scholarly journals Sand failure: effect of biocide on the geomechanical properties of outcrop carbonate rock under static condition

2020 ◽  
Vol 13 (23) ◽  
Author(s):  
Elizabeth Wuyep ◽  
Gbenga Oluyemi ◽  
Kyari Yates ◽  
Alfred R. Akisanya
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Prediction Models ◽  
Chemical Interaction ◽  
Pore Space ◽  
Uniaxial Compression Test ◽  
X Ray ◽  
Geomechanical Properties ◽  
Chemically Treated

AbstractThe effects of chemical interaction of a biocide with formation rocks on the rock geomechanical properties are examined. A combination of analytical tests (scanning electron microscopy/energy-dispersive X-ray analysis, X-ray powder diffraction and particle size distribution) and uniaxial compression test was used in this study. The particle size distribution in the effluent showed an increase in D50 with poor sorting for the chemically treated outcrop carbonate core samples. The XRPD shows evidence of altered minerals in the chemically treated samples. It was observed that the interaction led to precipitation of new materials that clogged the pore space of the samples leading to up to 150% increase in compressive strength of the carbonate following treatment with the biocide. The results give more insight into the limitations of existing sand production prediction models with respect to the effect of oilfield chemicals on the strength of the reservoir rocks.

X-ray fluorescence spectrometry for rapid screening of particle size in soils

2021 ◽  
Author(s):  
Maame Croffie ◽  
Paul N. Williams ◽  
Owen Fenton ◽  
Anna Fenelon ◽  
Karen Daly
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Soil Texture ◽  
Particle Size Analysis ◽  
Parent Material ◽  
Fluorescence Spectrometry ◽  
Rapid Screening ◽  
Size Analysis ◽  
X Ray

<p>Soil texture is an essential factor for effective land management in agricultural production. Knowledge of soil texture and particle size at field scale can aid with on-going soil management decisions. Standard soil physical and gravimetric methods for particle size analysis are time-consuming and X-ray fluorescence spectrometry (XRF) provides a rapid and cost-effective alternative. The objective of this study was to explore the use of XRF as a predictor for particle size. An extensive archive of Irish soils with particle size and soil texture data was used to select samples for XRF analysis. Regression and correlation analyses on XRF determined results showed that the relationship between Rb and % clay varied with soil type and was dependent on the parent material. There was a strong relationship (R > 0.62, R<sup>2</sup>>0.30, p<0.05) between Rb and clay for soils originating from bedrock such as limestones and slate. Contrastingly, no significant relationship (R<0.03, R<sup>2</sup>=0.00, p>0.05) exists between Rb and % clay for soils originating from granite and gneiss. Furthermore, there was a significant negative correlation (p<0.05) between Rb and % sand. The XRF is a useful technique for rough screening of particle size distribution in soils originating from certain parent materials. Thus, this may contribute to the rapid prediction of soil texture based on knowledge of the particle size distribution.</p><p> </p>

scholarly journals X-Ray Tomography Study on Porosity and Particle Size Distribution in In Situ Al-4.5Cu-5TiB2 Semisolid Rolled Composites

JOM ◽  
2019 ◽  
Vol 71 (11) ◽  
pp. 4050-4058 ◽  
Author(s):  
Swapnil Morankar ◽  
Monalisa Mandal ◽  
Nadia Kourra ◽  
Mark A. Williams ◽  
Rahul Mitra ◽  
...  
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
X Ray

Synthesis of the Mümetal Magnetic Powders by Mechanical Alloying

2011 ◽  
Vol 672 ◽  
pp. 157-160
Author(s):  
Ionel Chicinaş ◽  
Viorel Pop ◽  
Florin Popa ◽  
Virgiliu Călin Prică ◽  
Traian Florin Marinca ◽  
...  
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Mechanical Alloying ◽  
Size Distribution ◽  
Milling Time ◽  
Cast Alloy ◽  
Argon Atmosphere ◽  
X Ray Diffraction ◽  
X Ray ◽  
Rapid Formation

The formation of quaternary 76Ni17Fe5Cu2Cr (wt. %) alloy by mechanical alloying is investigated. The elemental powders of Ni, Fe, Cu and Cr where milled in argon atmosphere in a planetary ball mill for time up to 20 h. Formation of the alloy was checked by X-ray diffraction studies. It is found that the rapid formation of the alloy lead to the rapid establishment of an equilibrium between the welding and fracture process during milling, leading to a constant particle size distribution over a big range of milling time. The morphology of the powders, studied by scanning electron microscopy (SEM) confirms the rapid increase in size. The particle size distribution and the flowability of the powders are also analyzed as a function of milling time. Enhanced magnetization was found for the milled samples, compared to a cast alloy.

Predicting water retention curves of fine texture soils from particle size distribution

2020 ◽  
Author(s):  
Joseph Pollacco ◽  
Jesús Fernández-Gálvez ◽  
Sam Carrick
Keyword(s):  
Particle Size ◽  
Particle Size Distribution ◽  
Size Distribution ◽  
Hydraulic Properties ◽  
Water Retention ◽  
Pore Space ◽  
Water Retention Curve ◽  
Soil Hydraulic Properties ◽  
Retention Curve ◽  
Soil Particles

<p>Indirect methods for estimating soil hydraulic properties from particle size distribution have been developed due to the difficulty in accurately determining soil hydraulic properties, and the fact that particle size distribution is one piece of basic soil physical information normally available. The similarity of the functions describing the cumulative distribution of particle size and pore size in the soil has been the basis for relating particle size distribution and the water retention function in the soil. Empirical and semi-physical models have been proposed, but these are based on strong assumptions that are not always valid. For example, soil particles are normally assumed to be spherical, with constant density regardless of their size; and the soil pore space has been described by an assembly of capillary tubes, or the pore space in the soil matrix is assumed to be arranged in a similar way regardless of particle size. However, in a natural soil the geometry of the pores may vary with the size of the particles, leading to a variable relation between particle radius and pore radius.</p><p> </p><p>The current work is based on the hypothesis that the geometry of the pore size and the void ratio depends on the size of the soil particles, and that a physically based model can be generalised to predict the water retention curve from particle size distribution. The rearrangement of the soil particles is considered by introducing a mixing function that modulates the cumulative particle size distribution, while the total porosity is constrained by the saturated water content.</p><p> </p><p>The model performance is evaluated by comparing the soil water retention curve derived from laboratory measurements with a mean Nash–Sutcliffe model efficiency a value of 0.92 and a standard deviation of 0.08. The model is valid for all soil types, not just those with a marginal clay fraction.</p>

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