Synthesis of deuterium labelled analogues of very long chain fatty acids C22:0, C24:0 and C26:0 for use as internal standards in stable isotope dilution analysis

Author(s):  
H.J. ten Brink ◽  
C. Jakobs ◽  
F. Bickelhaupt
2005 ◽  
Vol 81 (3) ◽  
pp. 692-701 ◽  
Author(s):  
Eduard Cabré ◽  
José M Hernández-Pérez ◽  
Lourdes Fluvià ◽  
Cruz Pastor ◽  
August Corominas ◽  
...  

2009 ◽  
Vol 92 (3) ◽  
pp. 730-733 ◽  
Author(s):  
Thomas Erk ◽  
Hannah Bergmann ◽  
Elke Richling

Abstract Organic acids play an important role in the flavor and taste of plant-derived foods. Quinic acid (QA) is one of the major acids. In the past, several methods like HPLC/UV, GC, and capillary electrophoresis were used for identification and quantification of QA. For the first time, a novel, sensitive, and selective method for the quantification of QA in food using stable isotope dilution analysis with HPLC/MS/MS has been established. Uniformly labeled 13C-QA was used as a standard to reduce sample preparations and to overcome matrix and ionization effects. The method was used to determine the QA content of red wines, instant coffees, and cloudy apple juices. QA contents of instant coffees were 64.4 and 63.6 g/kg powder. The concentrations in red wines were 24.0 and 25.1 mg/L, and 1493.3 and 1705.2 mg/L in cloudy apple juices.


2014 ◽  
Vol 406 (24) ◽  
pp. 5765-5774 ◽  
Author(s):  
Katrin Kittler ◽  
Holger Hoffmann ◽  
Franziska Lindemann ◽  
Matthias Koch ◽  
Sascha Rohn ◽  
...  

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