Effect of hydration on the long-range order of lipid multilayers investigated by in situ time-resolved energy dispersive X-ray diffraction

By using chemical transport reactions with various transporting agents (HgCl2, NbCl5, Nb3O7Cl) a slightly substoiehiometric NbO2-phase, β-NbO2, was obtained from samples with O/Nb ∼ 1.5 (source; T > 1373 K) and with deposition temperatures > 1273 K (sink). The rango of composition of β-NbO2 was found to exist from NbO1.990 to NbO1.998.The structure of the tetragonal, column-shaped black crystals was determined by X-ray diffraction. It crystallizes tetragonally in the space group I41 with lattice constants a = 9.693(3) Å, c = 5.985(1) Å and Z = 10 formula units.The crystal structure of β-NbO2 is shown to be a deformed rutile type. As in α-NbO2 the Nb-atoms are grouped in pairs. However, both oxides are different with respect to their long-range order.

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Anomalous x-ray diffraction measurements of long-range order in (001)-texturedL10FePtCu thin films

Physical Review B ◽

10.1103/physrevb.86.024204 ◽

2012 ◽

Vol 86 (2) ◽

Cited By ~ 26

Author(s):

M. Maret ◽

C. Brombacher ◽

P. Matthes ◽

D. Makarov ◽

N. Boudet ◽

...

Keyword(s):

Thin Films ◽

Long Range ◽

Range Order ◽

Long Range Order ◽

X Ray Diffraction ◽

X Ray

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A furnace for the in situ study of the formation of inorganic solids at high temperature using time-resolved energy-dispersive x-ray diffraction

Review of Scientific Instruments ◽

10.1063/1.1315355 ◽

2000 ◽

Vol 71 (11) ◽

pp. 4177 ◽

Cited By ~ 9

Author(s):

Margret J. Geselbracht ◽

Richard I. Walton ◽

E. Sarah Cowell ◽

Franck Millange ◽

Dermot O’Hare

Keyword(s):

High Temperature ◽

Energy Dispersive ◽

X Ray Diffraction ◽

Time Resolved ◽

X Ray ◽

Inorganic Solids ◽

In Situ Study

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High-Resolution Small-Angle X-Ray Diffraction Study of Long-Range Order in Hard-Sphere Colloidal Crystals

Physical Review Letters ◽

10.1103/physrevlett.88.208301 ◽

2002 ◽

Vol 88 (20) ◽

Cited By ~ 45

Author(s):

A. V. Petukhov ◽

D. G. A. L. Aarts ◽

I. P. Dolbnya ◽

E. H. A. de Hoog ◽

K. Kassapidou ◽

...

Keyword(s):

High Resolution ◽

Diffraction Study ◽

Long Range ◽

Small Angle ◽

Hard Sphere ◽

Colloidal Crystals ◽

Range Order ◽

Long Range Order ◽

X Ray Diffraction ◽

X Ray

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Characterization of Interfacial Structure of InGaAs/InP Short Period Superlattices by Raman Scattering and High Resolution X-Ray Diffraction

MRS Proceedings ◽

10.1557/proc-324-285 ◽

1993 ◽

Vol 324 ◽

Cited By ~ 1

Author(s):

Teruo Mozume

Keyword(s):

Raman Scattering ◽

Long Range ◽

Range Order ◽

Interfacial Structure ◽

Long Range Order ◽

X Ray Diffraction ◽

X Ray ◽

Gas Source ◽

Short Period ◽

Short Period Superlattices

AbstractThe x-ray diffraction (XRD) of InGaAs/InP short-period superlattices (SPSL's) grown on (001)InP substrates by gas source molecular beam epitaxy (GSMBE) and by gas source migration enhanced epitaxy (GSMEE) shows that the GSMBE grown SPSL is strain free, and that GSMEE grown SPSL's with InGa-P and In-As heterointerfaces have strain-induced zerothorder satellite peak shift consistent with that in simulation results for the InGaAs/InP SPSL with one monolayer of InGaP and InAs inserted in each interface. Partial destruction of the long-range order is confirmed by the observation of the extra diffraction peak in GSMBE grown SPSL and by weak intensity of satellite peaks and nonuniform spacing between satellite peaks in GSMEE grown SPSL's. Raman scattering shows that the strain is accommodated in the interface layer in GSMEE grown samples. A confinement model without interface disorder fits the GaAs LO phonon very well. These results indicate that the local atomic arrangements are tailored by GSMEE, but that long range-order is impaired by the misfit dislocations in GSMEE grown SPSL's and by the exchange between As to P at the interfaces in GSMBE grown SPSL.

