Towards a large-scale production of boron carbide nano particles from poly (vinyl alcohol) and boric acid by a solid-state reaction-pyrolysis process (SRPP)

2018 ◽  
Vol 44 (1) ◽  
pp. 774-778 ◽  
Author(s):  
Nazar Shawgi ◽  
SanXi Li ◽  
Song Wang ◽  
Yang Li ◽  
Rania Ramzi
Nanoscale ◽  
2014 ◽  
Vol 6 (17) ◽  
pp. 10216-10223 ◽  
Author(s):  
Huaqiao Tan ◽  
Zhao Zhao ◽  
Mang Niu ◽  
Chengyu Mao ◽  
Dapeng Cao ◽  
...  

A simple and facile solid-state chemical reduction approach for a large-scale production of colored TiO2 with good photocatalytic properties was developed.


Materials ◽  
2018 ◽  
Vol 11 (9) ◽  
pp. 1699 ◽  
Author(s):  
Cheng Peng ◽  
Yefeng Feng ◽  
Jianbing Hu

Promising comprehensive properties, including high permittivity, low dielectric loss, high breakdown strength, low electrical conductivity, and high thermal conductivity, are very hard to simultaneously obtain in high-frequency applicable polymer nanocomposite dielectrics. Instead of traditional electric percolation, in this work, a novel route based on a synergy between electric percolation and induced polarization has been raised to prepare 0–3 type nanocomposites with an enhanced high permittivity (high-k) property and low loss at high frequency. This work aimed at optimizing that synergy to achieve the favorable properties mentioned above in composite dielectrics used at high frequencies such as 1 MHz and 1 GHz. Conductive beta-SiC nanoparticles with a particle size of ~30 nm were employed as filler and both insulating poly(vinyl alcohol) and polyvinyl chloride were employed as polymer matrices to construct two composite systems. Utilizing polyvinyl chloride rather than poly(vinyl alcohol) realizes higher comprehensive electrical properties in composites, ascribed to optimization of that synergy. The optimization was achieved based on a combination of mild induced polarization and polarization-assisted electric percolation. Therefore, this work might open the way for large-scale production of high-frequency applicable composite dielectrics with competitive comprehensive electrical properties.


2019 ◽  
Vol 7 (40) ◽  
pp. 22958-22966 ◽  
Author(s):  
Shenghui Shen ◽  
Shengzhao Zhang ◽  
Shengjue Deng ◽  
Guoxiang Pan ◽  
Yadong Wang ◽  
...  

Herein, we firstly proposed multidimensional titanium niobium oxides (1D/2D/3D-TNO) via a versatile bioinspired template method, which employed as high-performance anodes for both liquid and solid state lithium ion batteries


2021 ◽  
Vol 8 ◽  
Author(s):  
Yanhui Yao ◽  
Hongya Li ◽  
Jia Li ◽  
Baocheng Zhu ◽  
Tongguo Gao

The study evaluated the impact of fermentation with Bacillus sp. on the nutritional quality of soybean meal (SBM) and the changes of bacterial community structure during fermentation. High protease-producing strains were screened to degrade SBM macromolecular protein and anti-nutritional factors (ANFs). Unsterilized SBM then underwent an anaerobic solid-state fermentation method to evaluate the effects of fermentation. Results showed that for the nine high-producing protease strains that were screened, acid-soluble protein (ASP) contents in fermented SBM increased, with the highest value found to be 13.48%, which was fermented using strain N-11. N-11 was identified as Bacillus subtilis. N-11 fermentation reduced ANFs such as glycinin and β-conglycinin by 82.38 and 88.32%, respectively. During N-11 fermentation, the bacterial richness and diversity in SBM increased but not significantly. The high-yield protease strain B. subtilis N-11 selected in this experiment improved the nutritional quality of SBM through fermentation, and it can be used for industrial large-scale production.


2021 ◽  
Author(s):  
M. K. Ravindra ◽  
Giriyapura Prabhukumara Darshan ◽  
D. R. Lavanya ◽  
K. M. Mahadevan ◽  
H. B. Premkumar ◽  
...  

Abstract Aggregation-induced emission based organic heterocyclic luminogens bearing conjugated electronic structure have paid much attention due to its excellent fluorescence in aggregation state. In this communication, novel conjugated blue light emitting imidazole molecule is synthesized by one pot multicomponent reaction route is reported for the first time. The prepared molecule exhibits a strong fluorescence in aggregation state have gain much attention owing to their unique properties, namely simple synthesis, high purity, inexpensive, eco-friendly, large scale production, high photostability, etc. By considering these advantages of the prepared luminogen, a new fluorescence based platform has been setup for in-situ visualization of latent fingerprints and its preservation by spray method followed by Poly(vinyl alcohol) masking. A clear and well defined fluorescence fingerprint images on variety of surfaces by revealing level 1–3 ridge characteristics upon ultraviolet 365 nm light are noticed. The dual nature of binding specificity as well as excellent fluorescence properties permits the visualization of latent fingerprints for longer durations (up to 365 days) with superior contrast, sensitivity, efficiency, selectivity and negligible background hindrance. We further fabricated unclonable invisible security ink and make it highly suitable for various printing modes on valuable goods for protection against forging. The developed labels are displaying uniform distribution of ink and exceptional stability under various atmospheric environments. The development of long preservative forensic information as well as invisible ink opens new avenue in advanced forensic and data security applications.


2011 ◽  
Vol 15 (1) ◽  
pp. 5-10
Author(s):  
Jie Xu ◽  
Chunju Lv ◽  
Guanglei Tian

Spinel lithium titanate (Li4Ti5O12) materials were synthesized by a hydrolysis precipitation-assisted solid-state method in the temperature range from 600 to 900℃ for large-scale production. DSC/TGA, XRD and SEM were used to characterize the as-prepared samples. The optimum synthesis condition was examined in relation to the charge–discharge performance. It was found that when the dry hydrolysis precipitation precursor with 8% Li excess was calcined at 700–800℃ for 12 h in air, a pure Li4Ti5O12 phase was obtained. The as-obtained material has the best electrochemical performance due to its narrow size distribution and precise stoichiometry of the oxide.


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