Terbium metal organic framework: Microwave synthesis and selective sensing of nitrite

2020 ◽  
Vol 111 ◽  
pp. 107627 ◽  
Author(s):  
Pimchanok Tapangpan ◽  
Kitt Panyarat ◽  
Chaiyos Chankaew ◽  
Kate Grudpan ◽  
Apinpus Rujiwatra
Keyword(s):  
Microwave Synthesis ◽  
Metal Organic Framework ◽  
Metal Organic ◽  
Organic Framework

scholarly journals Microwave Assisted Surfactant-Thermal Synthesis of Metal-Organic Framework Materials

2020 ◽  
Vol 10 (13) ◽  
pp. 4563
Author(s):  
Cory Forsyth ◽  
Tyler Taras ◽  
Adam Johnson ◽  
Jessica Zagari ◽  
Crystal Collado ◽  
...  
Keyword(s):  
Microwave Synthesis ◽  
Metal Organic Framework ◽  
Application Of Surfactants ◽  
Green Solvents ◽  
X Ray Diffraction ◽  
Thermal Synthesis ◽  
Synthesis Time ◽  
Framework Materials ◽  
Metal Organic ◽  
Organic Framework

This research explores the application of surfactants as green solvents for the rapid microwave synthesis of metal-organic framework (MOF) materials. Lead, copper, and iron metal-organic framework materials were synthesized using surfactant-thermal microwave synthesis. The MOF materials were characterized by powder X-ray diffraction, infrared spectroscopy, scanning electron microscopy, and thermogravimetric analysis. With the exception of the iron MOF, which was expected to be amorphous, the MOF materials are crystalline, though generally exhibiting smaller crystals than those achieved with traditional solvothermal synthesis. This green synthetic method reduced synthesis time and reduced the use of traditional organic solvents as the reaction media.

Microwave Synthesis of a photoluminescent Metal-Organic Framework based on a rigid tetraphosphonate linker

2017 ◽  
Vol 455 ◽  
pp. 584-594 ◽  
Author(s):  
Ana D.G. Firmino ◽  
Ricardo F. Mendes ◽  
Duarte Ananias ◽  
Sérgio M.F. Vilela ◽  
Luís D. Carlos ◽  
...  
Keyword(s):  
Microwave Synthesis ◽  
Metal Organic Framework ◽  
Metal Organic ◽  
Organic Framework

Microwave Synthesis of the CPM-5 Metal Organic Framework

2012 ◽  
Vol 35 (6) ◽  
pp. 1085-1092 ◽  
Author(s):  
R. Sabouni ◽  
H. Kazemian ◽  
S. Rohani
Keyword(s):  
Microwave Synthesis ◽  
Metal Organic Framework ◽  
Metal Organic ◽  
Organic Framework

scholarly journals COMPARATIVE STUDY ON SYNTHESIS OF METAL ORGANIC FRAMEWORK-199 BY MICROWAVE AND SOLVOLTHERMAL PROCESS

2017 ◽  
Vol 126 (1C) ◽  
pp. 107
Author(s):  
Tran Vinh Thien
Keyword(s):  
Comparative Study ◽  
Microwave Synthesis ◽  
Metal Organic Framework ◽  
Textural Properties ◽  
Nitrogen Adsorption ◽  
X Ray Diffraction ◽  
Synthesis Time ◽  
Metal Organic ◽  
Adsorption Desorption ◽  
Organic Framework

<p>In the present paper, a comparative study on the synthesis of metal organic framework-199 by microwave and solvolthermal method was demonstrated.<strong> </strong>The obtained materials were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM), nitrogen adsorption/desorption isotherms and thermal gravity (TG). The microwave synthesis of MOF-199 has been compared to its conventional hydrothermal synthesis. It is found that by using microwave synthesis MOF-199 can be obtained in a much shorter synthesis time with improved yield and textural properties. It is supposed that the microwave energy emitted fast and uniformly, creating nuclei through the solution which quickly grew to crystals and both the nucleation and crystallization steps were accelerated. These make the microwave synthesis advantages over solvolthermal synthesis.<strong></strong></p>

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