In-situ measurement of mechanical properties and dimensional changes of preceramic thermosets during their pyrolysis conversion to ceramics using thermomechanical analysis

Author(s):  
Martin Černý ◽  
Zdeněk Chlup ◽  
Adam Strachota ◽  
Jiří Brus ◽  
Jana Schweigstillová ◽  
...  
2021 ◽  
Author(s):  
Meng Meng ◽  
Luke Frash ◽  
James Carey ◽  
Wenfeng Li ◽  
Nathan Welch ◽  
...  

Abstract Accurate characterization of oilwell cement mechanical properties is a prerequisite for maintaining long-term wellbore integrity. The drawback of the most widely used technique is unable to measure the mechanical property under in situ curing environment. We developed a high pressure and high temperature vessel that can hydrate cement under downhole conditions and directly measure its elastic modulus and Poisson's ratio at any interested time point without cooling or depressurization. The equipment has been validated by using water and a reasonable bulk modulus of 2.37 GPa was captured. Neat Class G cement was hydrated in this equipment for seven days under axial stress of 40 MPa, and an in situ measurement in the elastic range shows elastic modulus of 37.3 GPa and Poisson's ratio of 0.15. After that, the specimen was taken out from the vessel, and setted up in the triaxial compression platform. Under a similar confining pressure condition, elastic modulus was 23.6 GPa and Possion's ratio was 0.26. We also measured the properties of cement with the same batch of the slurry but cured under ambient conditions. The elastic modulus was 1.63 GPa, and Poisson's ratio was 0.085. Therefore, we found that the curing condition is significant to cement mechanical property, and the traditional cooling or depressurization method could provide mechanical properties that were quite different (50% difference) from the in situ measurement.


2021 ◽  
Author(s):  
Pascal Bertsch ◽  
Danai Etter ◽  
Peter Fischer

Kombucha is a traditional beverage obtained by the fermentation of sugared tea by a symbiotic culture of bacteria and yeast which has recently re-emerged as a popular lifestyle product with...


1987 ◽  
Vol 58 (7) ◽  
pp. 1284-1286
Author(s):  
Katsumi Tanimura ◽  
Noriaki Itoh ◽  
Kazuaki Arima ◽  
Hiroshi Imaike ◽  
Dale W. Heikkinen

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