A novel colloidal deposition method to prepare copper nanoparticles/polystyrene nanocomposite with antibacterial activity and its comparison to the liquid-phase in situ reduction method

Bi nanoparticles on BiOCl nanosheets, synthesized via in situ reduction, enhance the UV light photocatalytic activity and achieve visible light activity.

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Preparation of Hybrid Hydrogel Containing Ag Nanoparticles by a Green in Situ Reduction Method

Langmuir ◽

10.1021/la302011x ◽

2012 ◽

Vol 28 (30) ◽

pp. 11188-11194 ◽

Cited By ~ 41

Author(s):

Bihua Xia ◽

Qianling Cui ◽

Fang He ◽

Lidong Li

Keyword(s):

Ag Nanoparticles ◽

Reduction Method ◽

In Situ Reduction ◽

Hybrid Hydrogel

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Semiconductor/metal nanocomposites formed by in situ reduction method in multilayer thin films

Materials Research Bulletin ◽

10.1016/j.materresbull.2008.04.012 ◽

2009 ◽

Vol 44 (1) ◽

pp. 30-34 ◽

Cited By ~ 1

Author(s):

Yanli Song ◽

Enbo Wang ◽

Chungui Tian ◽

Baodong Mao ◽

Chunlei Wang

Keyword(s):

Thin Films ◽

Reduction Method ◽

Multilayer Thin Films ◽

In Situ Reduction ◽

Metal Nanocomposites

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Preparation of the Gold Nanoparticles and its Activity for Single-Step Amination of Benzene to Aniline

Advanced Materials Research ◽

10.4028/www.scientific.net/amr.661.47 ◽

2013 ◽

Vol 661 ◽

pp. 47-52

Author(s):

Gang Chen ◽

Chun Hua Yang

Keyword(s):

Gold Nanoparticles ◽

Single Step ◽

Xps Analysis ◽

Deposition Method ◽

Reaction Conditions ◽

Catalyst Amount ◽

Mild Conditions ◽

Colloidal Deposition ◽

Alumina Particles

Gold nanoparticles (AuNPs) were attached to the surface of alumina particles by an in-situ immobilizing method. SEM and XPS analysis showed that the coverage of alumina particles by AuNPs increased as the amount of alumina decreased; AuNPs onto alumina particles by the conventional colloidal deposition method were also prepared, whose TEM showed that the coverage of AuNPs was evidently smaller than that in the case of modified colloidal deposition method，although the AuNPs were spread almost uniformly over the surface of alumina particles. Au-immobilized alumina particles were subsequently utilized as the catalysts for direct amination of benzene with NH3H2O as an aminating agent and H2O2 as an oxidant under mild conditions. The reaction conditions were optimized: when catalyst amount was 2.0 g, reaction temperature was 50 °C, NH3H2O amount was 60 mL, H2O2 amount was 30 mL, and reaction time is 2 h, Au-immobilized alumina particles showed the highest aniline yield (1.96 mg) for 25 mL benzene.

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Supercapacitor electrode of nano-Co3O4 decorated with gold nanoparticles via in-situ reduction method

Journal of Power Sources ◽

10.1016/j.jpowsour.2017.07.054 ◽

2017 ◽

Vol 363 ◽

pp. 1-8 ◽

Cited By ~ 67

Author(s):

Yongtao Tan ◽

Ying Liu ◽

Lingbin Kong ◽

Long Kang ◽

Fen Ran

Keyword(s):

Gold Nanoparticles ◽

Reduction Method ◽

In Situ Reduction ◽

Supercapacitor Electrode

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In Situ Compensation Method for Precise Integral SQUID Magnetometry of Miniscule Biological, Chemical, and Pow-der Specimens Requiring the Use of Capsules

10.26434/chemrxiv-2021-s390r-v2 ◽

2022 ◽

Author(s):

Katarzyna Gas ◽

Maciej Sawicki

Keyword(s):

Reduction Method ◽

Experimental Methodology ◽

Sample Holder ◽

Squid Magnetometry ◽

In Situ Reduction ◽

Magnetic Characterization ◽

Data Reduction Method ◽

Alignment Errors

Steadily growing interest in magnetic characterization of organic compounds for therapeutic purposes or of other irregularly shaped specimens calls for refinements of experimental methodology to satisfy experimental challenges. Encapsulation in capsules remains the method of choice, but its applicability in precise magnetometry is limited. This is particularly true for minute specimens in the single milligram range as they are outweighed by the capsules and are subject to large alignment errors. We present here a completely new experimental methodology that permits 30-fold in situ reduction of the signal of capsules by substantially restoring the symmetry of the sample holder that is otherwise broken by the presence of the capsule. In practical terms it means that the standard 30 mg capsule is seen by the magnetometer as approximately a 1 mg object, effectively opening the window for precise magnetometry of single milligram specimens. The method is shown to work down to 1.8 K and in the whole range of the magnetic fields. The method is demonstrated and validated using the reciprocal space option of MPMS-SQUID magnetometers; however, it can be easily incorporated in any magnetometer that can accommodate straw sample holders (i.e., the VSM-SQUID). Importantly, the improved sensitivity is accomplished relying only on the standard accessories and data reduction method provided by the SQUID manufacturer, eliminating the need for elaborate raw data manipulations.

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