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Comparison of temperature driven ordering in bulk foil and thin film of L10ordered FePd

MRS Proceedings ◽

10.1557/proc-842-s3.10 ◽

2004 ◽

Vol 842 ◽

Author(s):

Chaisak Issro ◽

Wolfgang Püschl ◽

Wolfgang Pfeiler ◽

Bogdan Sepiol ◽

Peter F. Rogl ◽

...

Keyword(s):

Thin Film ◽

Electrical Resistivity ◽

Long Range ◽

Molecular Beam ◽

Resistivity Measurement ◽

Range Order ◽

Electrical Resistivity Measurement ◽

Long Range Order ◽

X Ray Diffraction ◽

X Ray

ABSTRACTChanges in the degree of long-range order of 10 μm thick FePd foil are presented and compared with results on 50 nm thick FePd films. The films were produced by dc and rf magnetron co-sputtering on Si as well as by molecular beam epitaxy co-deposition on MgO substrates. Long-range order was studied by electrical resistivity measurement, X-ray diffraction and Möβbauer spectroscopy.

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Destruction of long-range order recorded within situsmall-angle x-ray diffraction in drying colloidal crystals

Physical Review E ◽

10.1103/physreve.69.031405 ◽

2004 ◽

Vol 69 (3) ◽

Cited By ~ 19

Author(s):

A. V. Petukhov ◽

I. P. Dolbnya ◽

D. G. A. L. Aarts ◽

G. J. Vroege

Keyword(s):

Long Range ◽

Colloidal Crystals ◽

Range Order ◽

Long Range Order ◽

X Ray Diffraction ◽

X Ray

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ANALISIS PERBANDINGAN PARAMETER LONG-RANGE ORDER SEBAGAI ACUAN KONTROL KUALITAS HASIL ANNEALING PASCA ECAP PADA Al-5052

Metal Indonesia ◽

10.32423/jmi.2017.v39.63-75 ◽

2017 ◽

Vol 39 (2) ◽

pp. 63

Author(s):

R. Ibrahim Purawiardi

Keyword(s):

Long Range ◽

Range Order ◽

Long Range Order ◽

X Ray Diffraction ◽

X Ray

Telah dilakukan analisis perbandingan parameter long-range order dalam satu sudut pandang pada logam paduan Al-5052 yang diberikan perlakuan ECAP dan annealing pasca ECAP. Sudut pandang yang dipakai adalah sudut pandang tegak lurus bidang (220). Dalam analisis, bidang fundamental adalah bidang (111), sementara bidang superlattice diasumsikan bidang (220). Terdapat 4 sampel uji Al-5052 yang digunakan. Keempat sampel diberikan perlakuan ECAP rute Bc sebanyak 4 pass. Kemudian, 3 dari 4 sampel diberikan perlakuan annealing pasca ECAP dengan variasi temperatur annealing 100 oC, 200 oC, dan 300 oC, sementara satu sampel tersisa sebagai kontrol pembanding. Karakterisasi dilakukan dengan analisis x-ray diffraction. Hasil analisis menunjukkan nilai parameter order sampel tanpa annealing, sampel dengan temperatur annealing 100 oC, sampel dengan temperatur annealing 200 oC, dan sampel dengan temperatur annealing 300 oC secara berturut-turut adalah 0.54526, 0.693152, 0.92553, dan 1.183165. Dengan demikian, terjadi perubahan kondisi dari kondisi lebih disordered menjadi lebih ordered akibat perlakuan annealing pasca ECAP. Sementara itu, kondisi fully ordered diprediksi terjadi saat penerapan temperatur annealing 226.065704 oC. Dari studi ini dapat disimpulkan bahwa metode perbandingan parameter order ini dapat digunakan sebagai acuan kontrol kualitas logam paduan Al-5052 setelah proses annealing pasca ECAP. Namun, analisis ini tidak direkomendasikan untuk menentukan nilai mutlak parameter order, namun hanya direkomendasikan untuk dibandingkan antar sampel satu sama lain.

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