Experimental investigations of the structural transformations induced by the heat treatment in manganese ferrite synthesized by ultrasonic assisted co-precipitation method

2016 ◽  
Vol 42 (15) ◽  
pp. 16744-16748 ◽  
Author(s):  
I. Malaescu ◽  
A. Lungu ◽  
C.N. Marin ◽  
P. Vlazan ◽  
P. Sfirloaga ◽  
...  
RSC Advances ◽  
2016 ◽  
Vol 6 (54) ◽  
pp. 49228-49235 ◽  
Author(s):  
Chengwei Gao ◽  
Baojun Li ◽  
Ning Chen ◽  
Jie Ding ◽  
Qiang Cai ◽  
...  

Fe3O4/HNT@rGO composite (FHGC) was fabricated via a facile co-precipitation process, followed by heat treatment. For RhB and As5+removal, the high performance and easy separation of FHGC highlight its potential application in water treatment.


2017 ◽  
Vol 46 (5) ◽  
pp. 356-361 ◽  
Author(s):  
Liliya Frolova ◽  
Alexander Pivovarov ◽  
Tatyana Butyrina

Purpose The purpose of this work is to study the patterns of pigment colour formation and to develop metal compositions for obtaining spinels using the precipitation and heat treatment methods. Design/methodology/approach Precursor materials were prepared using co-precipitation method. Phase composition of pigments were determined by X-ray diffraction. Colour of pigments was determined spectrophotometry. Modelling of colour formation was performed using simplex method. Planning in the future to carry out full synthesis of pigments of blue, red and yellow colours. Findings The paper deals with the results of theoretical and experimental research on the synthesis pigments of blue, red and yellow colours based on Fe-Co-Al-O spinel. The influence of the chromophore cation content and the heat treatment temperature on optical and colour characteristics of pigments were studied. Originality/value The resulting composition-property diagrams make it possible to evaluate the effect of chromophore cations and heat treatment on the colour formation for Fe2O3-Al2O3-CoO system. Crystal-phase composition of the pigments is installed and its relationship with the optical colour characteristics. That makes it possible carry out targeted synthesis of pigments blue, red and yellow colours in further. The phase composition of pigments and its relationship with optical and colour properties has been established thus enabling the directed synthesis of blue, red and yellow pigments.


2012 ◽  
Vol 620 ◽  
pp. 7-11
Author(s):  
Abdollah Javidan ◽  
Mir Hassan Hosseini ◽  
S.L. Shaifi

Nanoparticles of Cobalt-zinc ferrite (Co0.5Zn0.5Fe2O4) and Cobalt-manganese ferrite (Co0.5Mn0.5Fe2O4) have been synthesized at room temperature by co-precipitation method with and without calcination process. Starting materials for preparation of nanooxides were Co (NO3)2.6H2O, ZnCl2, Fe (NO3)3.9H2O and Mn (NO3)2.4H2O. These salats were mixed in stoichiometric amounts and precipitated with sodium hydroxide. Synthesised materials are confirmed by XRD and SEM analysis. The FTIR spectra of nanooxides have been analyzed in the frequency range of 400-4000cm-1.


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