A Novel method of synthesis of high purity nano plated boron carbide powder by a solid-state reaction of poly (vinyl alcohol) and boric acid

2017 ◽  
Vol 43 (13) ◽  
pp. 10554-10558 ◽  
Author(s):  
Nazar Shawgi ◽  
SanXi Li ◽  
Song Wang
Keyword(s):  
Solid State ◽  
Boron Carbide ◽  
Boric Acid ◽  
High Purity ◽  
Solid State Reaction ◽  
Vinyl Alcohol ◽  
Poly Vinyl Alcohol ◽  
Carbide Powder ◽  
Novel Method

Synthesis of nano particles and fiber-like shape boron carbide powder from ploy (vinyl alcohol) and boric acid

2017 ◽  
Vol 82 (2) ◽  
pp. 450-457 ◽  
Author(s):  
Nazar Shawgi ◽  
San Xi Li ◽  
Song Wang ◽  
Zan Wang ◽  
Ya Nan Nie
Keyword(s):  
Boron Carbide ◽  
Boric Acid ◽  
Vinyl Alcohol ◽  
Nano Particles ◽  
Carbide Powder

Preparation of High-Purity Ultrafine α-Al2O3 by Solid-State Reaction at Room Temperature

2008 ◽  
Vol 368-372 ◽  
pp. 683-685
Author(s):  
Cheng Wei Hao ◽  
Bo Lin Wu ◽  
Ji Yan Li
Keyword(s):  
Solid State ◽  
High Purity ◽  
Solid State Reaction ◽  
Room Temperature ◽  
Raw Materials ◽  
Phase Particle ◽  
Phase Transformation Temperature ◽  
Particle Size And Morphology ◽  
Size And Morphology ◽  
Α Al2o3

Ammonium aluminium carbonate hydroxide (AACH), with a small quantity of γ-AlOOH, was synthesized through solid-state reaction at room temperature using AlCl3·6H2O and NH4HCO3 as raw materials and polyethylene glycol (PEG-10000) as the dispersant. After calcined at 1100°C for 1.5h, α-Al2O3 powders with primary particle sizes of 20~30nm were obtained. The crystal phase, particle size and morphology of the high-purity ultrafine α-Al2O3 were characterized. The results showed that a small quantity of γ-AlOOH in the AACH decomposed and formed crystal seeds. The presence of crystal seeds reduced the nucleation activation energy and therefore reduced the phase transformation temperature.

Synthesis of high-purity Li8ZrO6 powder by solid state reaction under hydrogen atmosphere

2016 ◽  
Vol 109-111 ◽  
pp. 1739-1743 ◽  
Author(s):  
Kiyoto Shin-mura ◽  
Yu Otani ◽  
Seiya Ogawa ◽  
Eiki Niwa ◽  
Takuya Hashimoto ◽  
...  
Keyword(s):  
Solid State ◽  
High Purity ◽  
Solid State Reaction ◽  
Hydrogen Atmosphere

Structural study of poly(vinyl alcohol) in the gel state by high-resolution solid-state 13C NMR spectroscopy

1995 ◽  
Vol 28 (19) ◽  
pp. 6677-6679 ◽  
Author(s):  
Masatoshi Kobayashi ◽  
Isao Ando ◽  
Takahiro Ishii ◽  
Shigetoshi Amiya
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
High Resolution ◽  
Structural Study ◽  
13C Nmr ◽  
Vinyl Alcohol ◽  
13C Nmr Spectroscopy ◽  
Poly Vinyl Alcohol ◽  
Solid State 13C Nmr
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