Neutron diffraction investigation of lattice microstrain in ferrite steel

The distribution of residual stresses was determined in an overlay dissimilar joining pipe weld using neutron diffraction. The specimen was dissimilarly welded between the bcc ferrite steel (SA508) and fcc austenite (SA182) steel with the Ni-based welding consumable (Alloy 182). The weld pipe simulates the nozzle joint component of the nuclear power plants with the dimension of about 130-mm diameter, 500-mm length, and 21-mm thickness. A total of 13 positions were measured from 2 mm to 20 mm underneath the pipe outer wall with 1∼2 mm steps along the weld centerline. The neutron beam gauge volume provides 1-mm spatial resolution along the thickness direction of the weld pipe. The macroscopic ‘stress-free’ lattice spacing (do) was also measured using 2-mm width comb teeth coupons taken from the identical location of the bulk weld neutron-diffraction measurements. The result shows that the hoop stress component developed tension of about 100 MPa and compression of −600 MPa near the outer and inner wall surface of the overlay pipe weld, respectively.

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Texture measurements in Al2O3 using BEKP

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100170773 ◽

1994 ◽

Vol 52 ◽

pp. 608-609

Author(s):

M. D. Vaudin ◽

J. P. Cline

Keyword(s):

Neutron Diffraction ◽

Rapid Method ◽

Crystallographic Orientation ◽

Specimen Surface ◽

X Ray Diffraction ◽

Anisotropic Crystal ◽

X Ray ◽

Verification Method ◽

Crystal Properties ◽

Backscattered Electron

The study of preferred crystallographic orientation (texture) in ceramics is assuming greater importance as their anisotropic crystal properties are being used to advantage in an increasing number of applications. The quantification of texture by a reliable and rapid method is required. Analysis of backscattered electron Kikuchi patterns (BEKPs) can be used to provide the crystallographic orientation of as many grains as time and resources allow. The technique is relatively slow, particularly for noncubic materials, but the data are more accurate than any comparable technique when a sufficient number of grains are analyzed. Thus, BEKP is well-suited as a verification method for data obtained in faster ways, such as x-ray or neutron diffraction. We have compared texture data obtained using BEKP, x-ray diffraction and neutron diffraction. Alumina specimens displaying differing levels of axisymmetric (0001) texture normal to the specimen surface were investigated.BEKP patterns were obtained from about a hundred grains selected at random in each specimen.

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A study of oxygen and vacancy ordering in YBa2Cu3O7−x

Proceedings, annual meeting, Electron Microscopy Society of America ◽

10.1017/s0424820100152793 ◽

1989 ◽

Vol 47 ◽

pp. 164-165

Author(s):

Y. P. Lin ◽

A. H. O’Reilly ◽

J. E. Greedan ◽

M. Post

Keyword(s):

Electron Microscopy ◽

Neutron Diffraction ◽

Oxygen Content ◽

Carbon Film ◽

Nitrogen Atmosphere ◽

Vacancy Ordering ◽

Powder Samples ◽

Vacancy Chains ◽

Chain Ordering

In the basal planes of the orthorhombic YBa2Cu3O7-X compound with x=0.07, which has a Tc of around 90K, chains of copper-oxygen are formed along the [010] direction. Previous investigations on the variation of Tc with oxygen content have shown the existence of a plateau at Tc = 60K for x=0.3 to 0.4, suggesting the presence of a separate phase. This phase has also been identified to be orthorhombic, but with a 2x superlattice along [100] of the parent structure, and the superlattice has been attributed to the formation of alternating copper-oxygen and copper-vacancy chains. In our work, we have studied the chain ordering phenomenon by electron microscopy and neutron diffraction on samples with different oxygen contents. We report here some of our electron microscopy findings for samples with x=0.4.Powder samples of YBa2Cu3O7-X were prepared by controlled re-oxidation of previously reduced material. For electron microscopy, the sample was dry ground using a mortar and pestle in a dry nitrogen atmosphere without the use of any solvent and transferred dry onto holey carbon film for examination in a Philips CM12 microscope.

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