Characterisation and evolution of the full size range of pores and fractures in rocks under freeze-thaw conditions using nuclear magnetic resonance and three-dimensional X-ray microscopy

2020 ◽  
Vol 271 ◽  
pp. 105616 ◽  
Author(s):  
Yong Sun ◽  
Cheng Zhai ◽  
Jizhao Xu ◽  
Yuzhou Cong ◽  
Lei Qin ◽  
...  
1990 ◽  
Vol 217 ◽  
Author(s):  
S.L. Dieckman ◽  
P. Rizo ◽  
N. Gopalsami ◽  
R. E. Botto

ABSTRACTThis paper presents a new, three-dimensional (3-D) nuclear magnetic resonance (NMR) imaging technique for spatially mapping proton distributions in green-state ceramic composites. The technique is based on a 3-D back-projection protocol for data acquisition, and a reconstruction technique based on 3-D Radon transform inversion. In principle, the 3-D methodology provides higher spatial resolution of solid materials than is possible with conventional slice-selection protocols. The applicability of 3-D NMR imaging has been demonstrated by mapping the organic additive distribution (2.5 wt.%) in cold-pressed Si34 whisker-reinforced Si34 ceramic composites. Three-dimensional X-ray computed tomography (CT) also has been employed for mapping voids and inclusions within the composite specimen. Combining information from both imaging modalities provides an extremely powerful nondestructive evaluation tool for materials characterization.


2007 ◽  
Vol 21 (3) ◽  
pp. 1548-1561 ◽  
Author(s):  
S. R. Kelemen ◽  
M. Afeworki ◽  
M. L. Gorbaty ◽  
M. Sansone ◽  
P. J. Kwiatek ◽  
...  

Tetrahedron ◽  
2001 ◽  
Vol 57 (49) ◽  
pp. 9789-9798 ◽  
Author(s):  
Shawn R Hitchcock ◽  
George P Nora ◽  
David M Casper ◽  
Michael D Squire ◽  
Christopher D Maroules ◽  
...  

1980 ◽  
Vol 58 (17) ◽  
pp. 1821-1828 ◽  
Author(s):  
Gary D. Fallon ◽  
Bryan M. Gatehouse ◽  
Allan Pring ◽  
Ian D. Rae ◽  
Josephine A. Weigold

Ethyl-3-amino-2-benzoyl-2-butenoate crystallizes from pentane as either the E (mp 82–84 °C) or the Z-isomer (mp 95.5–96.5 °C). The E isomer is less stable, and changes spontaneously into the Z, which bas been identified by X-ray crystallography. The structure is characterised by an N–H/ester CO hydrogen bond and a very long C2—C3 bond (1.39 Å). Nuclear magnetic resonance methods have been used to measure the rate of [Formula: see text] isomerization at several temperatures, leading to the estimate that the free energy of activation at 268 K is 56 ± 8 kJ.


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