Recent advances in mass spectrometry analysis of low molecular weight heparins

2018 ◽  
Vol 29 (1) ◽  
pp. 11-18 ◽  
Author(s):  
Zhangjie Wang ◽  
Lianli Chi
Keyword(s):  
Mass Spectrometry ◽  
Molecular Weight ◽  
Mass Spectrometry Analysis ◽  
Low Molecular Weight ◽  
Low Molecular Weight Heparins ◽  
Spectrometry Analysis ◽  
Recent Advances

Advances in structure elucidation of low molecular weight carbohydrates by liquid chromatography-multiple-stage mass spectrometry analysis

2020 ◽  
Vol 1612 ◽  
pp. 460664 ◽  
Author(s):  
A. Martín-Ortiz ◽  
C. Carrero-Carralero ◽  
O. Hernández-Hernández ◽  
R. Lebrón-Aguilar ◽  
F.J. Moreno ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Molecular Weight ◽  
Liquid Chromatography ◽  
Structure Elucidation ◽  
Mass Spectrometry Analysis ◽  
Low Molecular Weight ◽  
Spectrometry Analysis

scholarly journals Synthesis of a Low-Molecular-Weight Form of Exopolysaccharide by Bradyrhizobium japonicum USDA 110

2001 ◽  
Vol 67 (2) ◽  
pp. 1011-1014 ◽  
Author(s):  
Heather A. Louch ◽  
Karen J. Miller
Keyword(s):  
Molecular Weight ◽  
Bradyrhizobium Japonicum ◽  
Compositional Analysis ◽  
Mass Spectrometry Analysis ◽  
Low Molecular Weight ◽  
Nuclear Magnetic Resonance Analysis ◽  
Spectrometry Analysis ◽  
Resonance Analysis ◽  
Dimeric Form ◽  
Molecular Weight Form

ABSTRACT A novel extracellular low-molecular-weight polysaccharide was detected as a contaminant within extracellular cyclic β-1,6-β-1,3-glucan preparations from Bradyrhizobium japonicum USDA 110 cultures. Compositional analysis, methylation analysis, and nuclear magnetic resonance analysis revealed that this low-molecular-weight polysaccharide was composed of the same pentasaccharide repeating unit previously described for the high-molecular-weight form of the exopolysaccharide (EPS) synthesized by B. japonicum strains. Mass spectrometry analysis indicated that the size of this low-molecular-weight form of EPS was consistent with a dimeric form of the pentasaccharide repeating unit.

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