Polyurethane foam sampling for the determination of acetochlor in the air of workplace-gas chromatography

2022 ◽  
Author(s):  
Mengyao Chen ◽  
Jian Wu ◽  
Hao Chen ◽  
Zongli Huo ◽  
Xuexue Ding ◽  
...  
Keyword(s):  
Gas Chromatography ◽  
Polyurethane Foam

Determination of dibutyltin compounds in soft polyurethane foam by gas chromatography with flame photometric detection

The Analyst ◽  
1998 ◽  
Vol 123 (5) ◽  
pp. 1091-1094
Author(s):  
Makoto Nagase ◽  
Mineki Toba ◽  
Hiroyuki Kondo ◽  
Kiyoshi Hasebe
Keyword(s):  
Gas Chromatography ◽  
Polyurethane Foam ◽  
Photometric Detection ◽  
Flame Photometric Detection

Determination of Three Kinds of Volatile Residue of Ozone-Depleting Substances in Polyurethane Foam by Gas Chromatography

2011 ◽  
Vol 480-481 ◽  
pp. 609-613
Author(s):  
Hai Feng Chen ◽  
Feng Cao
Keyword(s):  
Gas Chromatography ◽  
Polyurethane Foam ◽  
Matrix Interference ◽  
External Standard Method ◽  
Relative Standard ◽  
Volatile Organic ◽  
External Standard ◽  
The Matrix ◽  
Ozone Depleting Substances

This paper developed a gas chromatography for the determination of volatile residue of ozone-depleting substances (OSD) in polyurethane foam. The sample was detected by gas chromatography - electron capture detector (GC-ECD) under the condition of 120 oC, 5 oC of condensing reflux temperature, 30 min of extraction time and external standard method for quantification. The experimental results of spike recovery showed that: the average recovery of residue of Trichloromonofluoromethane, difluoromonochloroethane and 1, 1, 2 - trifluoro -1, 2, 2 – trichloroethane, the three volatile organic solvent, was 72.7% ~ 116.1%, and the relative standard deviations were less than 5%. This method can effectively overcome the matrix interference, and one introduction of samples can separate and detect three kinds of volatile organic compounds in polyurethane, which has the characteristics of wide linear range and short response time and improves the analytical efficiency.

Sign in / Sign up

Export Citation Format

Share Document