High-Resolution Strain/Stress Measurements by Three-Axis Neutron Diffractometer

Resolution properties of the unconventional high-resolution neutron diffraction three-axis setup for strain/stress measurements of large bulk polycrystalline samples are presented. Contrary to the conventional two-axis setups, in this case, the strain measurement on a sample situated on the second axis is carried out by rocking the bent perfect crystal (BPC) analyzer situated on the third axis of the diffractometer. Thus, the so-called rocking curve provides the sample diffraction profile. The neutron signal coming from the analyzer is registered by a point detector. This new setup provides a considerably higher resolution (at least by a factor of 5), which however, requires a much longer measurement time. The high-resolution neutron diffraction setting can be effectively used, namely, for bulk gauge volumes up to several cubic centimeters, and for plastic deformation studies on the basis of the analysis of diffraction line profiles, thus providing average values of microstructure characteristics over the irradiated gauge volume.

Residual Stress Distribution in Water Jet Peened Type 304 Stainless Steel

In materials with a surface treatment such as shot peening, the residual stress gradient in the surface layer is severe. When measuring the residual stress distribution near the surface with a severe stress gradient by the neutron diffraction method, the gauge volume must be removed from the measurement sample. However, when the gauge volume deviates from the sample, a pseudo peak shift occurs and accurate stress distribution cannot be evaluated. Therefore, it is necessary to evaluate the pseudo peak shift in advance under the same conditions, as in the case of actual residual stress measurement, using a sample in an unstressed state. In this study, the stress distributions in the surface layer of a type 304 stainless steel plate and bar with simulated stress-corrosion cracks which were subjected to water jet peening—giving a surface layer residual stress equivalent better than that of normal shot peening—were evaluated considering the pseudo peak shift. As a result, the residual stress distributions in the surface layer were measured in good agreement with the measurement result obtained by the sequential polishing X-ray diffraction method. It was clarified that the residual stress distribution in the near surface with steep stress gradient can be evaluated by the neutron diffraction method.

Minimizing and Characterizing Uncertainties in Neutron Strain Measurements with Special Attention to Grain Size Effects

The accurate determination of strain during measurement using neutron diffraction depends on many factors. The statistical uncertainty of the diffraction data is not always the most important contributor to the total uncertainty in the measured strain. Other contributors, such as sample positioning, size and shape of the sampling (gauge) volume and the size and distribution of grains within the sampling volume, often play an important role as well. Grain size issues have been the least studied and their impact is often ignored even though the potential uncertainty contribution can be large. Certain methods such as oscillating the sample during measurement can help in reducing the magnitude of the grain size effect and hence also that of the related uncertainty contribution. A thorough characterization of uncertainties due to grain size effects however, in terms of absolute values that should be added to the statistical peak fitting uncertainties has not yet been implemented. This paper will present an improved method to characterize and estimate absolute uncertainty values due to grain size effects.

Texture Characterization of Stainless Steel Cladded Layers of Process Vessels

In this study local texture of process vessels made of carbon steel cladded by protective layers of stainless steel by submerged arc welding (SAW) were investigated by neutron diffraction using the diffractometer STRESSSPEC at FRM 2 (Garching, Germany). Different samples were prepared: as welded and as welded plus relevant industrial heat treatment. Local texture measurements with a gauge volume of 3 x 3 x 2 mm3 of the three cladding layers (at depths of 2 mm, 5 mm and 7.5 mm) for each sample were determined. Texture results indicated that there exists an annealed cube component in all the studied samples. Based on the measured pole figures at each depth and sample, the calculated orientation distribution functions data were used to calculate the Young's modulus with respect to the main welding directions. The calculated local and bulk anisotropic Young’s modulus in depth is presented and discussed.

