Application of comprehensive two-dimensional gas chromatography–time-of-flight mass spectrometry in the analysis of volatile oil of traditional Chinese medicines

2004 ◽  
Vol 1034 (1-2) ◽  
pp. 199-205 ◽  
Author(s):  
Jianfang Wu ◽  
Xin Lu ◽  
Wanying Tang ◽  
Hongwei Kong ◽  
Shenfan Zhou ◽  
...  
2013 ◽  
Vol 2013 ◽  
pp. 1-11 ◽  
Author(s):  
Kunming Qin ◽  
Lijuan Zheng ◽  
Hao Cai ◽  
Gang Cao ◽  
Yajing Lou ◽  
...  

Pericarpium Citri Reticulatae (Chenpi in Chinese) has been widely used as an herbal medicine in Korea, China, and Japan. Chenpi extracts are used to treat indigestion and inflammatory syndromes of the respiratory tract such as bronchitis and asthma. This thesis will analyze chemical compositions of Chenpi volatile oil, which was performed by comprehensive two-dimensional gas chromatography with high-resolution time-of-flight mass spectrometry (GC × GC-HR-TOFMS). One hundred and sixty-seven components were tentatively identified, and terpene compounds are the main components of Chenpi volatile oil, a significant larger number than in previous studies. The majority of the eluted compounds, which were identified, were well separated as a result of high-resolution capability of the GC × GC method, which significantly reduces, the coelution.β-Elemene is tentatively qualified by means of GC × GC in tandem with high-resolution TOFMS detection, which plays an important role in enhancing the effects of many anticancer drugs and in reducing the side effects of chemotherapy. This study suggests that GC × GC-HR-TOFMS is suitable for routine characterization of chemical composition of volatile oil in herbal medicines.


2012 ◽  
Vol 1255 ◽  
pp. 202-206 ◽  
Author(s):  
Sonja Stadler ◽  
Pierre-Hugues Stefanuto ◽  
Jonathan D. Byer ◽  
Michał Brokl ◽  
Shari Forbes ◽  
...  

2007 ◽  
Vol 21 (1) ◽  
pp. 286-294 ◽  
Author(s):  
Jacqui F. Hamilton ◽  
Alistair. C. Lewis ◽  
Marcos Millan ◽  
Keith D. Bartle ◽  
Alan A. Herod ◽  
...  

Química Nova ◽  
2012 ◽  
Vol 35 (5) ◽  
pp. 982-987 ◽  
Author(s):  
Samantha S. Barbosa ◽  
Felipe D. Leal ◽  
Monica C. Padilha ◽  
Raphael S. F. Silva ◽  
Henrique Marcelo G. Pereira ◽  
...  

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