involved the rapid dilution of a zinc-bearing alkaline solution at 150°C in a convection oven on indium tin oxide (ITO) substrates. The synthesis was carried out by immersing an unseeded ITO substrate in a mixture of zinc nitrate hexahydrate (Zn(NO3)2·6H2O) and hexamethylenetetramine ((CH2)6N4) aqueous solution. The obtained sample was annealed at 400°C for 2 h. The structural, morphological and optical properties of the synthesized ZnO microstructures were investigated by X-ray diffraction, scanning electron microscopy and ultraviolet-visible spectroscopy, respectively. The ZnO rod clusters are hexagonal phase of the wurtzite structure. The crystal grain sizes of the films were found to be 72.6, 84.3 and 66.3 nm for the (100), (002) and (101) crystal planes, respectively. The optical bandgap of the ZnO was determined to be 3.147 eV.

Wet chemical synthesis and characterization of polypodal In2O3 nanoparticles

CrystEngComm ◽  
2013 ◽  
Vol 15 (35) ◽  
pp. 6918 ◽  
Author(s):  
Teyeb Ould-Ely ◽  
Dario Prieto-Centurion ◽  
Irene Rusakova ◽  
Kenton H. Whitmire
Keyword(s):  
Chemical Synthesis ◽  
Synthesis And Characterization ◽  
Wet Chemical Synthesis ◽  
Wet Chemical ◽  
In2o3 Nanoparticles

Wet Chemical Synthesis of La1-xSrxGa0.8Mg0.2O3-δ (x=0.1, 0.2, 0.3) Powders

2010 ◽  
Vol 636-637 ◽  
pp. 908-913 ◽  
Author(s):  
D. Kioupis ◽  
Anna Gaki ◽  
Glykeria Kakali
Keyword(s):  
Citric Acid ◽  
Ethylene Glycol ◽  
Chemical Synthesis ◽  
Single Phase ◽  
Complexing Agents ◽  
Polymeric Precursor ◽  
Wet Chemical Synthesis ◽  
Wet Chemical ◽  
Precursor Route

In the present work a modified polymeric precursor route is applied for the preparation of La1-xSrxGa0.8Mg0.2O3-δ (x=0.1, 0.2, 0.3). Citric acid and ethylene glycol are used as chelating and complexing agents respectively and microwave heating is used for the preparation of the precursors. The sintering reactions are recorded using TG/DTG measurements, while XRD, FTIR and SEM are used for the characterization of the intermediate and final products. As it is concluded, pure La0.9Sr0.1Ga0.8Mg0.2O3 can be prepared after sintering at 1300 °C for 6h. As the doping level of Sr increases, the formation of single phase perovskite is hindered. La0.8Sr0.2Ga0.8Mg0.2O3 contains minor amounts of SrLaGa3O7, while single-phase La0.7Sr0.3Ga0.8Mg0.2O3 can not be prepared at all. In all cases, the intermediate products at lower temperatures are mainly SrLaGa3O7, SrLaGaO4, La4Ga2O7 and La carbonates.

Solubility of Mn in ZnO Nanocrystallites using Wet Chemical Synthesis

2019 ◽  
Vol 2 (1) ◽  
pp. 53-61
Author(s):  
Esau Abekah Armah ◽  
Francis Kofi Ampong ◽  
Martin Egblewogbe ◽  
Hubert Azoda Koffi ◽  
Francis Boakye ◽  
...  
Keyword(s):  
Synthesis Method ◽  
Magnetic Semiconductor ◽  
Solubility Limit ◽  
Secondary Phases ◽  
X Ray Diffraction ◽  
Phase Synthesis ◽  
Wet Chemical Synthesis ◽  
Wet Chemical ◽  
Binary Compounds

There is a substantial amount of literature dealing with many aspects of synthesis and characterization of pure and doped binary compounds including Mn-doped ZnO which has been widely studied due to its superb properties as a dilute magnetic semiconductor (DMS). Aspects concerning doping limits for these compounds is an important stage in the search for new materials. Samples of Zn1-xMnxO nanocrystal were synthesized at temperatures of 180 °C and 200 °C using wet or liquid phase synthesis method. Dopant concentrations x=0.5, 1, 1.5, 2, 2.5, 5, 10, 20, 30, 40 and 50 per cent were studied. Powder x-ray diffraction (PXRD) patterns of the samples were analyzed with a view to determining the onset of secondary phases and hence the solubility limit of the dopant. The solubility limit for Mn in ZnO samples synthesized at temperature of 200 °C is realized at x <20%. For samples synthesized at temperature of 180 °C, the solubility limit is x <0.5%.

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