Fabrication and testing of a newly designed slit system for depth-resolved X-ray diffraction measurements

A new system of slits called `spiderweb slits' have been developed for depth-resolved powder or polycrystalline X-ray diffraction measurements. The slits act on diffracted X-rays to select a particular gauge volume of sample, while absorbing diffracted X-rays from outside of this volume. Although the slit geometry is to some extent similar to that of previously developed conical slits or spiral slits, this new design has advantages over the previous ones in use for complex heterogeneous materials andin situandoperandodiffraction measurements. For example, the slits can measure a majority of any diffraction cone for any polycrystalline material, over a continuous range of diffraction angles, and work for X-ray energies of tens to hundreds of kiloelectronvolts. The design is generated and optimized using ray-tracing simulations, and fabricated through laser micromachining. The first prototype was successfully tested at the X17A beamline at the National Synchrotron Light Source, and shows similar performance to simulations, demonstrating gauge volume selection for standard powders, for all diffraction peaks over angles of 2–10°. A similar, but improved, design will be implemented at the X-ray Powder Diffraction beamline at the National Synchrotron Light Source II.

Diffraction analysis of strongly inhomogeneous residual stress depth distributions by modification of the stress scanning method. I. Theoretical concept

Exploiting the advantages of energy-dispersive synchrotron diffraction, a method for the determination of strongly inhomogeneous residual stress depth gradients is developed, which is an enhancement of the stress scanning technique. For this purpose, simulations on the basis of a very steep residual stress depth profile are performed, and it is shown that conventional real space evaluation approaches fail, because they do not take into account the variation of the residual stresses within the gauge volume. Therefore, a concept facilitating the deconvolution of the diffraction signal by considering the effect of the gauge volume geometry as well as the influence of the material absorption on the average information depth is proposed. It is demonstrated that data evaluation requires a three-dimensional least-squares fit procedure in this case. Furthermore, possible aberrations and their impact on the analysis of the residual stresses by applying the `modified stress scanning' method are treated theoretically.

Determination and mitigation of the uncertainty of neutron diffraction measurements of residual strain in large-grained polycrystalline material

For large-grained samples it is advantageous to perform pairs of neutron diffraction measurements at the same spatial location but rotated 180° around the geometric centre of the gauge volume as a means of minimizing the scatter coming from the random positioning of grains within the gauge volume.

Residual Stress Measurement in an Ultrasonic Peened Specimen

Plastic deformation from peening induces a compressive residual stress on the treated surface which provides resistance to metal fatigue. Hence, peening is often used to extend the fatigue lives of welded components by reducing the effective tensile residual stress. This paper describes the influence of ultrasonic peening on the residual stress. For this study a four point plastically bent beam specimen, similar to the reeling process, was used. The specimen was made from 50D steel a material often used in offshore structural components. The residual stresses in the specimen were measured before ultrasonic peening with 5 different measurement techniques. After the ultrasonic peening treatment the residual stress was measured using the Incremental centre hole drilling and the ring core techniques. Measurements were carried within the homogeneously bent section location as well as outside. In order to see the variation of the results influenced by the gauge volume, strain gauges of three different sizes were used to provide results within 0.5mm, 1mm and 2mm depth. The measurements show that the ultrasonic peening surface treatment carried out induced high compressive residual stresses up to 2mm deep inside the specimen. Finally a compendium of residual stress profiles using different peening processes and materials is presented and discussed.

Improving Beamtime Efficiency for Residual Stress Neutron Experiments

Starting during the shut-down of the HZB research reactor BER-II in 2011/2012 the E3 residual stress and texture diffractometer in Berlin underwent a comprehensive upgrade. The investments were broken down into different criteria, such as enhancing the instrument performance and accuracy as well as extending the range of applications for the user community. Here, we report about the gains achieved after integrating and commissioning the individual hardware and software tools included in the upgrade project, namely a motorized primary slit to accurately adjust the gauge volume, a secondary optics radial collimator and a laser scanner to precisely and quickly align the sample. The integration of the presented devices is further supported by software developments to shorten the instrument alignment procedure and measurement time. The upgrade has improved the efficiency of the available neutron beamtime.